Optical Microscope

5 cases · 22 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

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FeCl3+HCl+H2O Etched Micro 2Kalling Etched Micrography by OM 11Micrography by OM, HF + HNO3 + H2O etch 3NaOH Electrolytic Etched Micro 6

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Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
74
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a longitudinal section of the pin, presenting a tempered martensitic structure with aligned delta ferrite and carbide phases.
80
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
The micrography of a transverse section of the shaft shows the granular austenitic structure close to the surface of the shaft.
67
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - At the Surface
The bar presented a large prior beta grain size and acicular alpha. Biphasic structure.
420
VIEW
ML00028 / Jan.2017
Titanium Bar for Subsea Application
M - Ti6Al4VP - BarAp - StructureCd - Typical manufacturing
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Coarse Structure
The micrography of the pin far from the fracture surface shows a biphasic brass, and Pb inclusions that are intentional to give a free machining condition for the alloy.
76
VIEW
ML00007 / Dec.2020
Free Machining Brass in Shear Pin
M - BrassP - Machined PartAp - LiftingCd - Shear
Cm - FeCl3+HCl+H2O Etched MicroDf - Two phases

More from these cases

ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
61
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. The ferrite amount, measured by metallographic method, manual counting, is 59%.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. The average austenite spacing is 80 microns, a lot larger than the maximum allowed in the specification, of 30 microns. No detrimental phases were identified at the ferrite/austenite interfaces, but the ferrite phase presented a rough aspect. Higher magnification analysis would be required to identify precipitation.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrographic detail of the ferrite and austenite structure in the transverse section of the forged bar, in the center of the thickness.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the ferrite and austenite structure in the longitudinal section of the forged bar, in the center of the thickness.
55
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
ML00046 — Brittle Fracture of SS Shear PinM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Micrographic detail of the pin structure, in the longitudinal section, at the segregated band with aligned inclusions and phases, delta ferrite and carbides.
70
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the pin structure, in the longitudinal section, presenting a martensitic matriz, aligned inclusions (grey, delta ferrite islands (poligonal white phases) and carbides (also white phases) surrounding the delta ferrite.
64
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
ML00041 — Fatigue Fracture of Inconel 718 Spline ShaftM - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Micrographic detail of the granular austenitic structure close to the surface of the shaft.
64
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - At the Surface
Granular austenitic structure close to the surface of the shaft.
61
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - Austenite
The micrography of a transverse section of the shaft shows a duplex grain size structure in the center of the shaft.
49
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - In the Center of the Thickness
The micrography of a transverse section of the shaft shows a duplex grain size structure in the center of the shaft. This conditions was probably generated due to the delta phase presented in segregated bands in the center of the original bar.
56
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - In the Center of the Thickness
Duplex grain size structure, austenitic. The small grains are probably due to the arresting effect of the delta phase during fabrication in high temperature.
47
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - Duplex structure

+2 more from this case →

ML00028 — Titanium Bar for Subsea ApplicationM - Ti6Al4VP - BarAp - StructureCd - Typical manufacturing
The bar presented alpha plus beta phases, acicular alpha and coarse prior beta grains.
97
VIEW
ML00028 / Jan.2017
Titanium Bar for Subsea Application
M - Ti6Al4VP - BarAp - StructureCd - Typical manufacturing
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Two phases
Acicular alpha structure in a biphasic alloy of a large prior beta grain size. 4" diameter bar.
100
VIEW
ML00028 / Jan.2017
Titanium Bar for Subsea Application
M - Ti6Al4VP - BarAp - StructureCd - Typical manufacturing
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Acicular Alpha
ML00007 — Free Machining Brass in Shear PinM - BrassP - Machined PartAp - LiftingCd - Shear
The micrography of the pin at the fracture surface shows a strong plastic deformation as expected during shearing.
69
VIEW
ML00007 / Dec.2020
Free Machining Brass in Shear Pin
M - BrassP - Machined PartAp - LiftingCd - Shear
Cm - FeCl3+HCl+H2O Etched MicroDf - Plastic Deformation