Sampling and Analysis

14 cases · 101 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Ship clear all

Sampling and Analysis — sub-branches

At the Surface 5Base Metal 3Close to the External Surface 9Close to the Internal Surface 7External Surface 6General View 22Heat Affected Zone 8In the Center of the Thickness 9Internal Surface 4Longitudinal Section 5Transverse Section 7Weld Metal 1Welded Joint 15

Results

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Pinion of hypoid gearbox, assembled in a 1560-mm long shaft that operated during more than 60,000 hours, and removed from service due to unacceptable wear damage.
1028
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Aspect Before AnalysisDf - General View
Aspect of the broken spring. The wire is 36 mm diameter and the ourter diameter of the spirals is 320 mm. It was broken in different locations.
434
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Aspect before cleaning of the heavy U bolt pipe clamp, 38 mm diameter wire, at the fractured position. It is possible to see that it broke in a region where the clamp was no longer coated and there is no insert in the groove (at the internal clamp diameter). The fracture is transverse to the clamp axis.
522
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - General View
Tin Bronze Wear Ring of Seawater Pump
2
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - General View
Aspect "as received" of the seamless tube at the curved position, showing the longitudinal crack and corrosion products at the tube surface.
836
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Macroscopic aspect of the outer diameter of the flanged sleeve presenting adhered products at the surface. The flanged sleeve was manufactured by centrifugal casting in a lean duplex stainless steel and it was externally coated by thermal spray (TS) in a position of sealing. After 5 years in service the system suffered leakage.
569
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Aspect Before AnalysisDf - External Surface
Fractured position of the casting cylinder of 10.5 mm thickness (minimum measured thickness) showing a brittle behavior (lack of plastic deformation), typical of overloading a material with 1% ductility (measured in the tensile test). This is the view of the internal surface of the cylinder, presenting regions of localized thinning in this surface that was in contact with (treated) cooling water. The external side of the cylinder was painted.
918
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fracture Surface AspectDf - General View
Micrography of the pipe transverse section presenting a granular microstructure.
147
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Nital Etched Micrography by OMDf - Transverse Section

More from these cases

ML00181 — Wear of a Carburized Hypoid GearM - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Detail of the 13 teeth hypoid gear, presenting a large longitudinal crack in the middle of one teeth.
105
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Aspect Before AnalysisDf - General View
Micrography of the tooth gear, in a transverse section, close to surface. The material presents light ghost marks that reveal chemical segregations.
80
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrography of the tooth gear, in a transverse section of center region. Again, some segregation patterns are visible.
58
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Aspect of the fractured tooth in a region presenting pitting, opening voids, and cracks.
51
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Surface Aspect by SEMDf - At the Surface
Wear of a Carburized Hypoid Gear
1
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Aspect Before AnalysisDf - General View
ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Micrography of a transverse section of the spring, at the surface showing pits full of deposits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
Rusted aspect of the spring surface.
26
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Micrography of the transverse section of the spring wire, in the center, presenting a refined structure and segregation bands that are detected only in low magnification.
24
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
ML00171 — Corrosion Fatigue of U Bolt Pipe ClampM - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Aspect of the U bolt clamp with partial detachment of the coating (white brown) in a region where the polimeric insert (dirty white) is still in the wire groove at the internal clamp diameter (ID).
91
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - General View
Metallographic image of a longitudinal section of the clamp (axis in the vertical direction), showing a refined ferritic perlitic structure.
34
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
The clamp presented several cracks, parallel, transverse to the axis. The appearance of the cracks in the metallographic section shows that some cracks propagate and growth with a irregular path.
24
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
ML00166 — Tin Bronze Wear Ring of Seawater PumpM - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Tin Bronze Wear Ring of Seawater Pump
2
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - General View
ML00165 — SCC of Aluminum Bronze Heating CoilM - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Aspect of the external tube surface after cleaning. It is possible to see that the cracks are longitudinal to the tube and localized in positions where the surface is corroded.
132
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Surface AspectDf - External Surface
Aspect of the internal tube surface after a longitudinal cut, without cleaning. It is possible to see a clean surface inside the tube.
104
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Surface AspectDf - Internal Surface
Micrography of the external side of the bent tube, showing detachement of several grains due to intergranular corrosion. The corroded layer is about 200 microns thick at this position. The differences of colours in the corroded layer suggests a dealloying effect, also known as selective leaching.
71
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - External Surface
Micrography of a tube transverse section, at the through wall cracking position, showing intergranular morphology of the stress corrosion cracking. In the center of the thickness, far from the external surface corroded layer, the cracks are intergranular but did not present any dealloying evidence.
49
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - In the Center of the Thickness
SCC of Aluminum Bronze Heating Coil
1
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View

+2 more from this case →

ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Detail of the external surface of the sleeve where the surface coating was detached, creating a lack of sealing condition.
67
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Surface AspectDf - External Surface
General view of the 10" diameter flanged sleeve, 1/2" wall thickness, manufactured by centrifugal casting of lean duplex stainless steel (DSS), Alloy 2304 (without Mo), with an external coating applied by thermal spray (TS). The sleeve is assembled in a shaft. The internal environment is oil and a seal box is assembled in the external side that is wet with seawater.
56
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Aspect Before AnalysisDf - General View
Longitudinal slice of the flanged sleeve, 180 mm long, in a macrography presenting the 1/2" tubular wall thickness where the sealing was applied. The external surface of the sleeve (seawater wet) is in the left side of the figure and the internal surface (oiled) is in the right side. The flange is to the top of the figure.
52
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Longitudinal Section AspectDf - General View
Micrography of a longitudinal section of the sleeve, at the external surface where there are two layers of coating. The electrolytic etch evidenced the duplex stainless steel substrate (bottom of the figure) and the weave interface of the substrate and the first thermal spray layer, about 1 mm thick, in a stainless steel. The surface layer, of tugnsten carbide, about 0.2 mm thick, is black and not clearly visible in this figure.
50
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - External Surface
Micrography of the longitudinal section of the sleeve, at the interface between the substrate and the first thermal spray layer. The substrate (bottom of the figure) shows a ferritic-austenitic microstructure and detrimental phases that look like sigma. The thermal spray layer (top of the figure) presents the non-etched stainless steel, disposed in layers, with oxides (gray) and voids (black). The substrate is deformed in a thin layer at the interface.
38
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Close to the External Surface

+5 more from this case →

ML00141 — Brittle Fracture of a Corroded Gray Cast IronM - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), close to the internal surface (left side). It is possible to see large graphite flakes.
98
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - Close to the Internal Surface
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), in the center of the thickness. It is possible to see a mixture of large graphite flakes and rosette grouping flakes.
80
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - In the Center of the Thickness
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), close to the external surface (left side). It is possible to see smaller graphite flakes, interdendritic .
79
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - Close to the External Surface
The fracture surface of the casting cylinder presented, at the internal surface, interconnected graphite flakes and a corroded matrix.
73
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fractography by SEMDf - Close to the Internal Surface
The fracture surface of the casting cylinder presented, in the center of the thickness, cleavage facets and graphite decohesion that corresponds to a brittle fracture of the material.
61
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fractography by SEMDf - In the Center of the Thickness

+16 more from this case →

ML00140 — Preferential Corrosion of Pipe Seam WeldM - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Aspect of the 4" pipe that was in seawater service for 8 years and leaked in a longitudinal line that corresponds to the seam weld. The internal surface presented thick deposits. Although the pipe was cut with a thermal process, the analysis was conducted after mechanical cutting.
100
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Aspect Before AnalysisDf - General View
Detail of the transverse section of the 4" pipe 90° from the seam weld. The thickness of the pipe is 8 mm. No evidences of general corrosion or pitting were identified.
77
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Transverse Section
Detail of the transverse section of the 4" pipe 90° from the seam weld. The thickness of the pipe is 8 mm. No evidences of general corrosion or pitting were identified.
70
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Transverse Section
Detail of the transverse section of the 4" pipe 180° from the seam weld. The thickness of the pipe is 8 mm. No evidences of general corrosion or pitting were identified.
64
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Transverse Section
Aspect of the internal surface of the pipe after cleaning, showing the leakage line.
67
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Aspect Before AnalysisDf - Internal Surface

+2 more from this case →