Sampling and Analysis

10 cases · 69 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Bainite clear all

Sampling and Analysis — sub-branches

At the Surface 2Base Metal 12Close to the External Surface 2Close to the Internal Surface 2External Surface 2Fusion Line 3General View 5Heat Affected Zone 9In the Center of the Thickness 1Internal Surface 1Longitudinal Section 9Weld Metal 13Welded Joint 8

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Aspect of the waterwall during removal of the leaking tube. The leakage was detected, by visual inspection, from the outside of the boiler.
1675
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Field photoDf - General View
The 6 1/2" nominal diameter longitudinal seam welded pipe is internally cladded with Alloy 625. The pipe was manufactured by forming a cladded plate (probably welded by rolling) and welding it longitudinally. The pipe was heat treated (quenched and tempered) after the seam weld.
96
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Aspect Before AnalysisDf - Welded Joint
The 4 1/2" nominal diameter seamless pipe internally overlaid with Alloy 625. This pipe corresponds to a 90° curve. The overlaid pipe was heat treated before and after bending. The final quenching and tempering heat treatment was conducted to meet API 5L X70 properties.
113
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Aspect Before AnalysisDf - Welded Joint
Shaft pinion presenting the bearing surface, with machining markes, from where the thermal spray layer was detached. The diameter of the 880 mm long shaft in this region is about 75 mm.
426
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - Aspect Before AnalysisDf - General View
Aspect of the superheater ND 1" tube that was in operation for about 35,000 hours and presented a thick deposit at the external surface.
211
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Aspect Before AnalysisDf - General View
Macrography of the tubular forging, butt welded using a LAS filler metal, and overlaid using Inconel 625 filler metal. The micrographic characterization was conducted for the HAZ of the overlay and for the HAZ of the butt weld, at the root position (with several welding cycles) and at the face.
608
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Electrolytically Etched MacroDf - Welded Joint
Aspect of three pins that were operating in a hydraulic system. Adjacent to the fracture of the broken pin (the one that is in the right side of the figure) it is possible to see multiple surface craks and detachment of the surface chromium layer.
88
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View
The macrography of a longitudinal section of the pipe and connector, at the welded joint, shows that the welding was conducted from both side of the groove, starting from the ID and finishing from the OD, ID later machined flush. The cracking was detected by ultrasonic test and the macro shows that it is at the fusion line, growthing into the weld metal. See the schematic drawing in the next figure
535
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - NItal Etched MacroDf - Longitudinal Section

More from these cases

ML00163 — Corrosion Fatigue of a Boiler Waterwall TubeM - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Aspect of the tube internal surface after removal from the boiler, presenting multiple longitudinal cracks.
295
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Internal Surface
Aspect of the external surface of the leaking tube, after removal of the membrane.
262
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - External Surface
Micrography of the external tube surface, presenting a crack at the weld margin. This cracking could have been created by thermal induced cycles (fatigue), but it did not propagate into the tube wall. In some regions of the external side of the tube the weld metal was detached.
77
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - External Surface
Micrography of the external tube surface, presenting the cracking at the margin of the weld. This cracking could have been created by thermal induced cycles (fatigue), but it did not propagate into the tube wall.
85
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Fusion Line
ML00133 — Seam Welded Pipe Cladded with Alloy 625M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
The macrography of a longitudinal section shows the low alloy (C-Mn) steel pipe, internally cladded with Ni alloy clad plate.
72
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Electrolytically Etched MacroDf - Longitudinal Section
Micrography of a longitudinal section of the pipe substrate, in low magnification, showing a uniform microstructure,
51
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure obtained by the pipe quenching and tempering,
48
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
ML00132 — Seamless Pipe Overlaid with Alloy 625M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
The macrography of a longitudinal section shows the low alloy (C-Mn) steel pipe, internally cladded by overlay in two layers.
88
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytically Etched MacroDf - Longitudinal Section
Micrography of a longitudinal section of the pipe substrate, in low magnification, showing a uniform microstructure,
79
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure obtained by the pipe quenching and tempering,
72
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Low magnification micrography of a longitudinal section of the pipe at the interface between overlay layers, with electrolytic etch that reveals the Ni alloy structure, large columnar grains with celular morphology.
66
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Chromic Acid Electrolytic EtchedDf - Weld Metal
Micrography of a longitudinal section of the pipe at the interface between overlay layers, with electrolytic etch that reveals the Ni alloy structure, large grains with celular dendritic morphology.
52
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Chromic Acid Electrolytic EtchedDf - Weld Metal

+1 more from this case →

ML00108 — Thermal Spray Layer in a Pinion ShaftM - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Macrographic detail of the thermal spray layer in a position of the shaft where it was not detached. Longitudinal section of the shaft. The waves are the machining marks created to anchor the thermal spray layer, that is about 1.5mm thick.
41
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - NItal Etched MacroDf - Longitudinal Section
Shaft microstructure in the longitudinal section, showing aligned segregations typical of the material forming.
31
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
ML00107 — Carburized 9Cr1MoV Superheater TubeM - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
The macrography of a longitudinal section shows that the tube did not present local thinning in any region, but the internal and external scales are evidenced. The external surface (OD) is to the top of the figure and the internal surface (ID) is to the bottom of the figure.
124
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - NItal Etched MacroDf - Longitudinal Section
Micrography of the longitudinal section of the tube, close to the external surface, presenting a thick deposit.
110
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - As polished micrographyDf - Close to the External Surface
Micrography of the longitudinal section of the tube, close to the internal surface, presenting a thick deposit.
98
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography of the longitudinal section of the tube, close to the external surface. A scale is evident at the surface as well as a carburizing layer.
83
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of the longitudinal section of the tube, close to the internal surface. A thick scale is evident, but no microstructural changes compared to the center of the tube.
92
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00102 — AISI 4130 Forging Welded and OverlaidM - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Micrography of the 4130 steel, normalized and tempered. The structure is sligthly banded (segregated) and the average hardness level is 20 HRc.
92
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the 4130 steel, normalized and tempered. The microstructure is bainitic.
88
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) of the Inconel overlay (white because it was not etched with the Nital). The structure is ferritic/bainitic because the overlay was conducted in two layers, and all the HAZ was reheated during welding.
66
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) of the Inconel overlay (white because it was not etched with the Nital). The structure is ferritic/bainitic because the overlay was conducted in two layers, and all the HAZ was reheated during welding.
61
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the tubular 4130 forging at the heat affected zone (HAZ), butt weld face. The structure is tempered martensite because the welded joint was PWHT at 630°C. The original forging was normalized and tempered at 660°C.
48
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone

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ML00081 — Hydrogen Cracking of a Chromium Plated Carburized PinM - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Micrography of a longitudinal section of the pin, in the center. The low carbon content of the steel in the center of the pin makes the structure bainitic even though it was quenched and tempered after carburizing.
80
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrographic detail a longitudinal section of the pin, at the surface, showing the case hardened. The pin carburized, quenched and tempered structure presents a gradient of carbon content and consequently a gradient of martensitic structure and hardness. Close to the surface the hardness level is 742 HV1 .
87
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - At the Surface
Scanning electron fractography showing that the fracture micromechanism is intergranular close to the surface of the pin, suggesting a hydrogen embrittlement effect at the carburized layer. The cracks were created during the electrolytic plating, and propagated later during service.
45
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - At the Surface
ML00072 — Liquation Cracks in a High Strength JointM - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Schematic drawing presenting the longitudinal section of the pipe and connector at the welded joint
105
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Identification drawingDf - Longitudinal Section
Hot cracking at the fusion line of the connector side, in a welded joint between a forging and a pipe, in a macrographic sample. The region of the heat affected zone of the connector presents a dendritic aspect suggesting that the forging reduction rate of the connector was not too high and did not broke the cast structure.
110
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - NItal Etched MacroDf - Welded Joint
The connector was welded to the pipe from both (internal and external) sides, a PWHT was applied and the part was machined. The UT indication was detected during final inspection.
78
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Aspect Before AnalysisDf - General View
The liquation crack is a hot crack in the base metal (at the HAZ) that induces a solidification crack in the weld metal.
66
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Weld Metal
Micrographic detail of the cracks at the fusion line of the welded joint, at the connector side. The cracking presents morphology of melting regions of impurities at grain boundaries of the large grains of the heat affected zone (HAZ).
57
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Fusion Line

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