Scanning Electron Microscope

17 cases · 56 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Oil and Gas clear all

Scanning Electron Microscope — sub-branches

Electrolytic Etch Micrography by SEM 5Fractography by SEM 35Nital Etched Micrography by SEM 3Surface Aspect by SEM 13

Results

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Low magnification image by scanning electron microscopy. In the bottom of the image the fracture appearance is brittle and presenting several secondary cracks. In the top of the image the fracture is fully flat, also without macroscopic plastic deformation.
33
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Fractography by SEMDf - Fracture
Aspect of the spring surface, with a layer of corroded products, and pits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Surface Aspect by SEMDf - Corrosion
The through wall cracking was opened and the fracture surface presents a full integranular morphology, typical of an intergranular stress corrosion cracking.
79
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Fractography by SEMDf - Stress Corrosion Cracks
Fractography of the broken Charpy V testpiece, in a high strength steel that absorbed 11 Joules at 20°C. Quasicleavage and dimples are the main fracture micromechanisms with some secondary cracks that appear to be intergranular, exactly as the fracture of the part.
48
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Fractography by SEMDf - Broken Testpiece
Low magnification SEM image showing the brittle aspect of the cracks in the bolt thread.
61
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Brittle Cracks
Micrographic detail of the pearlitic structure in the center of the shaft thickness.
82
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by SEMDf - Pearlite
Corroded spots (shallow pits full of products) at the spring surface.
80
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Corrosion
Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a seamless pipe in a low alloy steel X70 cladded by welding overlay of Alloy 625 (by automatic GTAW process). The region is a detail of the interface inside the Ni alloy weld metal, presenting columnar grains and intragranular preciptation. The pipe was heat treated before bending (solution annealing) and after bending (quenching and tempering to meet X70 grade). The microhardness of this region is higher than the value obtained out of this region, in the overlay.
657
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface

More from these cases

ML00176 — Hydride Formation in a Titanium BladeM - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
The position of the fracture at the starting point of the failure is brittle, transgranular, with a cleavage/quase-cleavage morphology.
24
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Fractography by SEMDf - Cleavage Facets
Aspect by SEM of the secondary crack at the blade surface.
18
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Surface Aspect by SEMDf - At the Surface
At the surface of the blade there are microcracks with a brittle aspect.
23
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Surface Aspect by SEMDf - Secondary Cracks
SEM fractograph showing a cleavage facet with radiating river-pattern markings and scattered fine surface particles.
1
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Fractography by SEMDf - Cleavage Facets
ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Micrographic detail of the martensitic structure, clearly obtained from a refined previous austenitic structure .
19
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Martensite
Micrographic detail of the martensitic structure.
19
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Martensite
ML00165 — SCC of Aluminum Bronze Heating CoilM - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Fractographic detail of the through wall cracking after opening, presenting a full integranular morphology, typical of an intergranular stress corrosion cracking.
79
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Fractography by SEMDf - Stress Corrosion Cracks
ML00161 — Brittle Fracture of a High Strength SocketM - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Fractography of the broken tensile testpiece, in a high strength steel (about 260Ksi Yield Strength) that presented 10% elongation. The fracture micromechanism in a static test is quasicleavage and dimples, with some secondary cracks that appear to be intergranular, exactly as the fracture of the part.
53
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Fractography by SEMDf - Broken Testpiece
ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Detail of the bolt thread in a SEM image, showing parts of the thread removed in a brittle way.
62
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Brittle Fracture
ML00137 — Brittle Fracture of a 15-5 PH Valve SpringM - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Corroded spots (shallow pits full of products) at the spring surface.
75
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Corrosion
The scanning electron microscopy image presents the surface of the spring (top of the figure) where it was broken (the fracture is in the bottom of the figure). It is possible to see that there is a product at the surface and the material presents intergranular fracture, suggesting there was a hydrogen embrittlement effect. Important to observe that the material does not present pits.
58
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Fractography by SEMDf - At the Surface
The scanning electron microscopy image presents the fracture surface at the fracture initiation point. The fracture is intergranular.
54
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Image detail presenting the intergranular fracture surface at the fracture initiation point.
46
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Fracture micromechanism changing from intergranular to transgranular, as the fracture is propagating.
45
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Fractography by SEMDf - Fracture

+4 more from this case →

ML00132 — Seamless Pipe Overlaid with Alloy 625M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Image by scanning electron microscopy of the interface of the internally cladded pipe. It is a seamless pipe in low alloy steel X70 overlaid with Alloy 625 (by automatic GTAW process). The region is a detail in the side of the Ni alloy weld metal, presenting transgranular precipitation. The pipe was heat treated before bending (solution annelaing) and after bending (quenching and tempering to meet X70 grade). The microhardness of this region is higher than the value obtained out of this region, in the overlay.
43
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface
Image by scanning electron microscopy of the interface of the internally cladded pipe, seamless low alloy steel X70 overlaid with Alloy 625 (by automatic GTAW process) and presenting maximum iron content of 5% at the thickness of 3 mm (the qualified thickness).
37
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface