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Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Austenite clear all

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Typical manufacturing 7Welding 3

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As received aspect of the sacrificial casting, 2" internal diameter. The casting was solution annealed heat treated.
488
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View
Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a longitudinal seam welded pipe, with substrate in low alloy steel X65 and clad plate in Alloy 625 (welded by a solid state process). The region is a detail in the side of the Ni alloy clad plate where a grain refinement has occurred probably due to recrystallization of a strain hardened region during later heat treatment. The microhardness of this region is a lot higher than the value obtained out of this region, in the clad plate.
904
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface
Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a seamless pipe in a low alloy steel X70 cladded by welding overlay of Alloy 625 (by automatic GTAW process). The region is a detail of the interface inside the Ni alloy weld metal, presenting columnar grains and intragranular preciptation. The pipe was heat treated before bending (solution annealing) and after bending (quenching and tempering to meet X70 grade). The microhardness of this region is higher than the value obtained out of this region, in the overlay.
656
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface
Micrographic detail of a longitudinal section in the center of the bolt. Granular austenitic microstructure, equiaxial, primary precipitates (isolated), precipitation hardened (not detectable by metalography, only because of the hardness level)
431
VIEW
ML00106 / Dec.2017
Inconel 718 Submarine Bolt
M - NiCrFe AlloyP - BoltAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
Aspect of the bolt with a special head, to be adopted in subsea condition. M12, 1/2" 13UNC.
342
VIEW
ML00105 / Jun.2018
Inconel 718 Bolt of Special Head
M - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View
Micrographic detail of the strain hardened austenitic structure in the longitudinal section of the bolt.
441
VIEW
ML00101 / Nov.2017
High Strength 316SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrographic detail of the strain hardened austenitic structure in the longitudinal section of the bolt.
412
VIEW
ML00087 / Nov.2017
High Strength Austenitic SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrographic detail of the austenitic structure at the surface, where the grain size of the material increased. By optical microscopy the intragranular precipitation due to solution annealing and aging is not revealed.
794
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite

More from these cases

ML00164 — Austenitic SS Casting for Valve BodyM - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Macrography of a longitudinal section of the valve body, presenting the granular structure. The main bore diameter is 2". The casting was tested in two positions. In radial direction in the center of the body (3" solid), and in the longitudinal direction in the wall (1" thick).
78
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Longitudinal Section
Micrography of a longitudinal section, in the center of the valve body, solid 3" thickness. The structure is austenitic with delta ferrite in interdendritic spaces.
67
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography of a longitudinal section, in the center of the valve body. The structure is austenitic with delta ferrite in interdendritic spaces. The austenite presents a cored matrix in the dendrites, indicating the chemical composition was not homogeneized during the heat treatment.
60
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrographic detail of the cored austenitic structure with delta ferrite in interdendritic spaces. The chemical composition was not homogeneized during the heat treatment.
55
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrography of a longitudinal section, in the 1" thickness valve wall. The structure is austenitic with delta ferrite in interdendritic spaces.
48
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite

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ML00133 — Seam Welded Pipe Cladded with Alloy 625M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
The 6 1/2" nominal diameter longitudinal seam welded pipe is internally cladded with Alloy 625. The pipe was manufactured by forming a cladded plate (probably welded by rolling) and welding it longitudinally. The pipe was heat treated (quenched and tempered) after the seam weld.
96
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Aspect Before AnalysisDf - Welded Joint
The macrography of a longitudinal section shows the low alloy (C-Mn) steel pipe, internally cladded with Ni alloy clad plate.
72
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Electrolytically Etched MacroDf - Longitudinal Section
Micrography of a longitudinal section of the pipe substrate, in low magnification, showing a uniform microstructure,
51
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure obtained by the pipe quenching and tempering,
48
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure,
50
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Bainite

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ML00132 — Seamless Pipe Overlaid with Alloy 625M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
The 4 1/2" nominal diameter seamless pipe internally overlaid with Alloy 625. This pipe corresponds to a 90° curve. The overlaid pipe was heat treated before and after bending. The final quenching and tempering heat treatment was conducted to meet API 5L X70 properties.
113
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Aspect Before AnalysisDf - Welded Joint
The macrography of a longitudinal section shows the low alloy (C-Mn) steel pipe, internally cladded by overlay in two layers.
88
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytically Etched MacroDf - Longitudinal Section
Micrography of a longitudinal section of the pipe substrate, in low magnification, showing a uniform microstructure,
79
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure obtained by the pipe quenching and tempering,
72
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure.
68
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Bainite

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ML00106 — Inconel 718 Submarine BoltM - NiCrFe AlloyP - BoltAp - SubseaCd - Typical manufacturing
Micrography of a longitudinal section in the center of the bolt. Granular austenitic microstructure, equiaxial, primary precipitates (isolated), precipitation hardened (not detectable by metalography, only because of the hardness level)
63
VIEW
ML00106 / Dec.2017
Inconel 718 Submarine Bolt
M - NiCrFe AlloyP - BoltAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Aspect of the bolt analyzed to qualify the lot of fasteners to be adopted in subsea conditions, exposed to cathodic protection.
62
VIEW
ML00106 / Dec.2017
Inconel 718 Submarine Bolt
M - NiCrFe AlloyP - BoltAp - SubseaCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View
Low magnification micrography of the bolt in a longitudinal section, at the bolt thread, showing no evidences of forming operations, indicating that it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial.
54
VIEW
ML00106 / Dec.2017
Inconel 718 Submarine Bolt
M - NiCrFe AlloyP - BoltAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of the bolt in a longitudinal section, at the bolt thread, showing no evidences of forming operations, indicating that it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial.
49
VIEW
ML00106 / Dec.2017
Inconel 718 Submarine Bolt
M - NiCrFe AlloyP - BoltAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
ML00105 — Inconel 718 Bolt of Special HeadM - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Low magnification micrography of the bolt in a longitudinal section, at the bolt thread, showing no evidences of forming operations, indicating it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial, precipitation hardened (shadow in the grains).
45
VIEW
ML00105 / Jun.2018
Inconel 718 Bolt of Special Head
M - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of the bolt in a longitudinal section, at the bolt thread, showing no evidences of forming operations, indicating it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial, precipitation hardened (shadow in the grains).
39
VIEW
ML00105 / Jun.2018
Inconel 718 Bolt of Special Head
M - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
Micrographic detail of the bolt in a longitudinal section, at the bolt thread, showing no evidences of forming operations, indicating it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial, precipitation hardened (shadow in the grains).
31
VIEW
ML00105 / Jun.2018
Inconel 718 Bolt of Special Head
M - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
Low magnification micrography of the bolt in a longitudinal section, at the bolt head, showing no evidences of forming operations, indicating it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial, precipitation hardened (shadow in the grains).
31
VIEW
ML00105 / Jun.2018
Inconel 718 Bolt of Special Head
M - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of the bolt in a longitudinal section, at the bolt head, showing no evidences of forming operations, indicating it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial, precipitation hardened (shadow in the grains).
31
VIEW
ML00105 / Jun.2018
Inconel 718 Bolt of Special Head
M - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite

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ML00101 — High Strength 316SS BoltM - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Micrography of the longitudinal section of the bolt, in the center of the body thickness. Strain hardened austenic structure.
52
VIEW
ML00101 / Nov.2017
High Strength 316SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Micrography of the longitudinal section of the bolt, in the center of the body thickness. Strain hardened austenic structure.
46
VIEW
ML00101 / Nov.2017
High Strength 316SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Aspect of the bolts M12 x 25.
41
VIEW
ML00101 / Nov.2017
High Strength 316SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View
Micrography of the longitudinal section of the bolt, at the thread. The bolt was cold deformed and the thread was cold rolled.
32
VIEW
ML00101 / Nov.2017
High Strength 316SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Micrography of the longitudinal section of the bolt, at the thread. The bolt was cold deformed and the thread was cold rolled.
31
VIEW
ML00101 / Nov.2017
High Strength 316SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Strain Hardened

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ML00087 — High Strength Austenitic SS BoltM - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Micrography of the longitudinal section of the bolt, in the center of the body thickness. Strain hardened austenic structure.
73
VIEW
ML00087 / Nov.2017
High Strength Austenitic SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Micrography of the longitudinal section of the bolt, in the center of the body thickness. Strain hardened austenic structure.
62
VIEW
ML00087 / Nov.2017
High Strength Austenitic SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Socket head capscrew bolt, M10 x 70, 1.5 coarse thread.
63
VIEW
ML00087 / Nov.2017
High Strength Austenitic SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View
Micrography of the longitudinal section of the bolt, at the thread. The bolt was cold deformed and the thread was cold rolled.
65
VIEW
ML00087 / Nov.2017
High Strength Austenitic SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Micrography of the longitudinal section of the bolt, at the thread. The bolt was cold deformed and the thread was cold rolled.
65
VIEW
ML00087 / Nov.2017
High Strength Austenitic SS Bolt
M - Austenitic Stainless SteelP - BoltAp - SubseaCd - Typical manufacturing
Cm - Micrography by OM using A262 Method ADf - Strain Hardened

+1 more from this case →

ML00089 — Inconel 718 Allen Bolt for Subsea ApplicationM - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
The macrography shows the longitudinal section of the allen bolt, 1/2" nominal diameter, that was machined from a heat treated bar (solution annealed and aged). The granular structure presents differences in the grain sizes. At the bolt head (external surface of the original bar) the austenitic grain size is larger than in the center of the bar where the particles in segregated bands "arrested" the grains during hot forming and solution annealing.
58
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched MacroDf - Machined Thread
The micrography of a longitudinal section of the bolt close to the surface, at the thread, shows that it was machined from a bar, not rolled.
37
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
The micrography of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"), shows an equiaxial granular structure. Although the material was hardened by heat treatment (solution annealing and aging), the microstructure at this magnification does not reveal the intragranular precipitation.
34
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Micrographic detail of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"). Although the material was hardened by heat treatment (solution annealing and aging), the microstructure observed by optical microscopy does not reveal the intragranular precipitation.
33
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched MacroDf - Austenite
The micrography of a longitudinal section, at the bolt head close to the surface of the original bar. In this region the material increased the grain size due to the lack of particles (inclusions), to "arrest" the grain boundaries (during hot forming and solution annealing). The smaller grain size is located in the center of the bar, that concentrated the inclusions.
30
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched MacroDf - Dual grain sizes

+1 more from this case →