Scanning Electron Microscope

6 cases · 34 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Product: Forging clear all

Scanning Electron Microscope — sub-branches

Electrolytic Etch Micrography by SEM 2Fractography by SEM 8Kalling Etched Micrography by SEM 3Micrography by SEM 5Nital Etched Micrography by SEM 9Surface Aspect by SEM 7

Results

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Fusion line at the forging side. The weld metal to the top and the heat affected zone to the bottom.
84
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by SEMDf - Fusion Line
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
92
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Microscopic image by scanning electron microscope (SEM) of the ring surface that presented pites under fouling deposits.
522
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
Detail of the fracture surface, predominantly transgranular with secondary cracks of intergranular morphology.
831
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Fusion line micrographic detail. The weld metal is in the right and HAZ in the left.
27
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by SEMDf - Fusion Line
External surface aspect of the flange showing preferential dissolution, responsible for nucleation of the through wall cracking.
245
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Surface Aspect by SEMDf - Preferential Dissolution

More from these cases

ML00178 — Cold cracks in Cr-Mo Welded ForgingM - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Quenched and tempered heat affected zone of the forging.
75
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by SEMDf - Heat Affected Zone
The cracking is located at the margin of the weld in the forging side. It is 1.2 mm deep.
66
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by SEMDf - Cracking
The intergranular morphology of the cracks, at the heat affected zone of the forging, indicates it is a cold cracking probably formed when the welded joint was not yet post welding heat treated. The actual hardness values at the HAZ is 270HV10, and when it was cracked it was probably a lot higher.
71
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by SEMDf - Intergranular Cracking
Detail of the cold cracking at the previous austenite grain boundary of the martensitic structure.
62
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by SEMDf - Cold cracking
Detail of the cold cracking at the previous austenite grain boundary of the martensitic structure.
55
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by SEMDf - Intergranular Cracking

+3 more from this case →

ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
85
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
High magnification details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
81
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Higher magnification detail of the sigma phase by scaning electron microscopy.
76
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Fractographic aspect of the valve body fracture surface after opening the crack. The fracture micromechanism is brittle, by cleavage, with several secondary microcracks associated to the sigma phase.
54
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets
Fractographic detail of the valve body fracture surface after opening the crack. The fracture micromechanism is brittle, by cleavage, with several secondary microcracks associated to the sigma phase.
52
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets

+1 more from this case →

ML00124 — MIC of a Martensitic Valve RingM - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Microscopic details of the ring surface showing the fouling at the surface and localized corrosion under the deposits.
42
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
Higher magnification of the localized corrosion, showing that there are cracks at the margin of the corroded region.
39
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
SEM image showing a branching surface crack extending from a region of granular corrosion deposits into the polished substrate.
32
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
Intergranular morphology inside the pitting and evidences of chemical attack (dissolution).
36
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
ML00078 — Hydrogen Cracking of IN 718 Subsea ConnectorM - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Fractography by SEM, showing intergranular and transgranular fracture micromechanisms.
72
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
ML00045 — Subsea Tubular F6NM Martensitic SSM - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Micrographic detail of the base metal tempered martensite.
24
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by SEMDf - Base Metal
Micrographic detail of the weld metal tempered martensitic microstructure.
25
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by SEMDf - Weld Metal
ML00002 — Preferential Dissolution and Cracks in SDSSM - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Detail of the region at the flange external surface where the material is suffering the preferential corrosion.
177
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Surface Aspect by SEMDf - Preferential Dissolution
Micrographic detail of the through wall cracking in the middle of the thickness, showing that the cracking is associated to ferrite network in the (super)duplex microstructure.
128
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Micrography by SEMDf - Crack
Micrographic detail of the cracking, associated to the ferrite network, that presents both corrosion (preferential dissolution) and fracture (clevage) aspects.
128
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Electrolytic Etch Micrography by SEMDf - Crack
The fracture surface, although presenting a large amount of corrosion products, shows also evidences of a brittle behavior with regions of cleavage micromechanism.
116
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Fractography by SEMDf - Cleavage Facets
Micrographic detail of the ferrite network with evidences of precipitation/formation of detrimental phases. NaOH solution was adopted for the electrolytic etching.
86
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Electrolytic Etch Micrography by SEMDf - Delta ferrite

+2 more from this case →