Optical Microscope

183 cases · 1637 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Optical Microscope — sub-branches

As polished micrography 128Chromic Acid Electrolytic Etched 7Eletrolytically Etched Micrography by OM 11FeCl3+HCl+Ethanol Etched Micro 15FeCl3+HCl+H2O Etched Micro 28Glyceregia Etched Micrography by OM 7H2SO4+HNO3+H3PO4 Etched Micro 4Kalling Etched Micrography by OM 202Keller Etched Micrography by OM 58Kroll Etched Micrography by OM 15Micro by OM, HCl + Ethanol + Picric Acid 12Micro by OM, picric acid+FeCl3+H2O etch 4Micrography by OM 73Micrography by OM using A262 Method A 80Micrography by OM, HF + HNO3 + H2O etch 8NH4OH+H2O+H2O2 Etched Micro 8NaOH Electrolytic Etched Micro 108Nital Etched Micrography by OM 801Oxalic Acid Electrolytic Etch 68

Results

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A small sample was removed from the steam drum and the micrography shows that the cracks are intergranular (previous austenite) and located in the weld metal.
285
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
Tempered martensitic structure of the plate base metal.
93
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of a longitudinal section of the shell plate base metal, presenting a typical ferritic-perlitic microstructure.
149
VIEW
ML00008 / Nov.2017
Cold Cracks in CMn Steel Pressure Vessel
M - CMn SteelP - In Field WeldAp - BoilerCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
The micrography of the transverse section shows coarse grains and biphasic structure. Alpha grains and a lamellar eutectoid structure can be observed in the material.
464
VIEW
ML00044 / Feb.2017
Centrifugally Cast CuAl Bushing
M - Aluminum BronzeP - Cast BushingAp - EngineCd - Removed From Service
Cm - NH4OH+H2O+H2O2 Etched MicroDf - Close to the External Surface
The micrography of the tube shows a granular structure and light deformation lines. No evidences of corrosion from the external surface (upper side of the figure) or internal surface (lower side of the figure).
440
VIEW
ML00043 / Apr.2017
CuNi Condenser Tube
M - CupronickelP - Seamless tubeAp - Heat ExchangerCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Longitudinal Section
Transverse section of the blade showing large grains of this poliycristaline cast material.
421
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - H2SO4+HNO3+H3PO4 Etched MicroDf - Coarse Structure
The micrography of a transverse section of the shaft shows the granular austenitic structure close to the surface of the shaft.
67
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - At the Surface
The cast iron microstructure is predominatly ferritic with graphite nodules.
169
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Graphite in Nodules

More from these cases

ML00020 — Intergranular SCC in Boiler Steam Drum RepairM - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
The micrography of the small sample removed from the steam drum shows that the cracks are intergranular (previous austenite) and located in the weld metal.
274
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
Secondary cracks in the weld metal showing an intergranular morphology. Stress Corrosion Cracking.
249
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
Detail of the secondary cracks in the weld metal with intergranular morphology. Stress Corrosion Cracking.
251
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
Detail of the intergranular stress corrosion cracking of the drum shell weld repair.
217
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
ML00010 — Cold Cracks in a Gouged Weld MetalM - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Detail of the tempered martensitic structure of the plate base metal. Hardness level of 27 HRc.
92
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
Low magnification micrography of a transverse section of the weld at the heat affected zone region. The macrosection was hardness tested and the base metal hardness is 27HRc, the HAZ is 32HRc and the weld metal is 45HRc, revealing something wrong in the weld metal at the position close to the cracked area.
79
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Transverse Section
High temperature heat affected zone of the plate, welded in repair. The micrography was taken from a sample collected close to the cracked region, but not containing any macroscopic cracking.
76
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Detail of the high temperature heat affected zone of the plate, welded in repair.
69
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
The weld metal, hard, presented a martensitic structure, probably due to the localized increase in carbon content, from the unsuitable carbon arc gouging procedure.
63
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Weld Metal

+5 more from this case →

ML00008 — Cold Cracks in CMn Steel Pressure VesselM - CMn SteelP - In Field WeldAp - BoilerCd - Welding Defect
Higher magnification of the ferritic-perlitic microstructure of the shell plate in the longitudinal section.
129
VIEW
ML00008 / Nov.2017
Cold Cracks in CMn Steel Pressure Vessel
M - CMn SteelP - In Field WeldAp - BoilerCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Cold cracking of the fillet weld adopted to attach a flat support into a vessel shell in the internal side, using an unsuitable welding procedure that created a too high hardness HAZ.
123
VIEW
ML00008 / Nov.2017
Cold Cracks in CMn Steel Pressure Vessel
M - CMn SteelP - In Field WeldAp - BoilerCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Cold cracking of the fillet weld adopted to attach a flat support into a vessel shell in the internal side, using an unsuitable welding procedure that created a too high hardness HAZ. The cracks are mainly located at the fusion line.
118
VIEW
ML00008 / Nov.2017
Cold Cracks in CMn Steel Pressure Vessel
M - CMn SteelP - In Field WeldAp - BoilerCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Cold cracking of the fillet weld adopted to attach a flat support into a vessel shell in the internal side, using an unsuitable welding procedure that created a too high hardness HAZ. Several internal cracks at the fusion line.
101
VIEW
ML00008 / Nov.2017
Cold Cracks in CMn Steel Pressure Vessel
M - CMn SteelP - In Field WeldAp - BoilerCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Cold cracking of the fillet weld adopted to attach a flat support into a vessel shell using an unsuitable welding procedure, with a low preheating and no PWHT. Cracks propagated in the heat affected zone.
99
VIEW
ML00008 / Nov.2017
Cold Cracks in CMn Steel Pressure Vessel
M - CMn SteelP - In Field WeldAp - BoilerCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks

+1 more from this case →

ML00044 — Centrifugally Cast CuAl BushingM - Aluminum BronzeP - Cast BushingAp - EngineCd - Removed From Service
Micrographic detail of the structure at the external surface.
58
VIEW
ML00044 / Feb.2017
Centrifugally Cast CuAl Bushing
M - Aluminum BronzeP - Cast BushingAp - EngineCd - Removed From Service
Cm - NH4OH+H2O+H2O2 Etched MicroDf - Close to the External Surface
The micrography of the transverse section shows coarse grains and biphasic structure. No diferentes close to the internal surface. Alpha grains and a lamellar eutectoid structure can be observed in the material.
46
VIEW
ML00044 / Feb.2017
Centrifugally Cast CuAl Bushing
M - Aluminum BronzeP - Cast BushingAp - EngineCd - Removed From Service
Cm - NH4OH+H2O+H2O2 Etched MicroDf - Close to the Internal Surface
Micrographic detail of the structure at the internal surface.
38
VIEW
ML00044 / Feb.2017
Centrifugally Cast CuAl Bushing
M - Aluminum BronzeP - Cast BushingAp - EngineCd - Removed From Service
Cm - NH4OH+H2O+H2O2 Etched MicroDf - Close to the Internal Surface
Detail of the structure in the center of the thickness. Alpha grains and lamellar eutectoid structure.
28
VIEW
ML00044 / Feb.2017
Centrifugally Cast CuAl Bushing
M - Aluminum BronzeP - Cast BushingAp - EngineCd - Removed From Service
Cm - NH4OH+H2O+H2O2 Etched MicroDf - In the Center of the Thickness
ML00043 — CuNi Condenser TubeM - CupronickelP - Seamless tubeAp - Heat ExchangerCd - Removed From Service
The material structure is monophasic.
110
VIEW
ML00043 / Apr.2017
CuNi Condenser Tube
M - CupronickelP - Seamless tubeAp - Heat ExchangerCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Single phase
Detail of the structure at the surface.
79
VIEW
ML00043 / Apr.2017
CuNi Condenser Tube
M - CupronickelP - Seamless tubeAp - Heat ExchangerCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - At the Surface
ML00042 — Gas Turbine Blade IN 939, CoatedM - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Micrography close to the surface of the blade, showing the diffusion coating (aluminum base alloy) that is still sound. No strong oxidation or erosion was detected.
53
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - H2SO4+HNO3+H3PO4 Etched MicroDf - Coating
Micrography as polished of the region where there was a refrigeration hole, presenting a cracking.
35
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - Micrography by OMDf - Cracking
The cracking from the refrigeration hole presents an intergranular morphology, as shown in the micrography of a transverse section of the blade.
35
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - H2SO4+HNO3+H3PO4 Etched MicroDf - Intergranular Cracking
ML00041 — Fatigue Fracture of Inconel 718 Spline ShaftM - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Micrographic detail of the granular austenitic structure close to the surface of the shaft.
64
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - At the Surface
Granular austenitic structure close to the surface of the shaft.
61
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - Austenite
The micrography of a transverse section of the shaft shows a duplex grain size structure in the center of the shaft.
49
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - In the Center of the Thickness
The micrography of a transverse section of the shaft shows a duplex grain size structure in the center of the shaft. This conditions was probably generated due to the delta phase presented in segregated bands in the center of the original bar.
56
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - In the Center of the Thickness
Duplex grain size structure, austenitic. The small grains are probably due to the arresting effect of the delta phase during fabrication in high temperature.
47
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - Duplex structure

+2 more from this case →

ML00040 — Brittle Fracture of a Valve StemM - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
The micrography of the stem at the fracture region shows a flat fracture with transgranular clevage at the ferritic structure.
137
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Fracture
Micrography presenting a detail of the fracture surface opening to the graphite nodules.
139
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Fracture