High Alloy Steel

26 cases · 378 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Aged microstructure of the HP stainless steel, modified with 1%Nb, cast fitting, tubular, operating for 6 years in a furnace which design temperature is 1100°C.  The material presented a network of primary carbides, white and grey, and an austenitic matrix with coalescing secondary precipitation. Some voids. The Vickers identation indicates a hardness value about 260HV 100g in the aged austenitic matrix.
491
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Microhardness identations
As received aspect of the sacrificial casting, 2" internal diameter.  The casting was solution annealed heat treated.
488
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View
Optical micrography of a longitudinal section of the fractured bolt, at the thread.  The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
756
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Vertical piping in a corrosive oil producing system of a FPSO.  The line is a nominal diameter 14" sch 10S (pipe thickness about 5 mm) and the flanged branch line is a 2" nominal diameter welded to the main pipe using a weldolet (forged fitting). The fatigue induced cracking occurred longitudinal to the main pipe, originated at the margem of the weld interface with the pipe.
1480
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Aspect Before AnalysisDf - General View
Aspect of the barrel nut that is broken in a brittle way (without plastic deformation).  The Nut diameter is 1", the nut length is 2" and the bolt thread is 1/2" (nominal diameter).
753
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Aspect Before AnalysisDf - General View
Aspect of the male part of the coupling, a pin, presenting the thermal spray layer detachment (right side of the figure). The pin was manufactured in a superduplex stainless steel tubular forging; the external surface was partially coated by thermal spray and machined.  The sealing is only elastomeric but a coating is required to avoid galling between the two materials of the coupling.
1154
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - Aspect Before AnalysisDf - Layer Detachment
Aspect of the cracked valve body, after disassembling and removing the internal parts.  The valve is part of a lot that was manufactured by forging a cubic 170mm from a  forged bar in SDSS UNS S32760, and heat treated (solution annealed) by the forging company. The fabrication using these bodies included the machining, fillet weld two inserts in Alloy 625, machining again, assembling the internals, and pressure test at 15,000 psi.  The cracking occurred during test, only for this valve body.
676
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Cracking
Fractographic detail of the longitudinal Charpy V testpiece,  broken at -46°C and presenting energy of 64J (the average energy of three tespieces was 70J).  The Charpy V testpiece was removed from the center of the bar. The micromechanism is quasicleavage and the test in this direction presented energy values superior than the minimum requirement of 45J.
944
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece

More from these cases

ML00173 — Welding Cracks in an Aged HP Cast FittingM - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Aspect Before AnalysisDf - General View
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Aspect by NDTDf - Cracks
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure

+13 more from this case →

ML00164 — Austenitic SS Casting for Valve BodyM - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Longitudinal Section
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite

+2 more from this case →

ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Aspect of a 5/16" bolt manufactured in an AISI 316 austenitic stainless steel, that was also operating inside the pressure vessel, but was not yet damaged.  It is a hexagonal head bolt, 1 1/2" long, fastened with a hexagonal nut and a lock washer.
118
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Low magnification micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides.
100
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Strain Hardened
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Strain Hardened
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Fracture

+8 more from this case →

ML00150 — Vibration Induced Fatigue in a SS Oil PipingM - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Macrography of the section transverse to the ND 14" main pipe (that is only 5mm thick) and to the ND 2" branch that is a weldolet fitting welded to the main pipe and flange. This image is interesting because it shows clearly how thin is the pipe compared with the fitting thickness and the large amount of welding required to assure a full penetration weld in the weldolet.
220
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MacroDf - Transverse Section
Transverse section of the 14" pipe in the center of the 2" branch using a weldolet fitting welded to the main pipe.  The internal side of the pipe is to the top of the figure and the through wall fatigue cracking is located at the margem of the weld.  It is possible to see that it is a full penetration weld and the fitting thickness is several times larger than the pipe thickness.
174
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Electrolytically Etched MacroDf - Crack
Detail of the fatigue cracking, staring from the margin of the weld. The crack propagated though wall of the pipe (5 mm).  The larger thickness of the weldolet requires a large amount of deposited weld metal, about 20 mm that is 4 times the pipe thickness. It is an interesting aspect to be considered by designers.
176
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Electrolytically Etched MacroDf - Fatigue Crack
After cutting the pipe and opening the crack, the fracture appearance shows a clean fracture, flat, starting from the margem of the weld of the pipe (right side of the figure), and propagating through wall into the pipe (aproximately 5 mm thickness). The external side of the pipe is to the right side of the figure (presenting the weld finishing) and the internal side of the pipe is to the left side of the figure.
176
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Fracture Surface AspectDf - Fracture
The same fracture appearance of the previous figure, looking at a higher magnification by scanning electron microscopy.  The fracture is clean, flat, starting in the right side of the figure, at the margem of the weld and propagating into the pipe thickness. The external side of the pipe is to the right side of the figure and the internal side of the pipe is to the left side of the figure.
154
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fracture

+29 more from this case →

ML00148 — Brittle Fracture of a 420 SS Barrel NutM - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Aspect Before AnalysisDf - Fracture
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Fracture Surface AspectDf - Chevron Marks
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure

+15 more from this case →

ML00146 — Plastic Deformation of a SDSS Riser PinM - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
The longitudinal section of the pin shows that it was deformed in a localized position, where the layer was detached, top side of the figure. The pin wall was plastically deformed decreasing the internal diameter.
222
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - Longitudinal Section AspectDf - Plastic Deformation
Micrography of the longitudinal section, in the center of the thickness of the pin, presenting an aligned ferritic-austeinitic structure.
180
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrography of a longitudinal section, at the surface of the pin, where the thermal spray layer is sound. The thickness of the layer is about 0.3 mm.
168
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - NaOH Electrolytic Etched MicroDf - Coating Layer
Micrographic detail of a longitudinal section of the pin, at the surface, evidencing the thermal spray layer, about 0.3 mm.  The layer presents typical characteristics of multiple layers, low amount of entrapped oxides and pores.  The interface presents a high roughness level for a good adherence and some entrapped oxides. The structure of the SDSS substrate did not show thermal effects.
154
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - NaOH Electrolytic Etched MicroDf - Coating Layer
The longitudinal section of the pin at the region of the thermal spray layer detachment, showing that the pin suffered a localized lateral bending with strong plastic deformation, responsible for the layer detachment.  The figure shows the external surface (top of the figure) with the layer detachment (gray aspect), the thickness of the pin (deformed) and the internal surface (bright aspect).
124
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - Longitudinal Section AspectDf - Plastic Deformation

+2 more from this case →

ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Detailed aspect of the cracking, straight and presenting a brittle aspect.
122
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Cracking
Detail of the internal bore, showing a brittle crack through the wall.
106
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Cracking
Aspect of a section cut transverse to the center of the body.  The crack is brittle, trough wall, and was arrested in the region where the valve body was welded to the insert.
105
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Transverse Section AspectDf - Cracking
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred.  The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
106
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrographic detail of the valve body structure, close to the position where the cracking has occurred.  The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
102
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma

+25 more from this case →

ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Fractography of the broken Charpy V testpiece,  longitudinal, broken at -46°C and presenting energy of 64J (the average of three values was 70J).  In this direction the material presented an energy value higher than the minimum requirement of 45J.
109
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
Fractography of the Charpy V testpiece, transverse section, broken at -46°C and presenting energy of 20J (the average of three results was 33J).  The coarse structure and the alignement created a condition for low energy results in this specific direction, and the material did not present the minimum requirement of 45J.
103
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section

+3 more from this case →