Scanning Electron Microscope

9 cases · 55 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Product: Casting clear all

Scanning Electron Microscope — sub-branches

Fractography by SEM 19Kalling Etched Micrography by SEM 13Micrography by SEM 14Nital Etched Micrography by SEM 9

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Low magnification view of the WHEEL 1 fracture surface. The thickness of the wheel in this position (flat and paralell to the wheel face) is about 2.5 mm. The aspect of the fracture is similar all through the fracture perimeter, including the region where the fracture propagation changes the direction.
66
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Fractography by SEMDf - General View
Micrographic detail, by scanning electron microscopy, of the graphite in nodules and a ferritic-pearlitic matrix.
32
VIEW
ML00154 / Jan.2019
High Strength Cast Iron Crankshaft
M - Nodular Cast IronP - CastingAp - EngineCd - Surface treatment
Cm - Nital Etched Micrography by SEMDf - Graphite in Nodules
The fracture surface of the casting cylinder presented, at the internal surface, interconnected graphite flakes and a corroded matrix.
73
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fractography by SEMDf - Close to the Internal Surface
Micrography of the casting at the surface, presenting a zinc layer deposited in a hot dip process. The thickness of the layer is about 0.3mm in this position, that is higher than expected for this process. The steel substrate is not revealed because the etch was light and the zinc layer protects the low aloy steel during the etch.
93
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by SEMDf - Zn Layer
Low magnification micrography of the welded region, showing the interface between the base in the bottom and the fusion zone (between the liquidus and solidus temperatures), as well as the weld metal in the top. There are pores close to the weld metal and in the fusion zone the interdendritic space was melted and the eutectic morphology was changed. Keller etch.
50
VIEW
ML00070 / Jan.2019
Automotive Light Alloy Wheel Repaired By Welding
M - Aluminum Silicon MagnesiumP - RimAp - AutomotiveCd - Removed From Service
Cm - Micrography by SEMDf - Weld Repair
Micrographic detail of the original casting blade structure. The tempered martensite is more clearly revealed by the scanning electron microscopy. The average hardness level measured in this side is 270 HV.
70
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by SEMDf - Base Metal Left Side
Micrography of the blade, view inside the grain. The intragranular precipitation presents one unique size of precipitation, not yet coalesced, although the blade was in high temperature service for 50.000 hours. Etched by H2SO4 + HNO3 + H3PO4 reagent.
66
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - Micrography by SEMDf - Intragranular Secondary Precipitation
The fracture surface is flat, shows the graphite nodules and cleavage of the ferritic microstructure, indicating that the material have exceeded the capacity to acomodate the stress.
944
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets

More from these cases

ML00183 — Ductile Behavior of an Aluminum WheelM - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
WHEEL 1 fracture detail showing a small shrinkage in the left side of the photo and dimples in the right side of the photo.
73
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Fractography by SEMDf - Ductile Fracture
WHEEL 1 fracture detail showing small regions of shearing.
67
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Fractography by SEMDf - Elongated Dimples
WHEEL 1 fracture detail showing small regions with smooth aspect, and brittle microcracks. But predominantly the micromechanism is by dimples.
70
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Fractography by SEMDf - Cracks
WHEEL 1 fracture detail of the brittle microcracks. The analysis of the material microstructure showed that these microcracks are associated to iron rich phases.
68
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Fractography by SEMDf - Cracks
Low magnification micrography transverse to the fracture surface of the WHEEL 1. The fracture is in the top of the image and there is a void (shrinkage) not connected to the fracture .
34
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Micrography by SEMDf - Fracture

+3 more from this case →

ML00154 — High Strength Cast Iron CrankshaftM - Nodular Cast IronP - CastingAp - EngineCd - Surface treatment
Micrographic detail by scanning electron microscopy, Nital etched, of the ferrite microstructure around a graphite nodule.
30
VIEW
ML00154 / Jan.2019
High Strength Cast Iron Crankshaft
M - Nodular Cast IronP - CastingAp - EngineCd - Surface treatment
Cm - Nital Etched Micrography by SEMDf - Ferrite and Pearlite
Micrographic detail of the pearlite in the matrix.
29
VIEW
ML00154 / Jan.2019
High Strength Cast Iron Crankshaft
M - Nodular Cast IronP - CastingAp - EngineCd - Surface treatment
Cm - Nital Etched Micrography by SEMDf - Pearlite
Micrography of the shaft at the surface in a heat treated position. The graphite nodule is degradating due to temperature and adjacent the microsctructure is martensitic.
27
VIEW
ML00154 / Jan.2019
High Strength Cast Iron Crankshaft
M - Nodular Cast IronP - CastingAp - EngineCd - Surface treatment
Cm - Nital Etched Micrography by SEMDf - Graphite in Imperfect Nodules
Micrographic detail of the graphite nodule surrounded by martensite.
30
VIEW
ML00154 / Jan.2019
High Strength Cast Iron Crankshaft
M - Nodular Cast IronP - CastingAp - EngineCd - Surface treatment
Cm - Nital Etched Micrography by SEMDf - Martensite
Micrographic detail of the martensite.
32
VIEW
ML00154 / Jan.2019
High Strength Cast Iron Crankshaft
M - Nodular Cast IronP - CastingAp - EngineCd - Surface treatment
Cm - Nital Etched Micrography by SEMDf - Martensite

+1 more from this case →

ML00141 — Brittle Fracture of a Corroded Gray Cast IronM - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
The fracture surface of the casting cylinder presented, in the center of the thickness, cleavage facets and graphite decohesion that corresponds to a brittle fracture of the material.
61
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fractography by SEMDf - In the Center of the Thickness
The fracture surface of the casting cylinder presented, close to the external surface, a more ductile aspect of the fracture.
58
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fractography by SEMDf - Close to the External Surface
Fractographic detail of the interconnected graphite flakes and corroded matrix.
50
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fractography by SEMDf - Corrosion
Fractographic detail of the graphite decohesion and cleavage facets in the center of the cast cylinder thickness.
47
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fractography by SEMDf - Brittle Fracture
Micrography of the longitudinal section of the cylinder, at the external diameter (right side of the figure), presenting smaller interdendritic graphite flakes in a ferritic-perlitic matrix. This surface is painted.
32
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Graphite in Flakes
ML00138 — Liquid Metal Embrittlement of a HSLA SteelM - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Scanning electron fractography in low magnification (originally 15x), showing the flat fracture surface with steps and secondary cracks.
72
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Scanning electron fractography (originally 500x), showing zinc deposits at the fracture surface.
73
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Fractography by SEMDf - Zn Layer
Scanning electron fractography (originally 1000x), showing details of the zinc deposits at the fracture surface.
72
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Fractography by SEMDf - Fracture
Scanning electron fractography (originally 500x), showing intergranular aspects in the fracture surface.
43
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
Scanning electron fractography (originally 1000x), showing intergranular aspects in the fracture surface.
42
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking

+2 more from this case →

ML00070 — Automotive Light Alloy Wheel Repaired By WeldingM - Aluminum Silicon MagnesiumP - RimAp - AutomotiveCd - Removed From Service
Micrographic detail of the cast rim at the heat affected zone presenting coalesced Si particles at the interdendritic space an neddles of Fe rich phase. Keller etch.
47
VIEW
ML00070 / Jan.2019
Automotive Light Alloy Wheel Repaired By Welding
M - Aluminum Silicon MagnesiumP - RimAp - AutomotiveCd - Removed From Service
Cm - Micrography by SEMDf - Heat Affected Zone
The coalesced silicon particles in the interdendritic space of the base metal presents a remelting at the fusion zone. The micrography by SEM shows the exactly line where the eutectic is remelted and refined. Keller etch.
40
VIEW
ML00070 / Jan.2019
Automotive Light Alloy Wheel Repaired By Welding
M - Aluminum Silicon MagnesiumP - RimAp - AutomotiveCd - Removed From Service
Cm - Micrography by SEMDf - Fusion Line
Refined dendrites in the weld metal. The Si/Al alpha eutectic in the interdendritic space is also refined. Keller etch.
38
VIEW
ML00070 / Jan.2019
Automotive Light Alloy Wheel Repaired By Welding
M - Aluminum Silicon MagnesiumP - RimAp - AutomotiveCd - Removed From Service
Cm - Micrography by SEMDf - Weld Metal
Hot cracks in the fusion zone. The eutectic regions were melted and cracked in an interdendritic morphology.
37
VIEW
ML00070 / Jan.2019
Automotive Light Alloy Wheel Repaired By Welding
M - Aluminum Silicon MagnesiumP - RimAp - AutomotiveCd - Removed From Service
Cm - Micrography by SEMDf - Cracks
Detail of the hot cracks in the fusion zone. The eutectic regions were melted and cracked in an interdendritic morphology. Keller etch.
50
VIEW
ML00070 / Jan.2019
Automotive Light Alloy Wheel Repaired By Welding
M - Aluminum Silicon MagnesiumP - RimAp - AutomotiveCd - Removed From Service
Cm - Micrography by SEMDf - Cracks
ML00055 — CA6NM Blade Remanufactured by WeldingM - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Higher magnification of the martensitic structure of the original casting blade structure, hardness level of 270HV10.
26
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by SEMDf - Base Metal Left Side
Micrographic detail of the inserted casting structure. The martensite presents a less tempering aspect than the original casting revealing that it was heat treated in a different condition. The average hardness level measured in this side is 370 HV.
157
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by SEMDf - Base Metal Right Side
Higher magnification of the martensitic structure of the inserted casting structure, hardness level of 370HV10.
23
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by SEMDf - Base Metal Right Side
Micrographic detail of the original casting blade fusion line, presenting the tempered martensitic structure similar for the HAZ (left side of the figure) and the weld metal (right side of the figure).
20
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by SEMDf - Fusion Line Left Side
Micrographic detail of the original casting blade fusion line, presenting the tempered martensitic structure similar for the HAZ (left side of the figure) and the weld metal (right side of the figure).
20
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by SEMDf - Fusion Line Left Side

+7 more from this case →

ML00042 — Gas Turbine Blade IN 939, CoatedM - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Micrographic detail of the diffusion coating. H2SO4 + HNO3 + H3PO4 etched.
47
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - Micrography by SEMDf - Coating
ML00040 — Brittle Fracture of a Valve StemM - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Detail of the cleavage micromechanism.
195
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets