Optical Microscope

4 cases · 48 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Surface layer of Thermal Spray clear all

Optical Microscope — sub-branches

As polished micrography 19NaOH Electrolytic Etched Micro 11Nital Etched Micrography by OM 18

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Micrography of a longitudinal section of the sleeve, at the external surface where there are two layers of coating. The electrolytic etch evidenced the duplex stainless steel substrate (bottom of the figure) and the weave interface of the substrate and the first thermal spray layer, about 1 mm thick, in a stainless steel. The surface layer, of tugnsten carbide, about 0.2 mm thick, is black and not clearly visible in this figure.
50
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - External Surface
Micrography, as polished, of the transverse section of the forged pin with the layer applied by a (thermal) spray and fuse process. The layer presented entrapped pores and globular oxides. It was melted after application by thermal spray (in this case using a flame) but the pin was not heat treated after the full application and melting of the layer and the base metal is ferritc-pearlitic.
51
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - As polished micrographyDf - Transverse Section
Micrography, as polished, of the transverse section of the forged pin with the layer applied by a (thermal) spray and fuse process. The structure of the layer that is 0.7 mm thick, presented entrapped pores and globular oxides. The layer was melted after application by thermal spray (in this case using a flame) and the pin was quenched and tempered after the full application and melting of the layer.
360
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - As polished micrographyDf - Transverse Section
Micrography of the thermal spray (TS) layer showing the different alloys, gray oxides and black voids. The Ni base TS alloy is of a yellow colour at the interface with the shaft substrate (in the left). The Cr base TS alloy appears white, similar to the shaft substrate. Longitudinal section of the shaft.
42
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - As polished micrographyDf - Coating Layer

More from these cases

ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Micrography of a longitudinal section of the sleeve close to the external surface, evidencing a tugnsten carbide thermal spray layer, thickness about 0.2 mm, at the sleeve outer diameter (OD), black due to the etch (top of the figure). This WC layer was deposited over a stainless steel layer disposed in several layers, non etched.
42
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Thermal Spray Layer
Micrographic detail of the interface between the two thermal spray layers, the first one in stainless steel (bottom of the figure) and the second one, at the surface,in tungsten carbide (top of the figure). The micrographic sample is etched and that is why the WC is dark (black) and the stainless steel is light (non etched).
41
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Thermal Spray Layer
Micrography of the longitudinal section of the sleeve, at the interface between the substrate and the first thermal spray layer. The substrate (bottom of the figure) shows a ferritic-austenitic microstructure and detrimental phases that look like sigma. The thermal spray layer (top of the figure) presents the non-etched stainless steel, disposed in layers, with oxides (gray) and voids (black). The substrate is deformed in a thin layer at the interface.
38
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Close to the External Surface
Micrographic detail of the interface between the substrate and the first thermal spray layer. The substrate (bottom of the figure) shows a ferritic-austenitic microstructure and detrimental phases that look like sigma at the delta and gamma interface. The thermal spray layer (top of the figure) presents the non-etched stainless steel, disposed in layers, with oxides (gray) and voids (black). The substrate is deformed in a thin layer at the interface.
34
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrography of the longitudinal section of the cast sleeve in the middle of the thickness. The microstructure is coarse, austenitic ferritic.
34
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - In the Center of the Thickness

+12 more from this case →

ML00110 — Non Conformance in Spray and Fuse PinM - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Micrography, as polished, of the transverse section of the forged pin with the layer applied by a (thermal) spray and fuse process. The layer was melted after thermal spray application and the layer presents a continuous matrix, but there are globular oxides and pores entrapped.
36
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - As polished micrographyDf - Surface Layer
Micrographic detail, as polished, of the transverse section of the forged pin at the interface between the pin and the spray and fuse layer. The interface presents globular oxides and small pores, entrapped.
35
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - As polished micrographyDf - Surface Layer
Low magnification micrography of the interface between the pin and the spray and fuse layer. Close to the surface, under the layer, the pin presents a ferritic perlitic structure, non conform with the high strenght requirement. Transverse section.
37
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - As polished micrographyDf - Low Mag
Micrography of the pin close to the interface with the spray and fuse layer. Transverse section. The fuse was conducted in high temperature and the pin was cooled very slowly, forming a ferritic-perlitic structure even for this high hardenability base metal.
35
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Low magnification micrography of the pin in the center of the 25 mm thickness. Ferritic-pearlitic structure of the material that slowly cooled after spray and fuse application. Transverse section.
25
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Base Metal

+5 more from this case →

ML00109 — Thermal Spray and Fuse Layer in Forged PinM - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Micrography, as polished, of the transverse section of the forged pin with the layer applied by a (thermal) spray and fuse process. The layer was melted after thermal spray application and the layer presents a continuous matrix, but there are globular oxides and pores entrapped.
29
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - As polished micrographyDf - Surface Layer
Micrographic detail, as polished, of the transverse section of the forged pin at the interface between the pin and the spray and fuse layer. The pin was heat treated after the thermal spray, and fuse treatment. The interface presents a higher concentration of globular oxides and pores, entrapped.
23
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - As polished micrographyDf - Surface Layer
Low magnification micrography of the interface between the pin and the spray and fuse layer. Close to the surface, under the layer, the pin presents a quenched and tempered structure, compatible with a high strenght requirement. Transverse section.
20
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - Nital Etched Micrography by OMDf - Surface Layer
Micrography of the pin close to the interface with the spray and fuse layer. Transverse section. The fuse is conducted in high temperature and the pin was quenched and tempered after the thermal spray deposition and fuse by flame (in this case the melting of the applied layer was conducted by a oxifuel flame.
21
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the tempered martensite structure close to the interface with the spray and fuse layer. Transverse section. The fuse is conducted in high temperature and the pin was heat treated after the thermal spray deposition and fuse.
16
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - Nital Etched Micrography by OMDf - Martensite

+3 more from this case →

ML00108 — Thermal Spray Layer in a Pinion ShaftM - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Micrographic detail, as polished in a longitudinal section, of the interface between the shaft substrate and the thermal spray layer. In the left it is the shaft substrate also presenting parts of aligned inclusions (gray). In the center it is the Ni base TS alloy and in the right it is the Cr base TS alloy. There are also black voids and grey oxides.
33
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - As polished micrographyDf - Coating Layer
Micrography of the interface between the shaft surface and the thermal spray layer. The shaft steel presents a quenched and tempered structure. Longitudinal section.
32
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - Nital Etched Micrography by OMDf - Coating Layer
Micrographic detail of the interface between the shaft surface and the thermal spray layer. The shaft steel presents a quenched and tempered structure. Longitudinal section.
33
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - Nital Etched Micrography by OMDf - Coating Layer
Micrographic detail of the interface between the shaft surface and the thermal spray layer. The shaft steel presents a quenched and (over) tempered structure. Longitudinal section.
35
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - Nital Etched Micrography by OMDf - Coating Layer
Shaft microstructure in the longitudinal section, showing aligned segregations typical of the material forming.
31
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - Nital Etched Micrography by OMDf - Longitudinal Section

+4 more from this case →