High Alloy Steel

40 cases · 317 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Detail focus: Damage clear all

High Alloy Steel — sub-branches

Austenitic / Martensitic 1Austenitic Stainless Steel 19Duplex Stainless Steel 1Ferritic Stainless Steel 2Heat Resistant Steel 4High Mn Austenitic Steel 1Lean Duplex Stainless Steel 1Martensitic Stainless Steel 10Nickel Alloy Steel 1Precipitation Hardened Stainless Steel 4Super Duplex Stainless Steel 7Wear Resistant Steel 1

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The circumferential welds presented several regions where the multiple cracks appeared, mainly revealed by dye check test.
49
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect by NDTDf - Multiple cracks
After removal of the cracked part of the fitting, the dye check test indicated the presence of several cracks in the internal diameter (ID), out of the buttered layer, that means, in the fitting base metal.
42
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Aspect by NDTDf - Cracks
Detail of the external side of the stub end showing that the cracking is circunferential, located in a corroded surface, that corresponds to the confined region under the flange.
85
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Cracking
Low magnification fractography by scanning electron microscopy, after a complete opening of the crack. At this magnification no micromechanism is evident.
51
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fracture
Transverse section macrography of the plate where the degradation by thinning is worst, close to the original corners of the tube. The thinning is occurrring from the product reaction side (side A to the bottom of the figure). The macrography shows a reduction in the thickness from 2 mm (right side, sample 2) to almost zero (left side, sample 1).
86
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Transverse Section AspectDf - Thinning
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
757
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Micrography of the longitudinal section from the fork tooth in the scoop. The microstructure is the same as in the scoop close to the handle, ferritic grains equiaxial and uniform, but at the cut surface the structure presents strong plastic deformation generated by a mechanical cutting.
36
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Plastic Deformation
Transverse section of the 14" pipe in the center of the 2" branch using a weldolet fitting welded to the main pipe. The internal side of the pipe is to the top of the figure and the through wall fatigue cracking is located at the margem of the weld. It is possible to see that it is a full penetration weld and the fitting thickness is several times larger than the pipe thickness.
174
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Electrolytically Etched MacroDf - Crack

More from these cases

ML00174 — Carburization of a 347 SS Welded JointM - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
The small sample removed for analysis. This wedge sample presents three faces: one polished face (that corresponds to the surface), one fractured face and one cut face.
38
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Testpiece aspectDf - Fracture
The small wedge sample is 4 mm deep in the thickness and the circumferential weld are is about 15 mm width where it appears in the internal side of the carcass. The image shows the crack surface (fracture) where the weld aspect is evident.
32
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect Before AnalysisDf - Fracture
The fracture surface in the sample shows columnar grains in the weld and large facets in the heat affected zone (HAZ) close to the internal surface of the carcass (to the top of the image).
32
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Fractography by SEMDf - Brittle Fracture
Detail of the fracture in the heat affected zone, showing a flat fracture where the fracture is close to the surface of the plate, exposed to the high temperature exhausting gases.
24
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Fractography by SEMDf - Brittle Fracture
Detailed microstructure of the plate base metal, exposed to high temperature exhausting gases. Refined austenite, precipitation of carbides in the grain boumdaries and some cracks.
24
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Oxalic Acid Electrolytic EtchDf - Crack

+2 more from this case →

ML00173 — Welding Cracks in an Aged HP Cast FittingM - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cast fitting microstructure. The material presented a network of primary carbided and an austenitic matrix with coalescing secondary precipitation.
38
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Micrographic detail of the network of primary carbided, white and grey, and an austenitic matrix with coalescing secondary precipitation.
30
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Macrographic detail close to the internal diameter (ID in the bottom), where the cracks were detected by dye check (after removal of the damaged part of the cast fitting). Close to the surface it is possible to see the layers of the weld metal that corresponds to the cast fitting buttering.
21
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched MacroDf - Cracks
Micrographic detail of the cracks at the fusion line, associated to the partially melted region suggesting a liquation effect in a material that presented low ductility. After opening the cracks they propagate brittle into the base metal and created a solidification cracking in the weld metal, detailed in the next figures.
23
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Multiple cracks
Micrographic detail of the cracks in the base metal created from the partially melted region suggesting that a liquation effect propagated brittle cracks into the low ductility base metal.
30
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Cracks

+1 more from this case →

ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Macrographic detail of the longitudinal section of the stub end, showing the external side to the top and the internal side to the bottom. There are multiple cracks starting from the external side.
54
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Longitudinal Section AspectDf - Multiple cracks
Micrography of the stub end longitudinal section, presenting multiple cracks, branched.
40
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - As polished micrographyDf - Multiple cracks
Micrography of the stub end longitudinal section, showing multiple branched transgranular cracks.
25
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transgranular Cracking
Micrography of the stub end longitudinal section, showing multiple branched transgranular cracks, typical of a Chloride Stress Corrosion Cracking mechanism.
34
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Corrosion Cracking
Micrographic details of the Chloride Stress Corrosion Cracks, transgranular and branched.
34
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Corrosion Cracking

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ML00167 — Fatigue of a Flared Tubing ConnectionM - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Flat aspect of the fracture. The striation micromechanism is revealed.
50
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
The thin striation is evident in the fracture surface, suggesting a high cycle fatigue, typically identified in vibration conditions.
45
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Striation
Detail of the striation micromechanism.
48
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Striation
When the fracture propagates, the striation becomes wider and with transgranular irregular steps.
47
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
Micrography of a longitudinal section of the flared tubing where the fracture occurred. The starting point of the fracture is associated to the external side of the tubing, where it was connected by a nut and there was a localized plastic deformation due to the fitting assembly.
33
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Transgranular Fracture

+1 more from this case →

ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Longitudinal section macrography of the plate where the degradation by thinning is reducing the thickness from 6mm to 4mm (sample 3). The thinning is occurrring from the product reaction side (side A to the bottom of the figure).
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Longitudinal Section AspectDf - Thinning
SAMPLE 1 AT THE FRACTURE - Micrographic detail of the intergranular fracture. The austenitic grains of the material are loosing.
80
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Intergranular Fracture
SAMPLE 1, AT THE FRACTURE - Micrography, as polished, of the oxides at the fracture (zero thickness). In this region the oxide layer penetrated through thickness, intergranular, and fractured the material.
63
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - As polished micrographyDf - Intergranular Fracture
SAMPLE 1, AT THE FRACTURE - Micrographic detail, as polished, of the oxides that are penetrating in the austenitic grain boundaries. The oxidation created intergranular cracks in regions close to the edge of the rectangular tube, that are more susceptible to suffer cyclic thermal stresses, since the furnace is weekly turned off, during two days.
55
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - As polished micrographyDf - Intergranular Cracking
SAMPLE 1 AT THE FRACTURE - Micrographic detail by scanning electron microscopy, as polished, of the oxides that are penetrating in the grain boundaries. The EDS showed high Molibdenium content in the penetrating oxides. The process uses Mo oxides to make metallic Mo and the high Mo content at the surface could be responsible for reducing the oxidation resistance of the material and intensifying the thinning at the process side (side A).
48
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Micrography by SEMDf - Oxide Layer
ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Aspect of a broken 5/16" bolt that was operating inside the pressure vessel in a condition that exceeds the limits of use of the AISI 316 steel. The fracture is located close to the position where there was the bolt head and the threads were "removed" close to the fracture surface.
75
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Fracture
Low magnification SEM image showing the brittle aspect of the cracks in the bolt thread.
61
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Brittle Cracks
Detail of the bolt thread in a SEM image, showing parts of the thread removed in a brittle way.
62
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Brittle Fracture
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were fully cracked by the stress corrosion mechanism.
58
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Optical micrography of a longitudinal section of the fractured bolt, under the thread, showing stress corrosion cracks through the section.
46
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks

+2 more from this case →

ML00151 — Ferritic Stainless Steel of a Flatware ForkM - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Micrographic detail of the strong plastic deformation at the edge of the scoop in the tooth cutting location. The hardness at this region of strong plastc deformation is about 240HV1.
38
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Plastic Deformation
ML00150 — Vibration Induced Fatigue in a SS Oil PipingM - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Detail of the fatigue cracking, staring from the margin of the weld. The crack propagated though wall of the pipe (5 mm). The larger thickness of the weldolet requires a large amount of deposited weld metal, about 20 mm that is 4 times the pipe thickness. It is an interesting aspect to be considered by designers.
176
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Electrolytically Etched MacroDf - Fatigue Crack
After cutting the pipe and opening the crack, the fracture appearance shows a clean fracture, flat, starting from the margem of the weld of the pipe (right side of the figure), and propagating through wall into the pipe (aproximately 5 mm thickness). The external side of the pipe is to the right side of the figure (presenting the weld finishing) and the internal side of the pipe is to the left side of the figure.
176
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Fracture Surface AspectDf - Fracture
The same fracture appearance of the previous figure, looking at a higher magnification by scanning electron microscopy. The fracture is clean, flat, starting in the right side of the figure, at the margem of the weld and propagating into the pipe thickness. The external side of the pipe is to the right side of the figure and the internal side of the pipe is to the left side of the figure.
154
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fracture
Fracture apperance by scanning electron microscopy of the region where the fatigue crack started, from the piping outside . The fracture is flat, presents some smashed regions close to the surface (to the right side) and there are some thin secondary cracks.
140
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
Fracture detail by scanning electron microscopy of the region where the cracking started, from the piping outside . The fracture is flat and shows fatigue striation.
138
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fatigue Striation

+6 more from this case →