Scanning Electron Microscope

15 cases · 52 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Hydrogen clear all

Scanning Electron Microscope — sub-branches

Fractography by SEM 41Micrography by SEM 4Nital Etched Micrography by SEM 1Surface Aspect by SEM 6

Results

SortNewestOldestTitle A-ZTitle Z-A
Aspect of the opened crack by scanning electron microscopy, showing the coarser structure in the weld (right side of the figure).
33
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Fractography by SEMDf - Fracture
Low magnification image by scanning electron microscopy. In the bottom of the image the fracture appearance is brittle and presenting several secondary cracks. In the top of the image the fracture is fully flat, also without macroscopic plastic deformation.
33
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Fractography by SEMDf - Fracture
The fractographic aspect of the broken bolt shows intergranular micromechanism, typical of a hydrogen embrittlement condition for this aged martensitic material.
88
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
Fractographic aspect of the stud fracture surface, by scanning electron microscopy, close to the bottom of the thread fillet. In the center of the image it is possible to see secondary cracks with intergranular morphology.
59
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Fractographic analysis by scanning electron microscopy of the stud fracture surface after opening the cracks. Brittle intergranular morphology with dimples and quasecleavage micromechanisms indicate that the internal cracks, intergranular, occurred by a hydrogen embrittlement effect during electroplating, and the ductile aspects are probably associated to overloading during torque.
517
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Fracture
Aspect of the fracture surface of the bolt, after cleaning with a plastic brush. Although there is a layer of oxides it is possible to see the intergranular morphology of the fracture, typical of a hydrogen embrittlement mechanism.
1154
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
The fractography by SEM shows intergranular fracture close to the external surface of the pin.
93
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
Scanning electron fractography of a chromium plated pin, close to the pin surface where the fatigue cracking started, showing intergranular morphology typical of a hydrogen embrittlement effect. It occurred because the low alloy pin was carburized, quenched and tempered, with a too high hardness structure, before the electrolytic plating.
837
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture

More from these cases

ML00179 — Hydrides in Titanium WeldM - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
In the region where the fracture started there are brittle aspects resembling a cleavage micromechanism and several secondary cracks, transverse to the fracture surface, as well as propagation by fatigue (striation).
36
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Fractography by SEMDf - Brittle Cracks
Fractography showing brittle secondaryy cracks in the region where the cracking was originated.
34
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Fractography by SEMDf - Secondary Cracks
Fractography showing propagation by fatigue. Striation.
26
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Fractography by SEMDf - Fatigue Striation
ML00176 — Hydride Formation in a Titanium BladeM - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
The position of the fracture at the starting point of the failure is brittle, transgranular, with a cleavage/quase-cleavage morphology.
24
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Fractography by SEMDf - Cleavage Facets
Aspect by SEM of the secondary crack at the blade surface.
18
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Surface Aspect by SEMDf - At the Surface
At the surface of the blade there are microcracks with a brittle aspect.
23
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Surface Aspect by SEMDf - Secondary Cracks
SEM fractograph showing a cleavage facet with radiating river-pattern markings and scattered fine surface particles.
1
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Fractography by SEMDf - Cleavage Facets
ML00139 — Hydrogen Fracture of a 17-4 PH Allen BoltM - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Fractographic aspect by scanning electron microscopy, close to the surface the broken bolt, presenting intergranular fracture micromechanism.
79
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
Microscopic detail of the intergranular fracture close to the bolt surface.
71
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
Fractographic aspect by scanning electron microscopy, in the center of the broken bolt, presenting transgranular fracture micromechanism.
45
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Cleavage Facets
Fractographic detail of the transgranular fracture micromechanism, brittle.
43
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Cleavage Facets
ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Fractographic detail by scanning electron microscopy of the secondary cracks with intergranular morphology.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Secondary Cracks
Micrography of the bottom of the thread fillet, presenting secondary cracks of intergranular morphology, propagating transverse to the stud axis, but presenting longitudinal openings.
28
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by SEMDf - Cracks
ML00127 — Hydrogen Cracks of Cadmium Plated StudsM - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Fractographic analysis by scanning electron microscopy of the stud fracture surface after opening the cracks. Brittle intergranular morphology with dimples and quasecleavage micromechanisms indicate that the internal cracks, intergranuar, occurred by a hydrogen embrittlement effect during electroplating, and the ductile aspects are probably associated to overloading during torque.
37
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
ML00126 — Hydrogen Fracture of Subsea Allen BoltsM - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Detailed aspect of the fracture surface of the bolt, evidencing the intergranular morphology of the fracture (although with an oxide scale), typical of a hydrogen embrittlement mechanism.
114
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
ML00009 — Hydrogen Cracking of a 5" Drill Pipe S135M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Fractographic detail by SEM of the intergranular fracture close to the external surface of the pin.
83
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
The fractography by SEM shows quasecleavage mechanism in the middle of the wall thickness of the pin.
81
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Transgranular Cracking
Fractographic detail by SEM of the quasecleavage mechanism in the middle of the wall thickness of the pin.
74
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Transgranular Crack
ML00081 — Hydrogen Cracking of a Chromium Plated Carburized PinM - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Scanning electron fractography showing that the fracture micromechanism is intergranular close to the surface of the pin, suggesting a hydrogen embrittlement effect at the carburized layer. The cracks were created during the electrolytic plating, and propagated later during service.
45
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - At the Surface
Scanning electron fractography of the pin in the fatigue subcritical crack growth, showing striation and regions of smashing .
40
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Fatigue Striation
Fractographic detail of the fatigue striation in the subcritical crack growth.
37
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Fatigue Striation
Fractography of the final fracture of the pin, presenting dimples (ductile fracture), after the nucleation and subcritical propagation of fatigue fracture.
36
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Dimples