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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Pinion of hypoid gearbox, assembled in a 1560-mm long shaft that operated during more than 60,000 hours, and removed from service due to unacceptable wear damage.
1028
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Aspect Before AnalysisDf - General View
Aspect of the broken spring. The wire is 36 mm diameter and the ourter diameter of the spirals is 320 mm. It was broken in different locations.
434
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Aspect before cleaning of the heavy U bolt pipe clamp, 38 mm diameter wire, at the fractured position. It is possible to see that it broke in a region where the clamp was no longer coated and there is no insert in the groove (at the internal clamp diameter). The fracture is transverse to the clamp axis.
522
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - General View
Macrography of a ring transverse section presenting a large variation in the grain size, revealing the diferences in the solidification rate.
453
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O solution Etched MacroDf - Casting Structure
Aspect "as received" of the seamless tube at the curved position, showing the longitudinal crack and corrosion products at the tube surface.
836
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Macroscopic aspect of the outer diameter of the flanged sleeve presenting adhered products at the surface. The flanged sleeve was manufactured by centrifugal casting in a lean duplex stainless steel and it was externally coated by thermal spray (TS) in a position of sealing. After 5 years in service the system suffered leakage.
569
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Aspect Before AnalysisDf - External Surface
Fractured position of the casting cylinder of 10.5 mm thickness (minimum measured thickness) showing a brittle behavior (lack of plastic deformation), typical of overloading a material with 1% ductility (measured in the tensile test). This is the view of the internal surface of the cylinder, presenting regions of localized thinning in this surface that was in contact with (treated) cooling water. The external side of the cylinder was painted.
918
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fracture Surface AspectDf - General View
Aspect of a transverse section of the 4" pipe showing the barnacles adhered to the internal pipe surface, and the leakage position (in the top of the figure). It is possible to see that the deposits are attached all throught the internal pipe perimeter but the damage is localized. The damage morphology suggests it is a crack, or a welding defect, but the microstructural analysis indicated that the damage is a galvanic effect at the autogenous seam weld.
1135
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Longitudinal Section AspectDf - Localized Corrosion

More from these cases

ML00181 — Wear of a Carburized Hypoid GearM - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Detail of the 13 teeth hypoid gear, presenting a large longitudinal crack in the middle of one teeth.
105
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Aspect Before AnalysisDf - General View
Macrography of a transverse section of a sound tooth, presenting a carburized layer of about 3 mm depth.
87
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - NItal Etched MacroDf - Carburized Layer
Micrography of the tooth gear, in a transverse section, close to surface. The material presents light ghost marks that reveal chemical segregations.
80
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrographic detail of the case hardened martensitic structure, close to the surface, with a microhardness level of about 600 Vickers (load 0.3kg).
70
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the tooth gear, in a transverse section of center region. Again, some segregation patterns are visible.
58
VIEW
ML00181 / Apr.2022
Wear of a Carburized Hypoid Gear
M - Low Alloy for Thermochemical TreatmentP - Pinion-crown assemblyAp - ShipCd - Wear
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness

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ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Aspect of the fracture of the spring. The spring surface shows shallow pits.
49
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Fracture
Surface to fracture interface. The spring shows corrosion and pits.
46
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Corrosion
Aspect of the spring surface, with a layer of corroded products, and pits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Surface Aspect by SEMDf - Corrosion
Micrography of a transverse section of the spring, at the surface showing pits full of deposits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
Micrographic detail of the transverse section of the spring, at the surface, showing the pits full of corrosion deposits.
31
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Surface Deposits

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ML00171 — Corrosion Fatigue of U Bolt Pipe ClampM - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Aspect of the U bolt clamp with partial detachment of the coating (white brown) in a region where the polimeric insert (dirty white) is still in the wire groove at the internal clamp diameter (ID).
91
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - General View
Detailed aspect of the fractured position, in a region where the clamp was no longer coated and there is no insert in the groove (at the internal clamp diameter). The fracture is transverse to the clamp axis.
86
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Fracture
Same aspect of the previous image after cleaning, showing a subcritical propagation aspect (fatigue), starting at the groove (ID) and also at the clamp surface in the OD.
75
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Fracture
In the region where the polimeric insert was loose, the protective coating of the clamp has suffered detachment.
69
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Layer Detachment
Close to the ID of the clamp, at the groove position, there are cracks in the coating (white brown) and also at the substrate.
63
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Cracks

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ML00166 — Tin Bronze Wear Ring of Seawater PumpM - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Low magnification micrography of a transverse section of the ring showing a dendritic structure.
64
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of a transverse section of the ring showing a cored alpha structure with segregation at interdendritic regions. This structure is in a region close to the ring surface.
52
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of a transverse section of the ring showing a cored alpha structure with strong segregation at interdendritic regions, and regions of a white structure at grain boundaries. This structure is in a region close to the center of the ring.
51
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrographic detail of the cored alpha structure with light segregation at intergranular regions (light layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the ring surface, where the solidification was quicker.
49
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics
Micrographic detail of the cored alpha structure with strong segregation at intergranular regions (dark layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the center of the ring, where the solidification was slower.
47
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics

+2 more from this case →

ML00165 — SCC of Aluminum Bronze Heating CoilM - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Aspect of the external tube surface after cleaning. It is possible to see that the cracks are longitudinal to the tube and localized in positions where the surface is corroded.
132
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Surface AspectDf - External Surface
Aspect of the internal tube surface after a longitudinal cut, without cleaning. It is possible to see a clean surface inside the tube.
104
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Surface AspectDf - Internal Surface
Micrography of the tranverse section of the tube, in the center of the thickness. There are small grains and large grains, characterizing a dual grain size. The large grains size is about 100 microns, more than 10 times larger than the average size of the smaller grains size.
101
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Dual grain sizes
Micrographic detail of the alpha microstructure presenting dual grain sizes. Two different types of twins are presented in the structure: annealing twins and deformation twins, suggesting that the material was probably partially recristalized after cold deformation and stress relief treatment.
87
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Alpha
Micrography of a transverse section of the bent tube, external surface (OD) to the top and internal surface (ID) to the bottom of the figure. At the through wall cracking position, the external surface presented a layer of intergranular corrosion.
95
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - As polished micrographyDf - Cracking

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ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Detail of the external surface of the sleeve where the surface coating was detached, creating a lack of sealing condition.
67
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Surface AspectDf - External Surface
General view of the 10" diameter flanged sleeve, 1/2" wall thickness, manufactured by centrifugal casting of lean duplex stainless steel (DSS), Alloy 2304 (without Mo), with an external coating applied by thermal spray (TS). The sleeve is assembled in a shaft. The internal environment is oil and a seal box is assembled in the external side that is wet with seawater.
56
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Aspect Before AnalysisDf - General View
Longitudinal slice of the flanged sleeve, 180 mm long, in a macrography presenting the 1/2" tubular wall thickness where the sealing was applied. The external surface of the sleeve (seawater wet) is in the left side of the figure and the internal surface (oiled) is in the right side. The flange is to the top of the figure.
52
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Longitudinal Section AspectDf - General View
Macrographic aspect of the sleeve longitudinal section where the coating was applied in the external side (top of the figure). It is possible to see that the sleeve was manufactured by centrifugal casting, with elongated grains from the external side, and equiaxial grains close to the internal side (bottom of the figure). There is a weaved interface between the sleeve and the first layer of thermal spray coating, 1 mm thick; and a second layer of thermal spray coating, 0.2mm thick (almost imperceptible at this low magnification).
49
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MacroDf - Coating Layer
Micrography of a longitudinal section of the sleeve, at the external surface where there are two layers of coating. The electrolytic etch evidenced the duplex stainless steel substrate (bottom of the figure) and the weave interface of the substrate and the first thermal spray layer, about 1 mm thick, in a stainless steel. The surface layer, of tugnsten carbide, about 0.2 mm thick, is black and not clearly visible in this figure.
50
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - External Surface

+24 more from this case →

ML00141 — Brittle Fracture of a Corroded Gray Cast IronM - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Fracture aspect of the casting cylinder at the 10.5 mm thickness, showing a brittle behavior (lack of plastic deformation). The internal side of the cylinder is to the top of the figure, and the painted surface is to the bottom of the figure.
129
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fracture Surface AspectDf - Brittle Fracture
Detailed aspect of the cylinder fracture, the internal surface to the top of the figure and the painted external surface to the bottom of the figure.
103
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fracture Surface AspectDf - Brittle Fracture
Macrographic aspect of a section of the cast cylinder, transverse to the fracture (top). The internal diameter of the cylinder (exposed to treated water) is to the left side and the external diameter of the cylinder (painted) is to the right side.
96
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - NItal Etched MacroDf - Brittle Fracture
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), close to the internal surface (left side). It is possible to see large graphite flakes.
98
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - Close to the Internal Surface
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), in the center of the thickness. It is possible to see a mixture of large graphite flakes and rosette grouping flakes.
80
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - In the Center of the Thickness

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ML00140 — Preferential Corrosion of Pipe Seam WeldM - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Micrography of the pipe transverse section presenting a granular microstructure.
147
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Nital Etched Micrography by OMDf - Transverse Section
Micrography of the pipe transverse section presenting a predominatly ferritic-perlitic microstructure.
132
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the predominatly ferritic-perlitic microstructure. Pipe transverse section.
95
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Aspect of the 4" pipe that was in seawater service for 8 years and leaked in a longitudinal line that corresponds to the seam weld. The internal surface presented thick deposits. Although the pipe was cut with a thermal process, the analysis was conducted after mechanical cutting.
100
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Aspect Before AnalysisDf - General View
Detail of the transverse section of the 4" pipe at the longitudinal seam weld evidencing the leakage position. The damage appears as a through wall opening. The pipe thickness is 8 mm and there are no evidences of general corrosion (the SCH 80 corresponds to 8.6 mm) or pitting at the internal surface.
99
VIEW
ML00140 / May.2019
Preferential Corrosion of Pipe Seam Weld
M - Low Carbon SteelP - Longitudinal Seam Welded PipeAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Leakage

+19 more from this case →