High Alloy Steel

52 cases · 825 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

High Alloy Steel — sub-branches

Austenitic / Martensitic 1Austenitic Stainless Steel 19Duplex Stainless Steel 1Ferritic Stainless Steel 2Heat Resistant Steel 4High Mn Austenitic Steel 1Lean Duplex Stainless Steel 1Martensitic Stainless Steel 10Nickel Alloy Steel 1Precipitation Hardened Stainless Steel 4Super Duplex Stainless Steel 7Wear Resistant Steel 1

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The carcass was manufactured using niobium stabilized plates, grade AISI 347, with circumferential welds, where the through wall cracks were detected.
300
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Field photoDf - General View
Aged microstructure of the HP stainless steel, modified with 1%Nb, cast fitting, tubular, operating for 6 years in a furnace which design temperature is 1100°C. The material presented a network of primary carbides, white and grey, and an austenitic matrix with coalescing secondary precipitation. Some voids. The Vickers identation indicates a hardness value about 260HV 100g in the aged austenitic matrix.
491
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Microhardness identations
Aspect of the stub end, that is used in combination with a lap joint flange. In this case it was prepared from a seam welded pipe, longitudinal, also with circunferential weld to the stub face (which means it was not flared). The cracking is circunferential in the non painted region, not associated to any welded area.
435
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Aspect of a flared tubing, cold deformed at 37°, and the circumferential cracking.
483
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Aspect Before AnalysisDf - General View
As received aspect of the sacrificial casting, 2" internal diameter. The casting was solution annealed heat treated.
488
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View
Aspect as received, side A, of the part removed from the rectangular tube that was manufactured from plates, and originally presented two welded seams (not included in the sample). Close to the edges of the sample, where probably were the corners of the rectangular tube, the degradation is in a highest level. Three samples were analysed, with different thicknesses (indicated in the figure). Side A is the side that was in contact with the reaction (product side).
445
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Aspect Before AnalysisDf - General View
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
756
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Decorative table service fork, with a non metallic handle that is broken. The metallic part is about 165 mm long and presents two shapes: the scoop and the handle. The scoop is 53mm wide and 73mm long and the handle is about 9 mm wide and 75 mm long.
731
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View

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ML00174 — Carburization of a 347 SS Welded JointM - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
The circumferential welds presented several regions where the multiple cracks appeared, mainly revealed by dye check test.
49
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect by NDTDf - Multiple cracks
Aspect of one region where the cracks appeared, after grinding and polishing. Several branched cracks located in welded regions. It is the region where the sample was taken.
36
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect Before AnalysisDf - At the Surface
The small sample removed for analysis. This wedge sample presents three faces: one polished face (that corresponds to the surface), one fractured face and one cut face.
38
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Testpiece aspectDf - Fracture
The small wedge sample is 4 mm deep in the thickness and the circumferential weld are is about 15 mm width where it appears in the internal side of the carcass. The image shows the crack surface (fracture) where the weld aspect is evident.
32
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect Before AnalysisDf - Fracture
The fracture surface in the sample shows columnar grains in the weld and large facets in the heat affected zone (HAZ) close to the internal surface of the carcass (to the top of the image).
32
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Fractography by SEMDf - Brittle Fracture

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ML00173 — Welding Cracks in an Aged HP Cast FittingM - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Condition of the joint between the centrifugally cast tube (bottom) and the buttered fitting (top). During this welding the cast fitting (buttered) showed several cracks but after removal of the fitting it was clear that the cracks were formed during the buttering and not during the joining.
46
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Aspect Before AnalysisDf - General View
After removal of the cracked part of the fitting, the dye check test indicated the presence of several cracks in the internal diameter (ID), out of the buttered layer, that means, in the fitting base metal.
42
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Aspect by NDTDf - Cracks
Cast fitting microstructure. Network of primary carbides and austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Cast fitting microstructure. The material presented a network of primary carbided and an austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Micrographic detail of the network of primary carbided, white and grey, and an austenitic matrix with coalescing secondary precipitation.
30
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure

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ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Detail of the external side of the stub end showing that the cracking is circunferential, located in a corroded surface, that corresponds to the confined region under the flange.
85
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Cracking
The stub end was manufactured from a plate and the microstructure in a longitudial section shows a refined granular austenitic structure.
62
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Micrography of a longitudinal section of the stub end showing a refined austenitic structure.
57
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrographic detail of the austenitic structure. Free from grain boundaries carbide precipitation.
53
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Macrographic detail of the longitudinal section of the stub end, showing the external side to the top and the internal side to the bottom. There are multiple cracks starting from the external side.
54
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Longitudinal Section AspectDf - Multiple cracks

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ML00167 — Fatigue of a Flared Tubing ConnectionM - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Same flared tubing, with a circumferential crack, with the focus at the internal side.
65
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Aspect Before AnalysisDf - General View
Micrography of a longitudinal section of the tubing showing a granular structure, austenitic.
52
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Micrography of a longitudinal section of the tubing, showing the austenitic structure free from strain hardening and free from grain boundary carbides.
51
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrographic detail of the austenitic structure, free from strain hardening and free from grain boundary carbides.
54
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Low magnification fractography by scanning electron microscopy, after a complete opening of the crack. At this magnification no micromechanism is evident.
51
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fracture

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ML00164 — Austenitic SS Casting for Valve BodyM - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Macrography of a longitudinal section of the valve body, presenting the granular structure. The main bore diameter is 2". The casting was tested in two positions. In radial direction in the center of the body (3" solid), and in the longitudinal direction in the wall (1" thick).
78
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Longitudinal Section
Micrography of a longitudinal section, in the center of the valve body, solid 3" thickness. The structure is austenitic with delta ferrite in interdendritic spaces.
67
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography of a longitudinal section, in the center of the valve body. The structure is austenitic with delta ferrite in interdendritic spaces. The austenite presents a cored matrix in the dendrites, indicating the chemical composition was not homogeneized during the heat treatment.
60
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrographic detail of the cored austenitic structure with delta ferrite in interdendritic spaces. The chemical composition was not homogeneized during the heat treatment.
55
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrography of a longitudinal section, in the 1" thickness valve wall. The structure is austenitic with delta ferrite in interdendritic spaces.
48
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite

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ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Aspect as received, side B, of the same part. Side B is the external side of the rectangular tube, that was in contact with the electric furnace atmosphere. This surface of side B presented less degradation than the internal surface (side A).
88
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Aspect Before AnalysisDf - General View
Transverse section macrography of the plate where the degradation by thinning is worst, close to the original corners of the tube. The thinning is occurrring from the product reaction side (side A to the bottom of the figure). The macrography shows a reduction in the thickness from 2 mm (right side, sample 2) to almost zero (left side, sample 1).
86
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Transverse Section AspectDf - Thinning
Longitudinal section macrography of the plate where the degradation by thinning is reducing the thickness from 6mm to 4mm (sample 3). The thinning is occurrring from the product reaction side (side A to the bottom of the figure).
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Longitudinal Section AspectDf - Thinning
SAMPLE 1 AT THE FRACTURE - Micrography in low magnification where the thickness is reduced to zero (fracture). Side A (process side) to the bottom and side B (furnace environment side) to the top.
85
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Low Mag
SAMPLE 1 AT THE FRACTURE - Micrography at the position where the thickness is reduced to zero. Side A to the bottom. The microstructure is austenite with intergranular and transgranular precipitation. The position of the zero thickness presents aspect of an intergranular fracture, and in side A there are several intergranular cracks from the surface.
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation

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ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Aspect of a 5/16" bolt manufactured in an AISI 316 austenitic stainless steel, that was also operating inside the pressure vessel, but was not yet damaged. It is a hexagonal head bolt, 1 1/2" long, fastened with a hexagonal nut and a lock washer.
118
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Low magnification micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides.
100
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides, strain hardened. The hardness values of the material are from 200HV1 to 300HV1, that meets the class 2 of strenght (ASTM A193 B8M class 2).
79
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Strain Hardened
Detail of the strain hardened austenitic microstructure. Micrography by optical microscope, of the longitudinal section of a bolt, in the center of the thickness.
76
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Strain Hardened
Aspect of a broken 5/16" bolt that was operating inside the pressure vessel in a condition that exceeds the limits of use of the AISI 316 steel. The fracture is located close to the position where there was the bolt head and the threads were "removed" close to the fracture surface.
75
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Fracture

+8 more from this case →

ML00151 — Ferritic Stainless Steel of a Flatware ForkM - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
The metallic part of the fork handle is about 9mm wide. It was cut in a transverse section and the profile is shown in this figure. The thickness is 1mm and the curvature depth is about 3mm.
85
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Transverse Section AspectDf - Formed Profile
Micrography of the fork handle in the transverse section, curved, presenting differences between grain size and morphology. In the middle section there are elongated grains and close to the surfaces there are smaller and more equiaxed grains.
81
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Transverse Section
Micrography of the fork handle in the center of the transverse section, curved, presenting larger ferritic grains with elongated morphology.
70
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Granular structure
Micrographic detail of the ferritic grains with elongated morphology in the center of the transverse section, curved.
58
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Ferrite
Lateral view of the fork showing the profile. The scoop convex depth is 10 mm and the handle concave depth is 3 mm. The overal thickness of the part is 1 mm.
53
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View

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