Chemical Industry

6 cases · 16 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Capture method: Scanning Electron Microscope clear all

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Aspect of the opened crack by scanning electron microscopy, showing the coarser structure in the weld (right side of the figure).
33
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Fractography by SEMDf - Fracture
SAMPLE 1 AT THE FRACTURE - Micrographic detail by scanning electron microscopy, as polished, of the oxides that are penetrating in the grain boundaries. The EDS showed high Molibdenium content in the penetrating oxides. The process uses Mo oxides to make metallic Mo and the high Mo content at the surface could be responsible for reducing the oxidation resistance of the material and intensifying the thinning at the process side (side A).
48
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Micrography by SEMDf - Oxide Layer
The scanning electron microscopy image of the internal surface of the tube in position 2 shows a localized corrosion region with intergranular morphology, as well a crack from the corroded region.
1237
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
Fracture surface after opening the shell cracking, presenting fatigue striation. The fracture presents also foreign particles.
132
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Striation
Aspect of the internal surface of the pipe at the welded region, showing the interface of the thinning area in the weld and the pipe base metal.
128
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Surface Aspect by SEMDf - Localized Thinning
After opening the crack the fracture surface presented different aspects close to the internal surface and through the wall propagation. Intergranular at the surface, showing intergranular SCC mechanism, and transgranular with striation, showing the contribution of pulsing loads.
101
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Fractography by SEMDf - Through Wall Cracking

More from these cases

ML00179 — Hydrides in Titanium WeldM - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
In the region where the fracture started there are brittle aspects resembling a cleavage micromechanism and several secondary cracks, transverse to the fracture surface, as well as propagation by fatigue (striation).
36
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Fractography by SEMDf - Brittle Cracks
Fractography showing brittle secondaryy cracks in the region where the cracking was originated.
34
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Fractography by SEMDf - Secondary Cracks
Fractography showing propagation by fatigue. Striation.
26
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Fractography by SEMDf - Fatigue Striation
ML00086 — Intergranular Corrosion of Sensitized 304SSM - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
The low magnification image of the internal surface of the tube, in position 2, shows several points of localized corrosion, with intergranular morphology.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
ML00005 — Environmental Hydrogen Damage in Ti PipeM - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Region of the localized thinning at the weld metal, in a metallographic section, as polished. In the base metal the hydride layer is continuous and no thinning is evident (left side of the figure) and in the weld metal it is detached and cracked (right side of the figure).
107
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Micrography by SEMDf - Localized Thinning
Hydride layer at the internal surface of the pipe base metal, after Kroll etch.
71
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Micrography by SEMDf - Hydride Formation
Detail of the hydride layer at the internal surface of the pipe base metal, after Kroll etch.
62
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Micrography by SEMDf - Hydride Formation
ML00011 — Intergranular SCC of Pure NickelM - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
After opening the crack the fracture surface presented different aspects close to the surface, initiation mechanism, and through the wall propagation. Detail of the intergranular cracking mechanism close to the internal surface.
98
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Fractography by SEMDf - Intergranular Cracking
After opening the crack the fracture surface presented different aspects close to the internal surface, in the initiation, and through the wall propagation. Detail of the transgranular striation, showing the contribution of pulsing loads.
98
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Fractography by SEMDf - Fatigue Striation
After opening the crack the fracture surface presented different aspects close to the internal surface, in the initiation, and through the wall propagation. Detail of the transgranular striation, showing the contribution of pulsing loads.
82
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Fractography by SEMDf - Fatigue Striation