Optical Microscope

183 cases · 1637 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Optical Microscope — sub-branches

As polished micrography 128Chromic Acid Electrolytic Etched 7Eletrolytically Etched Micrography by OM 11FeCl3+HCl+Ethanol Etched Micro 15FeCl3+HCl+H2O Etched Micro 28Glyceregia Etched Micrography by OM 7H2SO4+HNO3+H3PO4 Etched Micro 4Kalling Etched Micrography by OM 202Keller Etched Micrography by OM 58Kroll Etched Micrography by OM 15Micro by OM, HCl + Ethanol + Picric Acid 12Micro by OM, picric acid+FeCl3+H2O etch 4Micrography by OM 73Micrography by OM using A262 Method A 80Micrography by OM, HF + HNO3 + H2O etch 8NH4OH+H2O+H2O2 Etched Micro 8NaOH Electrolytic Etched Micro 108Nital Etched Micrography by OM 801Oxalic Acid Electrolytic Etch 68

Results

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The plate longitudinal section presents a granular refined structure. Biphasic.
340
VIEW
ML00029 / Jan.2017
Titanium Plate for Subsea Application
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Typical manufacturing
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Grain refined structure
The bar presented a large prior beta grain size and acicular alpha. Biphasic structure.
420
VIEW
ML00028 / Jan.2017
Titanium Bar for Subsea Application
M - Ti6Al4VP - BarAp - StructureCd - Typical manufacturing
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Coarse Structure
Micrography of a transverse section of the pipe, presenting the pitting corrosion. As polished.
310
VIEW
ML00014 / Apr.2017
Pitting Corrosion in 316SS Pipe
M - Austenitic Stainless SteelP - Seamless PipeAp - FPSOCd - Pitting Corrosion
Cm - Micrography by OMDf - Pitting
Micrography of a longitudinal section of the mooring chain in the base metal. The low magnification reveals the banded structure of the rolled bar. The base metal microstructure is bainitic..
79
VIEW
ML00013 / Apr.2017
Welding Cracks in Mooring Chain
M - Low Alloy Low Carbon QTP - Welded PartAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Banded Structure
The micrography of the pin far from the fracture surface shows a biphasic brass, and Pb inclusions that are intentional to give a free machining condition for the alloy.
76
VIEW
ML00007 / Dec.2020
Free Machining Brass in Shear Pin
M - BrassP - Machined PartAp - LiftingCd - Shear
Cm - FeCl3+HCl+H2O Etched MicroDf - Two phases
SPUR RACK ferritic perlitic microstructure in the center of the tooth.
89
VIEW
ML00027 / Apr.2017
Adhesive Wear of Spur Gear Rack
M - Medium Carbon SteelP - Spur GearAp - Mechanical IndustryCd - Adhesive Wear
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Transverse section of the 1/16" thick tube at the autogenous seam weld.
588
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Autogenous Weld
Macrography transverse to the circunferential weld, longitudinal to the piping, presenting the location, a little far from the welded joint margin, where the through wall cracking is positioned.
160
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Through Wall Cracking

More from these cases

ML00029 — Titanium Plate for Subsea ApplicationM - Ti6Al4VP - Rolled PlateAp - StructureCd - Typical manufacturing
Alpha and beta phases. Refined Structure.
52
VIEW
ML00029 / Jan.2017
Titanium Plate for Subsea Application
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Typical manufacturing
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Two phases
Alpha and beta phases. Refined Structure.
46
VIEW
ML00029 / Jan.2017
Titanium Plate for Subsea Application
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Typical manufacturing
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Two phases
ML00028 — Titanium Bar for Subsea ApplicationM - Ti6Al4VP - BarAp - StructureCd - Typical manufacturing
The bar presented alpha plus beta phases, acicular alpha and coarse prior beta grains.
97
VIEW
ML00028 / Jan.2017
Titanium Bar for Subsea Application
M - Ti6Al4VP - BarAp - StructureCd - Typical manufacturing
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Two phases
Acicular alpha structure in a biphasic alloy of a large prior beta grain size. 4" diameter bar.
100
VIEW
ML00028 / Jan.2017
Titanium Bar for Subsea Application
M - Ti6Al4VP - BarAp - StructureCd - Typical manufacturing
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Acicular Alpha
ML00014 — Pitting Corrosion in 316SS PipeM - Austenitic Stainless SteelP - Seamless PipeAp - FPSOCd - Pitting Corrosion
Austenitic structure at the transverse section of the pipe, free from carbides.
277
VIEW
ML00014 / Apr.2017
Pitting Corrosion in 316SS Pipe
M - Austenitic Stainless SteelP - Seamless PipeAp - FPSOCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Austenitic structure, free from carbides, exactly in the region of the pitting, indicating that the corrosion is not associated to the material microstructure.
261
VIEW
ML00014 / Apr.2017
Pitting Corrosion in 316SS Pipe
M - Austenitic Stainless SteelP - Seamless PipeAp - FPSOCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
ML00013 — Welding Cracks in Mooring ChainM - Low Alloy Low Carbon QTP - Welded PartAp - OffshoreCd - Welding Defect
Micrographic detail of the bainitic microstructure of the base metal in the longitudinal section.
72
VIEW
ML00013 / Apr.2017
Welding Cracks in Mooring Chain
M - Low Alloy Low Carbon QTP - Welded PartAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Bainite
Micrography of a longitudinal section of the mooring chain at the flash welded region. The banded structure is deformed by the upset, close to the weld metal that is ferritic-bainitic.
61
VIEW
ML00013 / Apr.2017
Welding Cracks in Mooring Chain
M - Low Alloy Low Carbon QTP - Welded PartAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Bainitic Ferrite
Micrographic detail of the ferritic-bainitic weld metal, autogenous flash butt weld.
56
VIEW
ML00013 / Apr.2017
Welding Cracks in Mooring Chain
M - Low Alloy Low Carbon QTP - Welded PartAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Bainitic Ferrite
Welded region etched to reveal impurities. The banded structure creates a continuous network parallel to the weld metal.
50
VIEW
ML00013 / Apr.2017
Welding Cracks in Mooring Chain
M - Low Alloy Low Carbon QTP - Welded PartAp - OffshoreCd - Welding Defect
Cm - Micro by OM, picric acid+FeCl3+H2O etchDf - Segregated Regions
Micrography of a longitudinal section of the mooring chain, at the main crack position. The crack follows a network of segregations.
48
VIEW
ML00013 / Apr.2017
Welding Cracks in Mooring Chain
M - Low Alloy Low Carbon QTP - Welded PartAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Segregated Regions

+1 more from this case →

ML00007 — Free Machining Brass in Shear PinM - BrassP - Machined PartAp - LiftingCd - Shear
The micrography of the pin at the fracture surface shows a strong plastic deformation as expected during shearing.
69
VIEW
ML00007 / Dec.2020
Free Machining Brass in Shear Pin
M - BrassP - Machined PartAp - LiftingCd - Shear
Cm - FeCl3+HCl+H2O Etched MicroDf - Plastic Deformation
ML00027 — Adhesive Wear of Spur Gear RackM - Medium Carbon SteelP - Spur GearAp - Mechanical IndustryCd - Adhesive Wear
SPUR RACK ferritic perlitic microstructure in the center of the tooth.
77
VIEW
ML00027 / Apr.2017
Adhesive Wear of Spur Gear Rack
M - Medium Carbon SteelP - Spur GearAp - Mechanical IndustryCd - Adhesive Wear
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
SPUR RACK ferritic perlitic microstructure in the center of the tooth.
67
VIEW
ML00027 / Apr.2017
Adhesive Wear of Spur Gear Rack
M - Medium Carbon SteelP - Spur GearAp - Mechanical IndustryCd - Adhesive Wear
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
SPUR RACK ferritic perlitic microstructure in the surface of the tooth, evidencing no surface hardening treatment.
53
VIEW
ML00027 / Apr.2017
Adhesive Wear of Spur Gear Rack
M - Medium Carbon SteelP - Spur GearAp - Mechanical IndustryCd - Adhesive Wear
Cm - Nital Etched Micrography by OMDf - Non Hardened Surface
The non hardened surface of the SPUR RACK tooth presents a strong plastic deformation at the metal to metal contact region.
51
VIEW
ML00027 / Apr.2017
Adhesive Wear of Spur Gear Rack
M - Medium Carbon SteelP - Spur GearAp - Mechanical IndustryCd - Adhesive Wear
Cm - Nital Etched Micrography by OMDf - Plastic Deformation
The non hardened surface of the SPUR RACK tooth presents a strong plastic deformation at the metal to metal contact region. There are also evidences of heat transformation due to the heat generated in the sliding.
49
VIEW
ML00027 / Apr.2017
Adhesive Wear of Spur Gear Rack
M - Medium Carbon SteelP - Spur GearAp - Mechanical IndustryCd - Adhesive Wear
Cm - Nital Etched Micrography by OMDf - Plastic Deformation

+8 more from this case →

ML00026 — Autogenous Seam Welded Tube in Ferritic SSM - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Equiaxial grains of a ferritic structure, in a longitudinal section of the tube.
97
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Equiaxial grains of a ferritic structure, in a longitudinal section of the tube.
67
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Equiaxial grains of a ferritic structure, in a longitudinal section of the tube.
48
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Ferrite
Equiaxial grains of a ferritic structure, in a transverse section of the tube.
40
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Transverse Section
Equiaxial grains of a ferritic structure, in a transverse section of the tube.
35
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains

+5 more from this case →

ML00002 — Preferential Dissolution and Cracks in SDSSM - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Longitudinal section micrography at the cracked position, close to the external surface of the flange, showing cracks transverse to the thickness, associated to the microstructure.
147
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Cracks Transverse to the Surface
Longitudinal section micrography at the cracked position, close to the internal surface of the flange (exposed to the corrosive fluid), showing preferential dissolution associated to the microstructure.
133
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Preferential Dissolution
Micrography of the flange in the longitudinal section. The flange microstructure is ferritic austenitic, presenting a coarse structure.
102
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Coarse Structure
Micrographic detail of the flange microstructure in the longitudinal section. The flange is ferritic austenitic, presenting 70% of austenite. In the ferrite network there are evidences of precipitation/formation of detrimental phases.
113
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Micrographic detail of the flange microstructure in the longitudinal section. The flange is ferritic austenitic, presenting 70% of austenite. In the ferrite network there are evidences of precipitation/formation of detrimental phases.
100
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure