Optical Microscope

183 cases · 1637 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Optical Microscope — sub-branches

As polished micrography 128Chromic Acid Electrolytic Etched 7Eletrolytically Etched Micrography by OM 11FeCl3+HCl+Ethanol Etched Micro 15FeCl3+HCl+H2O Etched Micro 28Glyceregia Etched Micrography by OM 7H2SO4+HNO3+H3PO4 Etched Micro 4Kalling Etched Micrography by OM 202Keller Etched Micrography by OM 58Kroll Etched Micrography by OM 15Micro by OM, HCl + Ethanol + Picric Acid 12Micro by OM, picric acid+FeCl3+H2O etch 4Micrography by OM 73Micrography by OM using A262 Method A 80Micrography by OM, HF + HNO3 + H2O etch 8NH4OH+H2O+H2O2 Etched Micro 8NaOH Electrolytic Etched Micro 108Nital Etched Micrography by OM 801Oxalic Acid Electrolytic Etch 68

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The longitudinal section of the shaft, in the center of the thickness, shows a coarse structure, and a ferritic/bainitic structure with pearlite islands.
97
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrography of the fork handle in the transverse section, curved, presenting differences between grain size and morphology. In the middle section there are elongated grains and close to the surfaces there are smaller and more equiaxed grains.
81
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Transverse Section
Micrography of a transverse section of the pipe, presenting a refined duplex structure. The ferrite is blue/red and the austenite is white/yellow.
95
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Micrography of a transverse section of the seamless pipe, presenting a ferritic-pearlitic structure.
84
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure.
55
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrography of the plate in a section, in the middle of the thickness. The aligned pitting is associated to the chemical etch of inclusions and second phases. The structure is granular but the grain boundaries do not appear at that magnification, originally 50x.
50
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Aligned particles
Micrography of a longitudinal section of the sleeve, at the external surface where there are two layers of coating. The electrolytic etch evidenced the duplex stainless steel substrate (bottom of the figure) and the weave interface of the substrate and the first thermal spray layer, about 1 mm thick, in a stainless steel. The surface layer, of tugnsten carbide, about 0.2 mm thick, is black and not clearly visible in this figure.
50
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - External Surface
Micrography of the plate in the middle of the thickness, showing the aligned structure tyical of a rolling process. The sample was mechanically-electrolitically polished and etched with HF (10%) + HNO3 (5%) +H2O (85%) solution.
28
VIEW
ML00144 / Aug.2018
Impact of a .380 Winchester on Ti64 Plate
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Micrography by OMDf - Alpha and Beta

More from these cases

ML00152 — Low Alloy Steel Pump ShaftM - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
The coarse structure in the center of the shaft thickness is evidenced by free ferrite islands at the previous austenite grains. The presence of a pearlitic structure evidences the slow cool of the material.
85
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Coarse Structure
The longitudinal section of the shaft, at the surface, also shows a coarse structure, and a ferritic/bainitic structure with pearlite islands. There is only a small refining in the previous austenite grain boundaries, indicating that the material was not heat treated.
75
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
The longitudinal section of the shaft, at the surface, presenting only a small refining in the previous austenite grain boundaries than in the center, indicating that the material was slowed colled from forming and not heat treated.
67
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Micrographic detail of the pearlitic structure at the surface of the shaft thickness.
69
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Pearlite
ML00151 — Ferritic Stainless Steel of a Flatware ForkM - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Micrography of the fork handle in the center of the transverse section, curved, presenting larger ferritic grains with elongated morphology.
70
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Granular structure
Micrographic detail of the ferritic grains with elongated morphology in the center of the transverse section, curved.
58
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Ferrite
The micrography as polished in the transverse section shows a small amount of inclusions in the steel.
62
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - As polished micrographyDf - Non Metallic Inclusions
Detail of the non metallic inclusions in the steel. The yellow and black colours and morphologies suggest Ti base and oxides.
65
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - As polished micrographyDf - Non Metallic Inclusions
Micrography of a longitudinal section of the fork, at the scoop to handle position (scoop to the right of the figure and handle to the left). The full thickness is presented in the image and it is possible to see that in the handle location the ferritic grains are larger in the center of the thickness than close to the surfaces, and in the scoop position the grains tend to be more uniform through the thickness.
50
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Longitudinal Section

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ML00150 — Vibration Induced Fatigue in a SS Oil PipingM - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Micrography of a transverse section of the pipe, presenting a refined duplex structure. The ferrite is blue/red and the austenite is white/yellow.
88
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Micrographic detail of the ferritic/austenitic structure of the pipe, in a transverse section. The ferrite is blue/red and the austenite is white/yellow.
84
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Banded Structure
Micrography of a transverse section of the fititng, presenting a coarser structure. The ferrite is blue/red and the austenite is white/yellow.
77
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Coarse Structure
Micrography of a transverse section of the fititng, presenting a coarser structure. The ferrite is blue/red and the austenite is white/yellow.
81
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Micrography of a transverse section of the fititng, presenting a coarser structure. The ferrite is red/orange and the austenite is white/yellow.
80
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Duplex structure

+16 more from this case →

ML00149 — Vibration Induced Fatigue in a Gas PipingM - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Micrography of a transverse section of the seamless pipe, presenting a ferritic-pearlitic structure.
70
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography showing the cracking starting point, in the pipe, exactly at the margin of the weld.
292
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Margin of the Weld Crack
Micrographic detail of the cracking starting point, in the pipe, exactly at the margin of the weld.
33
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Fatigue Crack
Micrography of a section tranverse to the pipe and to the weld between the 8"pipe and the 2" fitting weldolet. The crack starts exactly at the margin of the weld and propagates in the pipe longitudinal direction, in a straight line, not related to any metallurgical aspect.
30
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Micrography by OMDf - Cracking
Micrographic detail of the fatigue crack propagation in the pipe longitudinal direction, in a straight line, not related to any metallurgical aspect.
29
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Micrography by OMDf - Fatigue Crack

+2 more from this case →

ML00148 — Brittle Fracture of a 420 SS Barrel NutM - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Microstructural aspect of a longitudinal section of the nut, in the middle of the thickness. Martensitic structure, banded.
46
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Microstructural detail of the banded structure. The rough aspect of the band is created by the carbides (better seen in the higher magnification image) in the segregation band.
38
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrographic detail of the nut longitudinal section presenting the large carbides (white islands) in the segregation band, and small precipitates all through the martensite matrix, indicating that this high carbon steel was tempered in a high temperature. The 36HRc hardness also confirms this high tempering temperature.
39
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Martensite
Vickers microhardness identations using 100 grams. In a position out of the band (top line). Values from left to right, 380HV; 390HV and 394HV. In a position inside the band (bottom line). Values from left to right, 433HV, 483HV and 473 HV.
33
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure. It is possible to see that the contact pressure in the thread caused a surface plastically deformation.
24
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure

+6 more from this case →

ML00145 — Impact of a .380 Winchester on 6061 T6 PlateM - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Micrography of the plate in a section, in the middle of the thickness, in a position where the plate was not affected by the shot. The microstructure is granular although the grain boundaries are not resolvable at this magnification. The black spots are localized corrosion in aligned particles.
49
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Aligned particles
Micrographic detail of the plate in the middle of the thickness. At this magnification it is possible to see the grain boundaries and the black spots are localized etching in aligned particles.
43
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Granular structure
Micrographic detail of the plate in the middle of the thickness. At this magnification it is possible to see the grain boundaries and the black spots are localized etching in aligned particles.
37
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Granular structure
Micrography of the damaged plate at the side of the bullet impact, top of the figure. The perforated hole expulsed the material to the top and bottom directions. There are evidences of plastic deformation of the plate microstructure and the hardness level close to the hole increased from 123 HV to 131 HV (1kg)
17
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Strain Hardened
Micrography of the damaged plate at the side of the bullet impact, top of the figure. The perforated hole expulsed the material to the top and bottom directions and the microstructure shows plastic deformation.
16
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Plastic Deformation

+10 more from this case →

ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Micrography of a longitudinal section of the sleeve close to the external surface, evidencing a tugnsten carbide thermal spray layer, thickness about 0.2 mm, at the sleeve outer diameter (OD), black due to the etch (top of the figure). This WC layer was deposited over a stainless steel layer disposed in several layers, non etched.
42
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Thermal Spray Layer
Micrographic detail of the interface between the two thermal spray layers, the first one in stainless steel (bottom of the figure) and the second one, at the surface,in tungsten carbide (top of the figure). The micrographic sample is etched and that is why the WC is dark (black) and the stainless steel is light (non etched).
41
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Thermal Spray Layer
Micrography of the longitudinal section of the sleeve, at the interface between the substrate and the first thermal spray layer. The substrate (bottom of the figure) shows a ferritic-austenitic microstructure and detrimental phases that look like sigma. The thermal spray layer (top of the figure) presents the non-etched stainless steel, disposed in layers, with oxides (gray) and voids (black). The substrate is deformed in a thin layer at the interface.
38
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Close to the External Surface
Micrographic detail of the interface between the substrate and the first thermal spray layer. The substrate (bottom of the figure) shows a ferritic-austenitic microstructure and detrimental phases that look like sigma at the delta and gamma interface. The thermal spray layer (top of the figure) presents the non-etched stainless steel, disposed in layers, with oxides (gray) and voids (black). The substrate is deformed in a thin layer at the interface.
34
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrography of the longitudinal section of the cast sleeve in the middle of the thickness. The microstructure is coarse, austenitic ferritic.
34
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - In the Center of the Thickness

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ML00144 — Impact of a .380 Winchester on Ti64 PlateM - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Micrography showing the alpha plus beta microstructure in the middle of the thickness. The sample was mechanically-electrolitically polished and etched with HF (10%) + HNO3 (5%) +H2O (85%) solution.
32
VIEW
ML00144 / Aug.2018
Impact of a .380 Winchester on Ti64 Plate
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Micrography by OMDf - Alpha and Beta
Micrographic detail of the plate, showing the alpha (light grains as a matrix) plus beta (dark phase) microstructure. Etched with HF (10%) + HNO3 (5%) +H2O (85%) solution.
28
VIEW
ML00144 / Aug.2018
Impact of a .380 Winchester on Ti64 Plate
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Micrography by OMDf - Alpha and Beta
Micrographic detail of the plate, showing the aligned beta phase (dark) in the alpha grains (light) microstructure. Etched with HF (10%) + HNO3 (5%) +H2O (85%) solution.
24
VIEW
ML00144 / Aug.2018
Impact of a .380 Winchester on Ti64 Plate
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Micrography by OMDf - Alpha and Beta
Micrographic detail of the plate, showing the aligned beta (dark phase) in alpha microstructure. Etched with HF+ HNO3+H2O solution.
26
VIEW
ML00144 / Aug.2018
Impact of a .380 Winchester on Ti64 Plate
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Micrography by OMDf - Alpha and Beta
Micrography by SEM of the plate in the middle of the thickness, showing the alpha microstructure (dark grains) and the beta phase (light). Etched with HF+HNO3+H2O.
35
VIEW
ML00144 / Aug.2018
Impact of a .380 Winchester on Ti64 Plate
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Micrography by OMDf - Alpha and Beta

+12 more from this case →