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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Aspect of the broken spring. The wire is 36 mm diameter and the ourter diameter of the spirals is 320 mm. It was broken in different locations.
434
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Aspect before cleaning of the heavy U bolt pipe clamp, 38 mm diameter wire, at the fractured position. It is possible to see that it broke in a region where the clamp was no longer coated and there is no insert in the groove (at the internal clamp diameter). The fracture is transverse to the clamp axis.
522
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - General View
Macrography of a ring transverse section presenting a large variation in the grain size, revealing the diferences in the solidification rate.
453
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O solution Etched MacroDf - Casting Structure
Aspect "as received" of the seamless tube at the curved position, showing the longitudinal crack and corrosion products at the tube surface.
836
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Macroscopic aspect of the outer diameter of the flanged sleeve presenting adhered products at the surface. The flanged sleeve was manufactured by centrifugal casting in a lean duplex stainless steel and it was externally coated by thermal spray (TS) in a position of sealing. After 5 years in service the system suffered leakage.
569
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Aspect Before AnalysisDf - External Surface
Aspect of the broken spring. The wire is 1 1/2" diameter and the ourter diameter of the spirals is 12 1/2", in a 20" height spring. It was broken in several pieces.
866
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Aspect Before AnalysisDf - General View
Aspect of the CuZn platesheet where it is corroded (cooling medium side). The (hot) air cooler uses treated seawater as the cooling medium and the corroded regions are associated to the regions in the heat exchanger of higher temperatures, and the leakage occurred in regions of contact of the platesheet to cooper alloy tubes.
1167
VIEW
ML00125 / Mar.2018
Dezincification of a Cooler Tubesheet
M - BrassP - PlateAp - ShipCd - Preferential Dissolution
Cm - Aspect Before AnalysisDf - Corrosion
The hose connector fracture surface presented different fracture micromechanisms associated to the microstructure: inclusion decohesion, small regions of intergranular fractures (probably due to cementite at grain boundaries), and cleavage of the ferritic structure. All these mechanisms are brittle.
560
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Brittle Fracture

More from these cases

ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Aspect of the fracture of the spring. The spring surface shows shallow pits.
49
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Fracture
Surface to fracture interface. The spring shows corrosion and pits.
46
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Corrosion
Aspect of the spring surface, with a layer of corroded products, and pits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Surface Aspect by SEMDf - Corrosion
Micrography of a transverse section of the spring, at the surface showing pits full of deposits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
Micrographic detail of the transverse section of the spring, at the surface, showing the pits full of corrosion deposits.
31
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Surface Deposits

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ML00171 — Corrosion Fatigue of U Bolt Pipe ClampM - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Aspect of the U bolt clamp with partial detachment of the coating (white brown) in a region where the polimeric insert (dirty white) is still in the wire groove at the internal clamp diameter (ID).
91
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - General View
Detailed aspect of the fractured position, in a region where the clamp was no longer coated and there is no insert in the groove (at the internal clamp diameter). The fracture is transverse to the clamp axis.
86
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Fracture
Same aspect of the previous image after cleaning, showing a subcritical propagation aspect (fatigue), starting at the groove (ID) and also at the clamp surface in the OD.
75
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Fracture
In the region where the polimeric insert was loose, the protective coating of the clamp has suffered detachment.
69
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Layer Detachment
Close to the ID of the clamp, at the groove position, there are cracks in the coating (white brown) and also at the substrate.
63
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Cracks

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ML00166 — Tin Bronze Wear Ring of Seawater PumpM - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Low magnification micrography of a transverse section of the ring showing a dendritic structure.
64
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of a transverse section of the ring showing a cored alpha structure with segregation at interdendritic regions. This structure is in a region close to the ring surface.
52
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of a transverse section of the ring showing a cored alpha structure with strong segregation at interdendritic regions, and regions of a white structure at grain boundaries. This structure is in a region close to the center of the ring.
51
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrographic detail of the cored alpha structure with light segregation at intergranular regions (light layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the ring surface, where the solidification was quicker.
49
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics
Micrographic detail of the cored alpha structure with strong segregation at intergranular regions (dark layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the center of the ring, where the solidification was slower.
47
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics

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ML00165 — SCC of Aluminum Bronze Heating CoilM - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Aspect of the external tube surface after cleaning. It is possible to see that the cracks are longitudinal to the tube and localized in positions where the surface is corroded.
132
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Surface AspectDf - External Surface
Aspect of the internal tube surface after a longitudinal cut, without cleaning. It is possible to see a clean surface inside the tube.
104
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Surface AspectDf - Internal Surface
Micrography of the tranverse section of the tube, in the center of the thickness. There are small grains and large grains, characterizing a dual grain size. The large grains size is about 100 microns, more than 10 times larger than the average size of the smaller grains size.
101
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Dual grain sizes
Micrographic detail of the alpha microstructure presenting dual grain sizes. Two different types of twins are presented in the structure: annealing twins and deformation twins, suggesting that the material was probably partially recristalized after cold deformation and stress relief treatment.
87
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Alpha
Micrography of a transverse section of the bent tube, external surface (OD) to the top and internal surface (ID) to the bottom of the figure. At the through wall cracking position, the external surface presented a layer of intergranular corrosion.
95
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - As polished micrographyDf - Cracking

+12 more from this case →

ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Detail of the external surface of the sleeve where the surface coating was detached, creating a lack of sealing condition.
67
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Surface AspectDf - External Surface
General view of the 10" diameter flanged sleeve, 1/2" wall thickness, manufactured by centrifugal casting of lean duplex stainless steel (DSS), Alloy 2304 (without Mo), with an external coating applied by thermal spray (TS). The sleeve is assembled in a shaft. The internal environment is oil and a seal box is assembled in the external side that is wet with seawater.
56
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Aspect Before AnalysisDf - General View
Longitudinal slice of the flanged sleeve, 180 mm long, in a macrography presenting the 1/2" tubular wall thickness where the sealing was applied. The external surface of the sleeve (seawater wet) is in the left side of the figure and the internal surface (oiled) is in the right side. The flange is to the top of the figure.
52
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Longitudinal Section AspectDf - General View
Macrographic aspect of the sleeve longitudinal section where the coating was applied in the external side (top of the figure). It is possible to see that the sleeve was manufactured by centrifugal casting, with elongated grains from the external side, and equiaxial grains close to the internal side (bottom of the figure). There is a weaved interface between the sleeve and the first layer of thermal spray coating, 1 mm thick; and a second layer of thermal spray coating, 0.2mm thick (almost imperceptible at this low magnification).
49
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MacroDf - Coating Layer
Micrography of a longitudinal section of the sleeve, at the external surface where there are two layers of coating. The electrolytic etch evidenced the duplex stainless steel substrate (bottom of the figure) and the weave interface of the substrate and the first thermal spray layer, about 1 mm thick, in a stainless steel. The surface layer, of tugnsten carbide, about 0.2 mm thick, is black and not clearly visible in this figure.
50
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - External Surface

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ML00137 — Brittle Fracture of a 15-5 PH Valve SpringM - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Aspect of the fracture of the spring. Close to the surface the fracture presents the aspect of rusted spots.
132
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Aspect Before AnalysisDf - Fracture
The spring ruptured in several positions. This is the aspect of one of the fractures of the spring. In the initiation of the fracture (top side of the figure) the fracture presents a different morphology.
101
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Aspect Before AnalysisDf - Brittle Fracture
Microstructure of the spring in a transverse section, presenting an aged martensitic structure.
96
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Corroded spots (shallow pits) at the spring surface.
84
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Aspect Before AnalysisDf - At the Surface
Corroded spots (shallow pits full of products) at the spring surface.
80
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Corrosion

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ML00125 — Dezincification of a Cooler TubesheetM - BrassP - PlateAp - ShipCd - Preferential Dissolution
Micrography of a transverse section of the platesheet presenting a duplex structure, alpha (light yellow) and beta (orange) phases.
214
VIEW
ML00125 / Mar.2018
Dezincification of a Cooler Tubesheet
M - BrassP - PlateAp - ShipCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Alpha and Beta
Aspect of the tubesheet after removal of the cooper alloy tubes and water cleaning. The corrosion is more intense in the regions of tube connection.
176
VIEW
ML00125 / Mar.2018
Dezincification of a Cooler Tubesheet
M - BrassP - PlateAp - ShipCd - Preferential Dissolution
Cm - Surface AspectDf - Corrosion
Transverse section of the tubesheet, after removal of the tubes. The seawater sie is to the top of the figure. It is possible to see regions of localized corrosion close to the tube position and a red layer all through the plate surface.
182
VIEW
ML00125 / Mar.2018
Dezincification of a Cooler Tubesheet
M - BrassP - PlateAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Corrosion
Macrographic detail of the transverse section of the tubesheet at the cooper alloy tube position, after removal of the 5/8" tube. The red layer at the top of the plate (exposed to the cooling medium - treated seawater) is a region of selective corrosion, dezincification.
169
VIEW
ML00125 / Mar.2018
Dezincification of a Cooler Tubesheet
M - BrassP - PlateAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Corrosion
Macrographic detail of the transverse section of the tubesheet at the cooper alloy tube position, after removal of the 5/8" tube. The "layer" at the top of the plate (exposed to the cooling medium - treated seawater) is a region of selective corrosion, dezincification. It is possible to see that in the right side of the figure, where the cooper tube was positioned, the corrosion damage is deeper.
153
VIEW
ML00125 / Mar.2018
Dezincification of a Cooler Tubesheet
M - BrassP - PlateAp - ShipCd - Preferential Dissolution
Cm - Transverse Section AspectDf - Dezincification

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ML00103 — Brittle Fracture of a Free-Cutting ConnectorM - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Aspect of the external side of the connector, with a longitudinally crack of a brittle aspect. It is a 5/8" connector (15.8 mm).
134
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Aspect of the internal side of the connector. The fracture, in the longitudinal direction, presents a brittle aspect. The thickness of the connector is about 2 mm.
126
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Brittle Fracture
Macroscopic detail of the brittle fracture, in the longitudinal direction.
105
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Brittle Fracture
Micrography of the longitudinal section of the fitiing, in a free-cutting steel. The microstructure is predominantly ferritic and there is a large amount of sulfide inclusions, aligned perpendicular to the forming direction.
97
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of the longitudinal section of the fitiing, in a free-cutting steel. The microstructure is predominantly ferritic, with small perlitic areas and some free cementite at ferritic grain boundaries. There is a large amount of sulfide inclusions, aligned perpendicular to the forming direction.
106
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Non Metallic Inclusions

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