Optical Microscope

183 cases · 1637 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Optical Microscope — sub-branches

As polished micrography 128Chromic Acid Electrolytic Etched 7Eletrolytically Etched Micrography by OM 11FeCl3+HCl+Ethanol Etched Micro 15FeCl3+HCl+H2O Etched Micro 28Glyceregia Etched Micrography by OM 7H2SO4+HNO3+H3PO4 Etched Micro 4Kalling Etched Micrography by OM 202Keller Etched Micrography by OM 58Kroll Etched Micrography by OM 15Micro by OM, HCl + Ethanol + Picric Acid 12Micro by OM, picric acid+FeCl3+H2O etch 4Micrography by OM 73Micrography by OM using A262 Method A 80Micrography by OM, HF + HNO3 + H2O etch 8NH4OH+H2O+H2O2 Etched Micro 8NaOH Electrolytic Etched Micro 108Nital Etched Micrography by OM 801Oxalic Acid Electrolytic Etch 68

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The micrography of the transverse section of the plate, as polished, close to the surface. The material presents intergranular corrosion and some grains were lost.
1184
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
13Cr SS longitudinal section micrography, at the collapsed region, showing a ferritic matrix structure (overtempered) with the previous austenite grain boundaries decorated by phases (carbides and probably martensite islands), indicating that the material was exposed to a high tempering temperature that created a partial austenitizing condition. It explains the material low toughness and lower strenght (than required).
437
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of the transverse section of the NEW TUBE, in the center of the thickness, showing the austenitic structure with primary carbides network.
410
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides
The low magnification micrography of the longitudinal section of the pin shows the localized corrosion associated to the non metallic inclusions.
89
VIEW
ML00016 / Apr.2017
SCC in Free Cutting 303SS
M - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
Cm - Micrography by OM using A262 Method ADf - Localized Corrosion
The micrography in the longitudinal section in the middle of the thickness shows a light banding. Quenched and tempered structure.
346
VIEW
ML00037 / Jun.2017
LAS Forging for Pump Body
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Longitudinal section of the main pipe showing as austenitic structure with small amount of delta ferrite, aligned. The white band in the center of the figure is a segregation band that was not fully etched.
133
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Micrography by OM using A262 Method ADf - Austenite
Longitudinal section of the wire, close to the surface. Galvanized layer (zinc), 50 microns thickness.
368
VIEW
ML00036 / Jan.2018
High Strength Medium Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Surface Layer
The micrography of a longitudinal section of the pipe, close to the internal surface, shows a general corrosion mechanism (with slow wall thickness loss), although the graphite/matrix interface is corroded preferentially.
569
VIEW
ML00034 / Apr.2017
45 Years Old Acquaduct Grey Cast Iron
M - Gray Cast ironP - Centrifugally Cast PipeAp - AcquaductCd - General Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion

More from these cases

ML00015 — Intergranular Corrosion of 304SS PlateM - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Microstructure of the plate in the center of the ¼” thickness. Equiaxed austenitic grains with delta ferrite stringers and grain boundary carbide precipitation (sensitization).
303
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Microstructure of the plate in the center of the ¼” thickness. Equiaxed austenitic grains with delta ferrite stringers and grain boundary carbide precipitation (sensitization).
201
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrographic aspect of a longitudinal section of the plate, close to the surface, in a region where it was detected intergranular corrosion up to 0,5 mm depth. As polished.
188
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrographic detail of intergranular corrosion, up to 0,5 mm depth. As polished.
171
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrographic aspect of a longitudinal section of the plate, close to the surface, in a region with intergranular corrosion. Several loose grains were removed, indicating that the structure was embrittled by the intergranular corrosion.
171
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion

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ML00039 — Collapse in Tubular 13CrM - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
13Cr SS in the longitudinal section, at the collapsed region. Non uniform structure (ferritic matrix and decorated prior austenite grain boundaries) that evidences an usuitable heat treatment during fabrication, and explains the material low strenght.
53
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
13Cr SS in the longitudinal section, at the collapsed region. Detail of the non uniform structure (ferritic matrix and decorated prior austenite grain boundaries) that evidences an usuitable heat treatment during fabrication, and explains the material low strenght.
48
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Prior Austenite Boundaries Decorated
13Cr SS in the transverse section, at the collapsed region, showing a non uniform structure that evidences an usuitable heat treatment during fabrication, and explains the material low strenght.
29
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Transverse Section
13Cr SS transverse section micrography, at the collapsed region, showing a ferritic matrix structure (overtempered) with the previous austenite grain boundaries decorated by phases (carbides and probably martensite islands), indicating that the material was exposed to a high tempering temperature that created a partial austenitizing condition. It explains the material low toughness and lower strenght (than required).
29
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Transverse Section
The micrography of the 13Cr SS in the transverse section, at the collapsed region, shows a ferritic matrix structure (overtempered) with the previous austenite grain boundaries decorated by phases (carbides and probably martensite islands), indicating that the material was exposed to a high tempering temperature that created a partial austenitizing condition. It explains the material low toughness and lower strenght (than required).
32
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Overtempered Structure

+3 more from this case →

ML00038 — Cast SS Tube for High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Micrography of the transverse section of the NEW TUBE, close to the external surface, showing the austenitic structure with primary carbides network.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Close to the External Surface
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects close to the external surface.
49
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Close to the External Surface
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects in the center of the thickness.
47
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Transverse Section
Micrography of the transverse section of the TUBE REMOVED FROM SERVICE, in the center of the thickness, showing the austenitic structure with primary carbides network and secondary precipitation.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation
Micrography of the transverse section of the TUBE REMOVED FROM SERVICE,close to the external surface, showing the austenitic structure with coalesced carbides and secondary precipitation.
39
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Close to the External Surface

+2 more from this case →

ML00016 — SCC in Free Cutting 303SSM - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
The pin microstructure in the longitudinal section shows austenitic structure, free from carbides, and sulfide inclusions that characterize the free cutting condition of this stainless steel.
77
VIEW
ML00016 / Apr.2017
SCC in Free Cutting 303SS
M - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
Cm - Micrography by OM using A262 Method ADf - Non Metallic Inclusions
The micrographic detail of the longitudinal section of the pin shows the localized corrosion associated to the non metallic inclusions.
67
VIEW
ML00016 / Apr.2017
SCC in Free Cutting 303SS
M - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
Cm - Micrography by OM using A262 Method ADf - Localized Corrosion
The micrographic detail of the longitudinal section of the pin shows the stress corrosion cracks propagating from crevice corrosion regions.
52
VIEW
ML00016 / Apr.2017
SCC in Free Cutting 303SS
M - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
Cm - Micrography by OM using A262 Method ADf - Branched Cracks
ML00037 — LAS Forging for Pump BodyM - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Typical manufacturing
Quenched and tempered structure of the 1" thick forging presenting a light banding.
43
VIEW
ML00037 / Jun.2017
LAS Forging for Pump Body
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Banded Structure
Longitudinal section in the middle of the thickness. Quenched and tempered structure.
38
VIEW
ML00037 / Jun.2017
LAS Forging for Pump Body
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Martensite
Vickers microhardness in and out of the segregation bands. The average hardness value in the band (1, 2 and 3 identations) is 354 HV 50g and out of the band (4, 5 and 6 identations) is 286 HV 50g.
33
VIEW
ML00037 / Jun.2017
LAS Forging for Pump Body
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Banded Structure
ML00006 — Vibration Induced Fatigue in 304SSM - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Longitudinal section of the main pipe showing as austenitic structure with small amount of delta ferrite, aligned (black dots).
116
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrography transverse to the weld and to the fracture surface (right side of the figure).
116
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Micrography by OM using A262 Method ADf - Fracture
Micrography of the section transverse to the weld and in a region close to the fracture surface (to the right side of the figure). The secondary fatigue microcracks are associated to the stress concentration raisers of the margin of the weld, irregular.
110
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Micrography by OM using A262 Method ADf - Fatigue Crack
ML00036 — High Strength Medium Carbon Steel WireM - Medium Carbon SteelP - WireAp - OffshoreCd - Typical manufacturing
Longitudinal section of the 3.6 mm wire, presenting a refined structure.
46
VIEW
ML00036 / Jan.2018
High Strength Medium Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Longitudinal section of the 3.6 mm wire, presenting a strain hardened structure, predominantly perlitic.
41
VIEW
ML00036 / Jan.2018
High Strength Medium Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Longitudinal section of the 3.6 mm wire, presenting a strain hardened structure, predominantly perlitic.
38
VIEW
ML00036 / Jan.2018
High Strength Medium Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Predominantly Pearlitic
Transverse section of the 3.6 mm wire, presenting a refined structure.
32
VIEW
ML00036 / Jan.2018
High Strength Medium Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Transverse Section
Transverse section of the 3.6 mm wire, presenting a refined structure predominatly perlitic.
19
VIEW
ML00036 / Jan.2018
High Strength Medium Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Transverse Section

+1 more from this case →

ML00034 — 45 Years Old Acquaduct Grey Cast IronM - Gray Cast ironP - Centrifugally Cast PipeAp - AcquaductCd - General Corrosion
Micrographic detail of the graphite/matrix interface corrosion, leading to a general corrosion loss.
189
VIEW
ML00034 / Apr.2017
45 Years Old Acquaduct Grey Cast Iron
M - Gray Cast ironP - Centrifugally Cast PipeAp - AcquaductCd - General Corrosion
Cm - Nital Etched Micrography by OMDf - Graphite in Flakes
Micrography of the longitudinal section of the pipe, close to the internal surface, showing graphite in flakes and ferritic matrix with small regions of perlite.
231
VIEW
ML00034 / Apr.2017
45 Years Old Acquaduct Grey Cast Iron
M - Gray Cast ironP - Centrifugally Cast PipeAp - AcquaductCd - General Corrosion
Cm - Nital Etched Micrography by OMDf - Predominantly Ferritic Matrix
Micrography of the longitudinal section of the pipe, close to the internal surface, showing graphite in flakes and ferritic matrix with small regions of perlite and eutetic in the middle of the perlite colonies.
192
VIEW
ML00034 / Apr.2017
45 Years Old Acquaduct Grey Cast Iron
M - Gray Cast ironP - Centrifugally Cast PipeAp - AcquaductCd - General Corrosion
Cm - Nital Etched Micrography by OMDf - Predominantly Ferritic Matrix
Micrography of the longitudinal section of the pipe, in the center of the thickness. Graphite in flakes and ferritic matrix with small regions of perlite.
179
VIEW
ML00034 / Apr.2017
45 Years Old Acquaduct Grey Cast Iron
M - Gray Cast ironP - Centrifugally Cast PipeAp - AcquaductCd - General Corrosion
Cm - Nital Etched Micrography by OMDf - Predominantly Ferritic Matrix
Micrography of the longitudinal section of the pipe, in the center of the thickness. Graphite in flakes and ferritic matrix with small regions of perlite.
162
VIEW
ML00034 / Apr.2017
45 Years Old Acquaduct Grey Cast Iron
M - Gray Cast ironP - Centrifugally Cast PipeAp - AcquaductCd - General Corrosion
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite

+4 more from this case →