Scanning Electron Microscope

10 cases · 66 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Standard: ALLOY clear all

Scanning Electron Microscope — sub-branches

Electrolytic Etch Micrography by SEM 6Fractography by SEM 21Micrography by SEM 11Nital Etched Micrography by SEM 2Surface Aspect by SEM 26

Results

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Micrography, by scanning electron microscopy. The alloy is a precipitation hardened material, and the stains at the surface are associated to differential etching in second phases and inclusions.
35
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Micrography by SEMDf - Granular structure
Micrographic detail by scanning electron microscopy of the interface between the two thermal spray layers, the first one in stainless steel (bottom of the figure) and the second one, at the surface,in tungsten carbide (top of the figure). The composition of the first layer is similar to the base metal (lean duplex) and the composition of the second layer is WC in a Co matrix.
16
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Electrolytic Etch Micrography by SEMDf - Thermal Spray Layer
Micrography of the plate section, in the middle of the plate. Martensitic structure.
47
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Nital Etched Micrography by SEMDf - Martensite
Corroded spots (shallow pits full of products) at the spring surface.
80
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Corrosion
Microscopical aspect by scanning electron microscopy (SEM) of the external surface of a drilling tool in a position that presented localized deposits and corrosion under deposit. The deep corrosion in a short time is only possible associated to the biological growth and aggressive environment generated by the microorganisms metabolites - Microbiologically Induced Corrosion (MIC).
104
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Deposits
Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a seamless pipe in a low alloy steel X70 cladded by welding overlay of Alloy 625 (by automatic GTAW process). The region is a detail of the interface inside the Ni alloy weld metal, presenting columnar grains and intragranular preciptation. The pipe was heat treated before bending (solution annealing) and after bending (quenching and tempering to meet X70 grade). The microhardness of this region is higher than the value obtained out of this region, in the overlay.
656
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface
Scanning electron microscopy image of the external surface of the line at the cracking position showing multiple cracks, branched, transverse to the line axis.
79
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Aspect by scanning electron microscopy of the cracking at the external surface of the fitting.
47
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface

More from these cases

ML00145 — Impact of a .380 Winchester on 6061 T6 PlateM - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Micrographic detail, by scanning electron microscopy, of the precipitation hardened granular structure. The stains are preferential etch of second particles.
32
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Micrography by SEMDf - Aligned particles
Detail of the margin of the perforated hole in the impact position. It is interesting to observe extreme plastic deformation created by the perforation expulsing the material from the hole, in the direction of the impact.
28
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Surface Aspect by SEMDf - Plastic Deformation
Detail of the plate surface showing striation as the finishing, deformed by the projectile effect in shearing the thickness.
24
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Surface Aspect by SEMDf - At the Surface
Detail of the plate surface showing striation as the finishing, deformed by the projectile effect in shearing the thickness.
24
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Surface Aspect by SEMDf - At the Surface
High magnification detail of the plate surface showing the deformed striation.
21
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Surface Aspect by SEMDf - At the Surface

+17 more from this case →

ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Micrographic detail of the first thermal spray layer, in stainless steel with the same composition of the base metal (lean duplex).
16
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Electrolytic Etch Micrography by SEMDf - Thermal Spray Layer
Micrographic detail, by scanning electron microscopy, of the duplex, austenitic and ferritic, structure with sigma phase.
16
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Electrolytic Etch Micrography by SEMDf - Sigma
ML00142 — Impact of a .308 Winchester on AR500 PlateM - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Micrographic detail of the plate section presenting the martensitic microstructure.
43
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Nital Etched Micrography by SEMDf - Martensite
Microscopically aspect of the plate surface at the bullet impact, by scanning electron microscopy, presenting the foreign material from the bullet adhered at the surface.
34
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Surface Aspect by SEMDf - Low Mag
Microscopically aspect of the plate surface in the center of the bullet impact. The light and smooth surface is the melted bullet on the plate and the dark surface is the steel plate with oxides and very small surface cracks (10 microns length).
30
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Surface Aspect by SEMDf - At the Surface
Detailed aspect of the plate surface where there was the bullet impact, by scanning electron microscopy, showing that the bullet has melted and solidified on the surface. The EDS analysis showed Pb-Sb peaks.
32
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Surface Aspect by SEMDf - At the Surface
Aspect of the plate surface a little far from the region of bullet impact, by scanning electron microscopy, showing bullet melted islands on the surface. The EDS analysis showed Pb-Sb peaks.
25
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Surface Aspect by SEMDf - At the Surface

+1 more from this case →

ML00137 — Brittle Fracture of a 15-5 PH Valve SpringM - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Corroded spots (shallow pits full of products) at the spring surface.
75
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Corrosion
The scanning electron microscopy image presents the surface of the spring (top of the figure) where it was broken (the fracture is in the bottom of the figure). It is possible to see that there is a product at the surface and the material presents intergranular fracture, suggesting there was a hydrogen embrittlement effect. Important to observe that the material does not present pits.
58
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Fractography by SEMDf - At the Surface
The scanning electron microscopy image presents the fracture surface at the fracture initiation point. The fracture is intergranular.
54
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Image detail presenting the intergranular fracture surface at the fracture initiation point.
46
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Fracture micromechanism changing from intergranular to transgranular, as the fracture is propagating.
45
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Fractography by SEMDf - Fracture

+4 more from this case →

ML00135 — MIC of a Non Magnetic Drilling ToolM - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Microscopical aspect by scanning electron microscopy (SEM) of the external surface of a drilling tool in a position that presented localized deposits and corrosion under deposit. It is possible to see that the strain hardened surface was etched by the aggressive metabolites of the microorganisms.
90
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
ML00132 — Seamless Pipe Overlaid with Alloy 625M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Image by scanning electron microscopy of the interface of the internally cladded pipe. It is a seamless pipe in low alloy steel X70 overlaid with Alloy 625 (by automatic GTAW process). The region is a detail in the side of the Ni alloy weld metal, presenting transgranular precipitation. The pipe was heat treated before bending (solution annelaing) and after bending (quenching and tempering to meet X70 grade). The microhardness of this region is higher than the value obtained out of this region, in the overlay.
42
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface
Image by scanning electron microscopy of the interface of the internally cladded pipe, seamless low alloy steel X70 overlaid with Alloy 625 (by automatic GTAW process) and presenting maximum iron content of 5% at the thickness of 3 mm (the qualified thickness).
36
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface
ML00095 — MIC of a Riser Control LineM - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Detail, by scanning electron microscopy, of the external surface of the line at the cracking position presenting branched cracks, transverse to the line axis. The surface of the fitting is fully stained (dark grey), from where the cracks start, indicating that the material loose passivation in these regions.
62
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Branched Cracks
The aspect of the fitting surface by SEM shows multiple cracks. Interesting to observe a stained region (dark grey) that corresponds to regions where the material passivation was destroyed.
43
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Detail of one region that had the passivation layer destroyed .
45
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Detail of one region that had the passivation layer destroyed and presented corrosion cracks.
48
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Corrosion Cracking
The aspect of the external surface of the fitting shows regions where the passivation was lost and where microcracks started already.
54
VIEW
ML00095 / Sep.2017
MIC of a Riser Control Line
M - Austenitic Stainless SteelP - Fabrication WeldAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Microcracks
ML00094 — MIC of a Subsea Hydraulic LineM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Aspect by scanning electron microscopy of the cracking at the external surface of the fitting. Interesting to observe that the cracks are deformed.
39
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Aspect by scanning electron microscopy of the cracking at the internal surface of the fitting.
36
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Internal Surface
Aspect by scanning electron microscopy of the cracking at the internal surface of the fitting. Interesting to observe multiple cracks with brittle characteristic.
39
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Internal Surface
The internal surface of the fitting presents multiple cracks not associated to pitting.
38
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Internal Surface
The through wall cracking was opened by citting the two sides and the aspect was characterized by SEM. Although there was a film at the fracture surface, probably because the fitting was removed from service some time after it was leaking, the fracture micromechanism is by quasecleavage, typical of a stress corrosion cracking.
56
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture