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Crevice Corrosion in a Subsea System — Aspect Before Analysis

24 images

TryAustenitic Stainless SteelML00072corrosionFerrous AlloysML00128brittle fractureAusteniteductile behaviorGranularfatigueRaw MaterialhydrogenFinished Productfractureembrittlementstress corrosion
Application: Chemical Industry Capture method: Optical Microscope Detail focus: Microstructure clear all
M

Material

79 classified

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P

Product

96 classified

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Ap

Application

37 classified

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C

Condition

84 classified

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Cm

Capture method

52 classified

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Df

Detail focus

208 classified

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Microstructure14
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Standard29
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The Materials
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24 images
Granular alpha structure of the pipe base metal.
49
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Alpha
Micrography of a longitudinal section of the stub end showing a refined austenitic structure.
57
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
SAMPLE 1 AT THE FRACTURE - Micrography at the position where the thickness is reduced to zero. Side A to the bottom. The microstructure is austenite with intergranular and transgranular precipitation. The position of the zero thickness presents aspect of an intergranular fracture, and in side A there are several intergranular cracks from the surface.
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in the colder part of the equipment, position 1. The material presented carbide precipitation at grain boundaries (not yet fully surrounding the grains) and at this point the tube presented no internal corrosion.
338
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
The shell plate micrography showed an austenitic structure.
101
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Austenite
The microstructure of the pipe base metal, in the center of the thickness, is granular alpha.
102
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Granular structure
Microstructure of the fitting in the transverse section, presenting a granular Ni austenitic structure. No evidences of any phase in the grain boundaries.
114
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Kalling Etched Micrography by OMDf - Austenite

More from these cases

ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Micrographic detail of the austenitic structure. Free from grain boundaries carbide precipitation.
54
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
SAMPLE 1 AT 1 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary precipitation, intergranular and intragranular.
76
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
SAMPLE 1 AT 1 mm THICKNESS - Micrographic detail of the austenite with secondary precipitation. This oxalic acid electrolytic etch is revealing the integranular and transgranular (or intragranular) precipitation. In the grain boundaries it is possible to see: 1) a continuous network of carbide precipitation and 2) isolated islands of sigma phase. In the middle of the grains there are rounded and neddles like carbides.
72
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
SAMPLE 2 AT 2 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary precipitation, intergranular and intragranular. There are no variations in the microstructure comparing to sample 1.
48
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Secondary Precipitation
SAMPLE 2 AT 2 mm THICKNESS - Micrographic detail of the austenite with secondary precipitation. This oxalic acid electrolytic etch is revealing the integranular and transgranular (or intragranular) precipitation. In the grain boundaries it is possible to see: 1) a continuous network of carbide precipitation and 2) isolated islands of sigma phase. In the middle of the grains there are rounded and neddles like carbides. There are no variations in the microstructure comparing to sample 1.
43
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Intergranular Precipitation
SAMPLE 3 AT 4 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary intergranular and intragranular precipitation, but this micrography was obtained in the longitudinal section, presenting the plate alignment and was etched with NaOH, adopted to colour the sigma phase.
45
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - NaOH Electrolytic Etched MicroDf - Austenitic with Secondary Precipitation

+4 more from this case →

ML00086 — Intergranular Corrosion of Sensitized 304SSM - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 2, where the temperature was higher and the carbide precipitation increased during service.
272
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 3, where intergranular and transgranular carbide precipitation occurred during service.
234
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation
Micrography of a longitudinal section of the tube in position 3, at the internal surface. Although there is a strong precipitation, both intergranular and transgranular, the tube did not corrode at this point.
144
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation
Micrographic detail of the internal side of the tube in position 3, with a strong intergranular and transgranular precipitation, but no corrosion at this point.
153
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation
ML00005 — Environmental Hydrogen Damage in Ti PipeM - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
The microstructure of the pipe seam weld metal, in the center of the thickness, presents a coarse prior beta grain size.
85
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Columnar Grains
ML00011 — Intergranular SCC of Pure NickelM - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Microstructure of the fitting in the transverse section, presenting a granular Ni austenitic structure. No evidences of any phase in the grain boundaries.
110
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Kalling Etched Micrography by OMDf - Austenite
Microstructure of the fitting in the transverse section, presenting a granular Ni austenitic structure. No evidences of any phase in the grain boundaries.
96
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Kalling Etched Micrography by OMDf - Austenite

View all 24 images in the Atlas →

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The location of the threaded fitting started leaking after less than five years in service. Although the corrosion rate was not high, the localized material loss in the threaded surface of the carbon steel flange allowed the connection leakage.
769
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Aspect Before AnalysisDf - General View
Front wheel 17 x 7J of a passenger vehicle (identified as WHEEL 1) that broke during a car accident on a road.
1644
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Aspect Before AnalysisDf - General View
Tool fixture 5" long, nominal diameter 2", presenting a recess 1/2" deep from two sides. The rupture occurred about 2" from the end of the rod. Scale in milimeters.
523
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Pinion of hypoid gearbox, assembled in a 1560-mm long shaft that operated during more than 60,000 hours, and removed from service due to unacceptable wear damage.
1028
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Aspect Before AnalysisDf - General View
Aspect of the 3 1/2" diameter tube after the water leakage in high temperature.
963
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - Aspect Before AnalysisDf - General View
2" drain line from the main 10" line. The leakage occurred at the margin of the weld, a short time after the introduction of the reinforced ribs to reduce vibration.
641
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Field photoDf - General View
The drilling connector, 21" diameter, presented a crack at the margin of the weld in the forging side (left side of the weld in the figure).
745
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Aspect Before AnalysisDf - General View
Macrography of the longitudinally seam weld of the 24" diameter tube, showing that it was welded from both sides and there is a segregation line in the center of the tube thickness.
737
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - NItal Etched MacroDf - Seam
The titanium rotor blade of a flowmeter broke after two years in service in an acid environment, containing H2S.
339
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Aspect Before AnalysisDf - General View
Aspect of the wire rope, 1 1/2" diameter, presenting regions of flattened areas at the surface of the outer wires. It is a 6 x 19 Seale construction, right regular lay.
553
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Aspect Before AnalysisDf - General View
The carcass was manufactured using niobium stabilized plates, grade AISI 347, with circumferential welds, where the through wall cracks were detected.
302
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Field photoDf - General View
Aged microstructure of the HP stainless steel, modified with 1%Nb, cast fitting, tubular, operating for 6 years in a furnace which design temperature is 1100°C. The material presented a network of primary carbides, white and grey, and an austenitic matrix with coalescing secondary precipitation. Some voids. The Vickers identation indicates a hardness value about 260HV 100g in the aged austenitic matrix.
492
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Microhardness identations

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