Chemical Industry

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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2" drain line from the main 10" line. The leakage occurred at the margin of the weld, a short time after the introduction of the reinforced ribs to reduce vibration.
641
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Field photoDf - General View
Aspect of the stub end, that is used in combination with a lap joint flange. In this case it was prepared from a seam welded pipe, longitudinal, also with circunferential weld to the stub face (which means it was not flared). The cracking is circunferential in the non painted region, not associated to any welded area.
435
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Aspect as received, side A, of the part removed from the rectangular tube that was manufactured from plates, and originally presented two welded seams (not included in the sample). Close to the edges of the sample, where probably were the corners of the rectangular tube, the degradation is in a highest level. Three samples were analysed, with different thicknesses (indicated in the figure). Side A is the side that was in contact with the reaction (product side).
445
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Aspect Before AnalysisDf - General View
The scanning electron microscopy image of the internal surface of the tube in position 2 shows a localized corrosion region with intergranular morphology, as well a crack from the corroded region.
1237
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
Micrographic detail of the fatigue cracking at the margin of the flange to shell fillet weld.
484
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Fatigue Crack
Region of the leakage close to the welded joint between the pipe and the 90° elbow, in the 1 1/2" nominal diameter piping, SCH 40 (3.7 mm thick). See the schematic drawing in the next figure
966
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Aspect Before AnalysisDf - Leakage
Aspect of the cracking after Dye Check Test (Liquid Penetrant) in the external side of the line that operates at 800°C, insulated, and presented the leakage associated to the longitudinal seam weld of the fitting. The circumferential butt weld of the fitting to a pipe did not fail. See the schematic drawing in the next figure
371
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Aspect by NDTDf - Through Wall Cracking
Internal surface detail of the 3 1/2" pipe, cut in a longitudinal section (transverse to the weld), presenting a localized corrosion at the margin of the welded joint (Keller etched), in the root. The pipeline was assembled with pipes manufactured in two different aluminum alloys, AA 3003 (top of the figure) and AA 6063 (bottom of the figure), and the localized corrosion occurred at the fusion line of the 6063 pipe.
1296
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Surface AspectDf - Welded Joint

More from these cases

ML00179 — Hydrides in Titanium WeldM - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Detail of the through wall cracking that caused the leakage in the 2" pipe. The crack was originated in the fillet weld, from the end of the reinforced rib.
72
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Aspect Before AnalysisDf - Fatigue Crack
Low magnification micrography transverse to the fillet weld in the pipe. The pipe base metal is to the bottom of the figure and the weld metal is to the top. The heat affected zone in the middle, shows a coarse grain size structure.
59
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Welded Joint
Low magnification micrography showing the weld metal, full of pores, indicating that the field welding was not properly shileded.
50
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal
Granular alpha structure of the pipe base metal.
49
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Alpha
Coarse grains in the heat affected zone.
46
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Heat Affected Zone

+22 more from this case →

ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Detail of the external side of the stub end showing that the cracking is circunferential, located in a corroded surface, that corresponds to the confined region under the flange.
85
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Cracking
The stub end was manufactured from a plate and the microstructure in a longitudial section shows a refined granular austenitic structure.
62
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Micrography of a longitudinal section of the stub end showing a refined austenitic structure.
57
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrographic detail of the austenitic structure. Free from grain boundaries carbide precipitation.
53
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Macrographic detail of the longitudinal section of the stub end, showing the external side to the top and the internal side to the bottom. There are multiple cracks starting from the external side.
54
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Longitudinal Section AspectDf - Multiple cracks

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ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Aspect as received, side B, of the same part. Side B is the external side of the rectangular tube, that was in contact with the electric furnace atmosphere. This surface of side B presented less degradation than the internal surface (side A).
88
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Aspect Before AnalysisDf - General View
Transverse section macrography of the plate where the degradation by thinning is worst, close to the original corners of the tube. The thinning is occurrring from the product reaction side (side A to the bottom of the figure). The macrography shows a reduction in the thickness from 2 mm (right side, sample 2) to almost zero (left side, sample 1).
86
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Transverse Section AspectDf - Thinning
Longitudinal section macrography of the plate where the degradation by thinning is reducing the thickness from 6mm to 4mm (sample 3). The thinning is occurrring from the product reaction side (side A to the bottom of the figure).
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Longitudinal Section AspectDf - Thinning
SAMPLE 1 AT THE FRACTURE - Micrography in low magnification where the thickness is reduced to zero (fracture). Side A (process side) to the bottom and side B (furnace environment side) to the top.
85
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Low Mag
SAMPLE 1 AT THE FRACTURE - Micrography at the position where the thickness is reduced to zero. Side A to the bottom. The microstructure is austenite with intergranular and transgranular precipitation. The position of the zero thickness presents aspect of an intergranular fracture, and in side A there are several intergranular cracks from the surface.
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation

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ML00086 — Intergranular Corrosion of Sensitized 304SSM - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in the colder part of the equipment, position 1. The material presented carbide precipitation at grain boundaries (not yet fully surrounding the grains) and at this point the tube presented no internal corrosion.
338
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 2, where the temperature was higher and the carbide precipitation increased during service.
272
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 3, where intergranular and transgranular carbide precipitation occurred during service.
234
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation
The low magnification image of the internal surface of the tube, in position 2, shows several points of localized corrosion, with intergranular morphology.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
Micrography of a longitudinal section of the tube in position 2, presenting thinning by intergranular corrosion at the internal surface.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion

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ML00050 — Fatigue Failure of a 316SS Pressure StabilizerM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Aspect of the equipment presenting a through wall cracking at the margin of the fillet weld.
142
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Aspect Before AnalysisDf - Cracking
Macrography of the welded joint between the flange and the shell, indicating the position where the cracking was detected, at 90°.
116
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Welded Joint
The shell plate micrography showed an austenitic structure.
101
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Austenite
The macrography of a transverse section of the shell to flange weld (Lepto's etch) shows that the cracking occurred through the shell plate thickness, at the margin of the fillet weld.
93
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Transverse Section AspectDf - Cracking
Fracture surface after opening the shell cracking, presenting fatigue striation. The fracture presents also foreign particles.
132
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Striation

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ML00065 — Erosion Corrosion of Monel PipingM - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Schematic drawing presenting the External piping surface
339
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Identification drawingDf - Leakage
Aspect of the piping cut in the longitudinal direction, presenting the leakage region close to the welded joint between the pipe and the 90° elbow. The original SCH 40 (3.7 mm thickness) presents an actual average thickness of 2 mm all through the piping extension, evidencing a general thinning. See the schematic drawing in the next figure.
364
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Aspect Before AnalysisDf - Leakage
Schematic drawing presenting the internal piping surface
234
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Identification drawingDf - Leakage
Detail of the internal piping surface, showing lack of deposits and a shinning surface, suggesting erosive conditions.
226
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Surface AspectDf - Leakage
Macrography of the pipe to fitting welded joint, in a region where the thickness loss is almost uniform. The pipe is in the left of the figure and the elbow is in the right, with a general thinning (average of 2 mm, considering that the original thickness was 3.7 mm), and a slightly more intense thickness loss at the weld metal near the elbow side.
183
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched MacroDf - Welded Joint

+18 more from this case →

ML00061 — Creep in a Seam Weld of a 304H SS FittingM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Schematic drawing presenting the aspect of the cracking after Dye Check Test (Liquid Penetrant) in the external side of the line that operates at 800°C, insulated, and presented the leakage associated to the longitudinal seam weld of the fitting. The circumferential butt weld of the fitting to a pipe did not fail.
62
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Identification drawingDf - Through Wall Cracking
Aspect of the internal side of the fitting, at the longitudinal seam weld, and macrography of a transverse section showing the through wall cracks.
62
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Transverse Section
Through wall cracking in the longitudinal seam weld of the fitting. Several cracks, longitudinal to the weld, were created by the connection of voids in the weld metal, associated to a strong microstructural evolution.
191
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Cracks
Micrography of a longitudinal section of the fitting, at the base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
44
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal
Micrographic detail of the fitting base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
40
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal

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ML00059 — Intergranular Corrosion of Aluminum PipingM - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
The macrography of the welded joint shows the AA 6063 alloy pipe in the right and the AA 3003 pipe in the left, welded in two passes. The root presents small regions of corrosion in the weld metal and a localized corrosion at the fusion line of the 6063 pipe (knife-line attack morphology).
397
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched MacroDf - Localized Corrosion
Micrography of a longitudinal section of the pipe AA 3003. Granular structure that reveals the forming direction and dispersed particles.
229
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Base Metal Left Side
Micrographic detail of a longitudinal section of the pipe AA 3003. Granular structure and dispersed particles.
199
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Base Metal Left Side
Micrography of a longitudinal section of the pipe AA 6063. Granular structure and dispersed particles.
169
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Base Metal Right Side
Micrographic detail of a longitudinal section of the pipe AA 6063. Granular structure and dispersed particles.
138
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched MacroDf - Base Metal Right Side

+12 more from this case →