Sampling and Analysis

154 cases · 925 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Sampling and Analysis — sub-branches

At the Surface 77Base Metal 65Broken Testpiece 9Close to the External Surface 41Close to the Internal Surface 33External Surface 27Fusion Line 29General View 132Heat Affected Zone 82In the Center of the Thickness 36In the Center of the Weld 2Internal Surface 33Longitudinal Section 102Low Mag 17Microhardness Indentations 1Microhardness identations 2Radial Section 3T/4 of the external surface 2Transverse Section 60Weld Metal 96Weld Repair 7Welded Joint 69

Results

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Red painted device where the 50 mm x 50 mm carbon steel plate was positioned (in the circle). The image presents the target, positioned 100 meters far from the gun, after the shot and the projectile perforated the plate, as will be presented in the other figures.
602
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Aspect Before AnalysisDf - General View
Red painted device where the 50 mm x 50 mm high strenght wear resistant steel plate (AR500) was positioned (in the circle). The image presents the target, positioned 100 meters far from the gun, after the shot and the projectile did not penetrate in the plate, and not even affected the material surface, as will be presented in the other figures.
500
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Aspect Before AnalysisDf - General View
Fractured position of the casting cylinder of 10.5 mm thickness (minimum measured thickness) showing a brittle behavior (lack of plastic deformation), typical of overloading a material with 1% ductility (measured in the tensile test). This is the view of the internal surface of the cylinder, presenting regions of localized thinning in this surface that was in contact with (treated) cooling water. The external side of the cylinder was painted.
918
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fracture Surface AspectDf - General View
Micrography of the pipe transverse section presenting a granular microstructure.
147
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Nital Etched Micrography by OMDf - Transverse Section
Micrography of a longitudinal section, in the center, of the broken 5/8" bolt, presenting an aged martensitic structure. There are vertical "lines" that correspond to segregation bands due to the forming direction. These bands are evident only using low magnification microscopy.
168
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Aspect of the broken spring. The wire is 1 1/2" diameter and the ourter diameter of the spirals is 12 1/2", in a 20" height spring. It was broken in several pieces.
866
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Aspect Before AnalysisDf - General View
Aspect of the broken stud that was fastening a flanged line in a subsea body (tapped hole) using a nut. The fracture, transverse to the stud axis, occurred exactly at the body to flange interface. Adjacent to the fracture, all thread fillets (positioned inside the flange hole) presented cracks at the bottom of the thread. The stud was operating during seven years and was not corroded, indicating it was protected by the anodes. There are also deposits in the fillets suggesting the cathodic protection was effective even inside the flange hole.
799
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View
Aspect of the internal side of the drilling tool, after cleaning for inspection. Several regions of corrosion where detected where the drilling mud was adhered and remained uncleaned for a period a little longer than 1 month.
775
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Aspect Before AnalysisDf - Internal Surface

More from these cases

ML00143 — Impact of a .308 Winchester on A36 PlateM - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Aspect of a typical .308 Winchester projectile, similar to the one adopted to shot the plate, cut in a longitudinal section. It is a Cu alloy case filled with Pb-Sb.
92
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Longitudinal Section AspectDf - Longitudinal Section
Aspect of the 3/8" thickness plate, 50 mm x 50 mm, of the low carbon steel steel, in the face of impact with the projectile. The plate was perforated by the bullet.
88
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Aspect Before AnalysisDf - General View
Other view of the 3/8" thickness plate, 50 mm x 50 mm, of the low carbon steel plate, in the face of impact with the projectile. The plate suffered a localized perforation.
48
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Aspect Before AnalysisDf - General View
Other view of the 3/8" thickness plate, 50 mm x 50 mm, of the low carbon steel plate, in the opposite face of impact. The plate suffered a localized perforation and this image shows the position of the exit of the bullet. It is also evident that the shot was very close to the red painted device since a straight line is marked at the surface of the plate (bottom of the figure).
46
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Aspect Before AnalysisDf - General View
Detail of the position where the projectile strike the plate. The plate suffered a localized perforation.
44
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Surface AspectDf - Low Mag

+11 more from this case →

ML00142 — Impact of a .308 Winchester on AR500 PlateM - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Aspect of a typical .308 Winchester projectile, similar to the one adopted to shot the plate, cut in a longitudinal section. It is a Cu alloy case filled with Pb-Sb.
57
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Longitudinal Section AspectDf - Longitudinal Section
Aspect of the 3/8" thickness plate, 50 mm x 50 mm, of the AR500 wear resistant steel, in the face of impact with the projectile. The plate did not suffer any macroscopic damage. It was only stained at the impact surface.
63
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Aspect Before AnalysisDf - General View
Other view of the 3/8" thick plate, 50 mm x 50 mm, of the AR500 wear resistant steel, in the face of impact with the projectile. The plate did not suffer any macroscopic damage. It was only stained at the impact surface.
41
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Aspect Before AnalysisDf - General View
Aspect of the 3/8" thick plate, 50 mm x 50 mm, of the AR500 wear resistant steel, in the opposite face of impact with the projectile. The plate did not suffer any macroscopic damage.
38
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Aspect Before AnalysisDf - General View
Detail of the position in the plate of impact with the projectile. No damage, only particles adhered at the surface.
36
VIEW
ML00142 / Aug.2018
Impact of a .308 Winchester on AR500 Plate
M - Low Alloy Wear ResistantP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Surface AspectDf - Low Mag

+18 more from this case →

ML00141 — Brittle Fracture of a Corroded Gray Cast IronM - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), close to the internal surface (left side). It is possible to see large graphite flakes.
98
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - Close to the Internal Surface
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), in the center of the thickness. It is possible to see a mixture of large graphite flakes and rosette grouping flakes.
80
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - In the Center of the Thickness
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), close to the external surface (left side). It is possible to see smaller graphite flakes, interdendritic .
79
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - Close to the External Surface
The fracture surface of the casting cylinder presented, at the internal surface, interconnected graphite flakes and a corroded matrix.
73
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fractography by SEMDf - Close to the Internal Surface
The fracture surface of the casting cylinder presented, in the center of the thickness, cleavage facets and graphite decohesion that corresponds to a brittle fracture of the material.
61
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fractography by SEMDf - In the Center of the Thickness

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ML00140 — Preferential Corrosion of Pipe Seam WeldM - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Aspect of the 4" pipe that was in seawater service for 8 years and leaked in a longitudinal line that corresponds to the seam weld. The internal surface presented thick deposits. Although the pipe was cut with a thermal process, the analysis was conducted after mechanical cutting.
100
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Aspect Before AnalysisDf - General View
Detail of the transverse section of the 4" pipe 90° from the seam weld. The thickness of the pipe is 8 mm. No evidences of general corrosion or pitting were identified.
77
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Transverse Section
Detail of the transverse section of the 4" pipe 90° from the seam weld. The thickness of the pipe is 8 mm. No evidences of general corrosion or pitting were identified.
70
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Transverse Section
Detail of the transverse section of the 4" pipe 180° from the seam weld. The thickness of the pipe is 8 mm. No evidences of general corrosion or pitting were identified.
64
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Transverse Section
Aspect of the internal surface of the pipe after cleaning, showing the leakage line.
67
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Aspect Before AnalysisDf - Internal Surface

+2 more from this case →

ML00139 — Hydrogen Fracture of a 17-4 PH Allen BoltM - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Micrography of a longitudinal section of the 5/8" bolt, at the bottom of the thread, presenting a refined structure compared to the center of the bolt and a mark at the thread flank that was probably created during tightening of the bolt.
95
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the bolt, close to the fracture surface (top of the figure), The fracture started at the surface (left side) in a position close to the bolt body to bolt head transition.
58
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Longitudinal Section
Macrography of the longidutinal section of a non broken allen bolt, at the threaded body to bolt head transition. The granular structure is different through the bolt, with refined structure in the threaded body and coarse at the transition.
44
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched MacroDf - Longitudinal Section
Micrography of a longitudinal section, in the center of a non-broken bolt that operated in the same assembling, presenting an aged martensitic structure, similar to the broken bolt.
41
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the non-broken 5/8" bolt, at the transition between the threaded body and the head, showing a variation in the grain size (of the previous austenite) and evidences of a deformed structure at this transition.
41
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
ML00137 — Brittle Fracture of a 15-5 PH Valve SpringM - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Corroded spots (shallow pits) at the spring surface.
84
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Aspect Before AnalysisDf - At the Surface
The scanning electron microscopy image presents the surface of the spring (top of the figure) where it was broken (the fracture is in the bottom of the figure). It is possible to see that there is a product at the surface and the material presents intergranular fracture, suggesting there was a hydrogen embrittlement effect. Important to observe that the material does not present pits.
58
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Fractography by SEMDf - At the Surface
ML00135 — MIC of a Non Magnetic Drilling ToolM - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Aspect of the external side of the nominal diameter 6 3/4" drilling tool, after cleaning for inspection. Several regions of corrosion where detected where the drilling mud was adhered and remained for a period a little longer than 1 month. This tool is a high strength steel, cold worked.
163
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Aspect Before AnalysisDf - General View
Optical micrography of the transverse section of the drill collar, in the center of the thickness, presenting an uniform, granular, fully austenitic microstructure.
76
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transverse Section
Optical micrography of the transverse section of the drill collar, in the center of the thickness, presenting an uniform, granular, fully austenitic microstructure.
64
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transverse Section
Optical micrography of the longitudinal section of the drill collar, in the center of the thickness, presenting slightly elongated grains of fully austenitic microstructure, cold worked. The material presented 38HRc hardness.
58
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Optical micrography of the longitudinal section of the drill collar, in the center of the thickness, presenting slightly elongated grains of fully austenitic microstructure, cold worked.
62
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section

+4 more from this case →