Sampling and Analysis

154 cases · 925 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Sampling and Analysis — sub-branches

At the Surface 77Base Metal 65Broken Testpiece 9Close to the External Surface 41Close to the Internal Surface 33External Surface 27Fusion Line 29General View 132Heat Affected Zone 82In the Center of the Thickness 36In the Center of the Weld 2Internal Surface 33Longitudinal Section 102Low Mag 17Microhardness Indentations 1Microhardness identations 2Radial Section 3T/4 of the external surface 2Transverse Section 60Weld Metal 96Weld Repair 7Welded Joint 69

Results

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The location of the threaded fitting started leaking after less than five years in service. Although the corrosion rate was not high, the localized material loss in the threaded surface of the carbon steel flange allowed the connection leakage.
769
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Aspect Before AnalysisDf - General View
Front wheel 17 x 7J of a passenger vehicle (identified as WHEEL 1) that broke during a car accident on a road.
1644
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Aspect Before AnalysisDf - General View
Tool fixture 5" long, nominal diameter 2", presenting a recess 1/2" deep from two sides. The rupture occurred about 2" from the end of the rod. Scale in milimeters.
523
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Pinion of hypoid gearbox, assembled in a 1560-mm long shaft that operated during more than 60,000 hours, and removed from service due to unacceptable wear damage.
1028
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Aspect Before AnalysisDf - General View
Aspect of the 3 1/2" diameter tube after the water leakage in high temperature.
962
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - Aspect Before AnalysisDf - General View
2" drain line from the main 10" line. The leakage occurred at the margin of the weld, a short time after the introduction of the reinforced ribs to reduce vibration.
641
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Field photoDf - General View
The drilling connector, 21" diameter, presented a crack at the margin of the weld in the forging side (left side of the weld in the figure).
744
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Aspect Before AnalysisDf - General View
Identification of the regions of metallographies of the base metal, heat affected zone (HAZ) and weld metal. Locations in the root, in the center of the thickness and close to the tube OD (external surface).
118
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - NItal Etched MacroDf - Welded Joint

More from these cases

ML00184 — Dissimilar Steels in a Threaded ConnectionM - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
The cleaned fitting is sound. No corrosion, only surface stains.
121
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Aspect After CleaningDf - General View
Micrography of the valve body carbon steel thread, in the valley. Ferritic-bainitic structure.
77
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Transverse Section
ML00183 — Ductile Behavior of an Aluminum WheelM - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Front wheel 17 x 7J of a passenger vehicle (identified as WHEEL 2) that cracked exactly in the same location that the other front wheel broke.
91
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Aspect Before AnalysisDf - General View
Aspect of the two wheels before disassembling the tires.
75
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Aspect Before AnalysisDf - General View
Low magnification view of the WHEEL 1 fracture surface. The thickness of the wheel in this position (flat and paralell to the wheel face) is about 2.5 mm. The aspect of the fracture is similar all through the fracture perimeter, including the region where the fracture propagation changes the direction.
66
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Fractography by SEMDf - General View
Macrography of a radial section of the WHEEL 1. The fracture occurred in the cylindrical wheel outer edge, the rim, and the thickness of the part in the fracture location varied from 2.5 mm to 4 mm.
62
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Keller Etched MacroDf - Radial Section
Macro view of a fractured wheel spoke section showing an irregular, shear-lip fracture edge consistent with ductile overload.
52
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Keller Etched MacroDf - Radial Section

+1 more from this case →

ML00182 — Brittle Fracture of a LAS Fixing RodM - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Low magnification micrography presenting segregation bands in a martensitic structure. In the segregated regions the Nital etch effect is lower and the bands appear lighter. The black spots and lines are inclusions (some elongated) in the band.
91
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Low magnification micrography, revealing (in black) the impurities in the segregated bands.
63
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Micro by OM, picric acid+FeCl3+H2O etchDf - Longitudinal Section
Broken tensile testpiece fractography showing predominantly dimples as the fracture micromechanism, and some integranular aspects. It shows that in this uniaxial and without stress concentration raisers, the material presented a ductile behavior.
30
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Fractography by SEMDf - Broken Testpiece
Broken Charpy V testpiece fractography showing intergranular fracture micromechanism. It reveals the brittle material behavior when under critical conditions, like the one that was present in the service application (with a triaxial condition in the notch).
26
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Fractography by SEMDf - Broken Testpiece
ML00181 — Wear of a Carburized Hypoid GearM - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Detail of the 13 teeth hypoid gear, presenting a large longitudinal crack in the middle of one teeth.
105
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Aspect Before AnalysisDf - General View
Micrography of the tooth gear, in a transverse section, close to surface. The material presents light ghost marks that reveal chemical segregations.
80
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrography of the tooth gear, in a transverse section of center region. Again, some segregation patterns are visible.
58
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Aspect of the fractured tooth in a region presenting pitting, opening voids, and cracks.
51
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Surface Aspect by SEMDf - At the Surface
Wear of a Carburized Hypoid Gear
1
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Aspect Before AnalysisDf - General View
ML00180 — Local Melting of Copper Cooling TubesM - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
View of the iinternal side of the tube (water side), deformed in the overheated area. There are several leaking points.
115
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - Aspect Before AnalysisDf - Internal Surface
Macroscopic aspect after cutting longitudinally in two halfs, at the damaged area. The tube internal surface showed a red copper colour at the overheated region and the perforation is associated to longitudinal cracks.
104
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - Longitudinal Section AspectDf - Internal Surface
Micrographic aspect of the tube out of the damaged region, in a longitudinal section, showing the grain refined copper structure.
96
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - FeCl3+HCl+H2O Etched MicroDf - In the Center of the Thickness
ML00179 — Hydrides in Titanium WeldM - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Low magnification micrography transverse to the fillet weld in the pipe. The pipe base metal is to the bottom of the figure and the weld metal is to the top. The heat affected zone in the middle, shows a coarse grain size structure.
59
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Welded Joint
Low magnification micrography showing the weld metal, full of pores, indicating that the field welding was not properly shileded.
50
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal
Coarse grains in the heat affected zone.
46
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Heat Affected Zone
Micrography of the weld metal at the fillet weld where the cracking started, showing several brittle microcracks that corresponds to the regions where the fractography showed secondary crackis.
35
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal
Micrographic detail of the weld metal brittle microcracks, in regions with hydrides formation.
32
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal

+8 more from this case →

ML00178 — Cold cracks in Cr-Mo Welded ForgingM - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Circumferential weld aspect. Two passes in the cap. This forging to pipe welded joint, 22 mm thick, was welded by an automatic process in a narrow gap. The pipe is to the top of the image and the forging is to the bottom of the image.
165
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Aspect Before AnalysisDf - External Surface
Macrography of the welded joint between the forging and the pipe, showing it was welded in a narrow gap, indicating by the arrow the location of the crack at the margin of the weld, in the forging side.
129
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - NItal Etched MacroDf - Welded Joint
Quenched and tempered structure of the F22 steel forging, presenting about 230HV10 average hardness.
133
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
Fusion line of the forging side, in the cap, showing the weld metal (to the top of the image) and the base metal (to the bottom of the image). The heat affected zone hardness is about 270HV10.
108
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Quenched and tempered heat affected zone of the forging.
75
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by SEMDf - Heat Affected Zone

+1 more from this case →

ML00177 — Cr-Mo Seam Welded TubeM - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
BASE METAL SURFACE - Ferritic structure, grain refined.
90
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Base Metal
HAZ SURFACE
72
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Last Bead HAZ
HAZ SURFACE
66
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Last Bead HAZ
WELD METAL SURFACE
47
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Weld Metal in the Cap
WELD METAL SURFACE
43
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Weld Metal in the Cap

+10 more from this case →