Scanning Electron Microscope

85 cases · 399 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Scanning Electron Microscope — sub-branches

Electrolytic Etch Micrography by SEM 12Fractography by SEM 166Kalling Etched Micrography by SEM 18Micrography by SEM 56Nital Etched Micrography by SEM 50Surface Aspect by SEM 97

Results

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Scanning electron microscopy image of the external surface of the line at the cracking position showing multiple cracks, branched, transverse to the line axis.
79
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Aspect by scanning electron microscopy of the cracking at the external surface of the fitting.
47
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
The microscopic aspect of the internal side of the housing evidences the characteristics of the multiple cracks, not directly related to pitting corrosion.
41
VIEW
ML00093 / Sep.2017
MIC of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Cracks
Microscopic detail of the fracture surface in the position where the fracture is intergranular, probably due to the MIC attack creating an embrittled condition of the material.
31
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
The fractography by SEM shows intergranular fracture close to the external surface of the pin.
93
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
Detail of the pin fracture surface, presenting both a flat aspect and a rough aspect in a shearing section of 2.5 mm width.
726
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Fractography by SEMDf - Fracture
Scanning electron fractography of a chromium plated pin, close to the pin surface where the fatigue cracking started, showing intergranular morphology typical of a hydrogen embrittlement effect. It occurred because the low alloy pin was carburized, quenched and tempered, with a too high hardness structure, before the electrolytic plating.
837
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Fractographic analysis of the pin fracture surface showing inter and transgranular morphologies of fracture micromechanisms.
53
VIEW
ML00088 / Dec.2017
Hydrogen Cracking of an API 5D S135 Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture

More from these cases

ML00095 — MIC of a Riser Control LineM - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Detail, by scanning electron microscopy, of the external surface of the line at the cracking position presenting branched cracks, transverse to the line axis. The surface of the fitting is fully stained (dark grey), from where the cracks start, indicating that the material loose passivation in these regions.
62
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Branched Cracks
The aspect of the fitting surface by SEM shows multiple cracks. Interesting to observe a stained region (dark grey) that corresponds to regions where the material passivation was destroyed.
43
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Detail of one region that had the passivation layer destroyed .
45
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Detail of one region that had the passivation layer destroyed and presented corrosion cracks.
48
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Corrosion Cracking
The aspect of the external surface of the fitting shows regions where the passivation was lost and where microcracks started already.
54
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Microcracks
ML00094 — MIC of a Subsea Hydraulic LineM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Aspect by scanning electron microscopy of the cracking at the external surface of the fitting. Interesting to observe that the cracks are deformed.
39
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Aspect by scanning electron microscopy of the cracking at the internal surface of the fitting.
36
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Internal Surface
Aspect by scanning electron microscopy of the cracking at the internal surface of the fitting. Interesting to observe multiple cracks with brittle characteristic.
39
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Internal Surface
The internal surface of the fitting presents multiple cracks not associated to pitting.
38
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Internal Surface
The through wall cracking was opened by citting the two sides and the aspect was characterized by SEM. Although there was a film at the fracture surface, probably because the fitting was removed from service some time after it was leaking, the fracture micromechanism is by quasecleavage, typical of a stress corrosion cracking.
56
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
ML00093 — MIC of a Drilling ToolM - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Brittle Behavior
Details of the pitting corrosion at the internal surface. There are cracks inside some pits.
31
VIEW
ML00093 / Sep.2017
MIC of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
The fracture micromechanism is intergranular in the region where the failure has iniciated.
22
VIEW
ML00093 / Sep.2017
MIC of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Fractographic detail by SEM of the intergranular micromechanism in the region where the failure has iniciated.
25
VIEW
ML00093 / Sep.2017
MIC of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
The fracture micromechanism is transgranular by quasecleavage in the region where the failure has propagated.
21
VIEW
ML00093 / Sep.2017
MIC of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
Fractographic detail by SEM of the transgranular micromechanism by quasecleavage in the region where the failure has propagated.
21
VIEW
ML00093 / Sep.2017
MIC of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
ML00080 — MIC of Stacking Disc SpringsM - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Microscopic detail of the fracture surface in the position where the fracture is intergranular, probably due to the MIC attack creating an embrittled condition of the material. A surface film is evident in this position suggesting that the fracture remained open and exposed to the environment during a certain time before the failure was detected.
29
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Fracture micromechanisms. Intergranular fracture in the top of the figure (close to the groove) and transgranular fracture in the bottom of the figure, where the mechanism changed to transgranular by quasecleavage.
27
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Microscopic detail of the fracture surface where it is transgranular, by quasecleavage. This aspect is similar to the one expected for this high strenght material without any embrittlement.
27
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
Microscopic detail of the fracture surface where it is transgranular, by quasecleavage. This aspect is similar to the one expected for this high strenght material without any embrittlement.
26
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
ML00009 — Hydrogen Cracking of a 5" Drill Pipe S135M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Fractographic detail by SEM of the intergranular fracture close to the external surface of the pin.
83
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
The fractography by SEM shows quasecleavage mechanism in the middle of the wall thickness of the pin.
81
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Transgranular Cracking
Fractographic detail by SEM of the quasecleavage mechanism in the middle of the wall thickness of the pin.
72
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Transgranular Crack
ML00046 — Brittle Fracture of SS Shear PinM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Fracture appearance in a sheared region, presenting a ductile morphology for the fracture micromechanism.
109
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Fractography by SEMDf - Ductile Fracture
Fracture appearance in a brittle region, presenting an intergranular morphology.
93
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Fractography by SEMDf - Intergranular Cracking
ML00081 — Hydrogen Cracking of a Chromium Plated Carburized PinM - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Scanning electron fractography showing that the fracture micromechanism is intergranular close to the surface of the pin, suggesting a hydrogen embrittlement effect at the carburized layer. The cracks were created during the electrolytic plating, and propagated later during service.
44
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - At the Surface
Scanning electron fractography of the pin in the fatigue subcritical crack growth, showing striation and regions of smashing .
40
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Fatigue Striation
Fractographic detail of the fatigue striation in the subcritical crack growth.
37
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Fatigue Striation
Fractography of the final fracture of the pin, presenting dimples (ductile fracture), after the nucleation and subcritical propagation of fatigue fracture.
36
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Dimples
ML00088 — Hydrogen Cracking of an API 5D S135 Drill PipeM - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Fractographic analysis of the pin showing several secondary intergranular cracks (in the middle of the figure) and quasecleavage transgranular fracture mechanism.
45
VIEW
ML00088 / Dec.2017
Hydrogen Cracking of an API 5D S135 Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Surface Aspect by SEMDf - Brittle Fracture
Fractographic analysis of the pin detailing a region of predominantly quasecleavage fracture micromechanism, associated to a macroscopic flat fracture surface.
46
VIEW
ML00088 / Dec.2017
Hydrogen Cracking of an API 5D S135 Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Surface Aspect by SEMDf - Cleavage Facets
Fractographic analysis of the pin showing a region of predominantly intergranular fracture micromechanism.
46
VIEW
ML00088 / Dec.2017
Hydrogen Cracking of an API 5D S135 Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Surface Aspect by SEMDf - Intergranular Cracking