Optical Microscope

77 cases · 649 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Optical Microscope — sub-branches

As polished micrography 43Eletrolytically Etched Micrography by OM 6Glyceregia Etched Micrography by OM 6Kalling Etched Micrography by OM 64Micrography by OM 26Micrography by OM using A262 Method A 58NaOH Electrolytic Etched Micro 52Nital Etched Micrography by OM 381Oxalic Acid Electrolytic Etch 13

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Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in the colder part of the equipment, position 1. The material presented carbide precipitation at grain boundaries (not yet fully surrounding the grains) and at this point the tube presented no internal corrosion.
338
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrography of the tool steel, in the longitudinal section of the part. The material presented a uniform structure, tempered martensite. The tempering was in low temperature since the hardness is high (58 HRc at the surface).
87
VIEW
ML00084 / Mar.2020
Walrus Tool Steel
M - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Uniform Structure
Micrographic detail of the forging lap defect that appears at the nut surface like a crack, filled with oxides. The nut presented a martensitic structure in the center of the nut, but in the regions adjacent to the defect the structure is ferritic-bainitic due to decarburization. There are several globular oxides (grey spots) that became entrapped during the forging.
654
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Crack
Micrography of a transverse section of the lifting part, showing interdendritic voids close to the surface at the inner diameter of the padeye. The microstructure is tempered martensite.
450
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Casting defects
Micrography of the new tube close to a region of a casting defect (shrinkage), presenting only austenitic structure with a network of primary precipitates.
351
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides
Micrographic detail of a transverse section of the rail, in the head, showing a fully perlitic structure.
520
VIEW
ML00096 / Oct.2017
Carbon Steel Tee Rail
M - High Strength Low AlloyP - RailAp - TransportationCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Pearlite
Micrographic detail of the slightly banded perlitic structure, in the center of the thickness. ND 3". 7.6 mm thick.
530
VIEW
ML00090 / Sep.2017
Carbon Steel Tubing for Structural Application
M - Low Carbon SteelP - TubeAp - StructureCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
The micrographic aspect of the cracks in a section transverse to the weld (the removed sample), shows that there are cracks with different sizes, the larger are filled with products that indicate they were opened for longer times.
67
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking

More from these cases

ML00086 — Intergranular Corrosion of Sensitized 304SSM - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 2, where the temperature was higher and the carbide precipitation increased during service.
272
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 3, where intergranular and transgranular carbide precipitation occurred during service.
234
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation
Micrography of a longitudinal section of the tube in position 2, presenting thinning by intergranular corrosion at the internal surface.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion
Micrographic detail of the intergranular corrosion at the internal surface of the tube in position 2. Several grains were already removed by the corrosion.
171
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion
Micrography of a longitudinal section of the tube in position 3, at the internal surface. Although there is a strong precipitation, both intergranular and transgranular, the tube did not corrode at this point.
144
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation

+1 more from this case →

ML00084 — Walrus Tool SteelM - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Micrographic detail of the tool steel, in the longitudinal section of the part. The material presented a uniform structure, tempered martensite, with small secondary carbides. The hardness in the section is 59 HRc.
73
VIEW
ML00084 / Mar.2020
Walrus Tool Steel
M - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Martensite
ML00099 — Forging Defect in a Cadmium Plated NutM - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Micrography of the nut in a section transverse to the surface indication. There are several microcracks (parallel and perpendicular to the nut surface) filled with oxides. The nut presented a martensitic microstructure in the center of the thickness and a ferritic-bainitic microstructure at surface and adjacent to the defect, due to decarburization occurred during high temperature forging.
130
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Crack
Micrographic detail of the lap at the nut surface, as polished. The 20 microns cadmium layer is evident, penetrating in the lap.
46
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - As polished micrographyDf - Lap
Tempered martensitic microstructure in the transverse section of the nut, in the center. The material presented 29 HRc that is typical of a quenched and tempered steel.
30
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Ferritic-bainitic microstructure in the transverse section of the nut, at the surface where the cadmium plate is also evident. The nut surface presents a decarburized layer and the lap entrapped oxides.
30
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Bainitic Ferrite
ML00098 — Brittle Fracture of a Casting Lifting DeviceM - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Micrography of the lifting padeye showing a dendritic path of a quenched and tempered martensitic microstructure. The segregated regions (white interdendritic regions) are more clearly identified in low magnification. Voids are located in these segregated regions.
21
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. Voids are located in interdendritic segregated regions.
20
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. Voids are located in interdendritic segregated regions. At this magnification the segregation is not clear.
16
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. The hardness level of the material is about 39 HRc.
14
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the secondary crack, paralel to fracture, starting from the internal diameter of the padeye. The crack propagates in an interdendritic morphology, interconnecting casting defects.
13
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Secondary Cracks

+8 more from this case →

ML00097 — Cast SS Tube Removed From High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Micrography close to the external surface of a new tube, sound.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the External Surface
Micrography close to the internal surface of a new tube, presenting casting defects.
47
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography of the tube removed from service after 6 month, close to a region of a casting defect (shrinkage), presenting austenitic structure with a network of primary precipitates (initial stage of coarsening) and intragranular secondary precipitation.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation
Micrography close to the internal surface of the tube removed from service after 6 month, presenting high temperature oxidation and shrinkage voids (casting defects).
31
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography close to the external surface of the tube removed from service, damaged by high temperature oxidation.
25
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the External Surface
ML00096 — Carbon Steel Tee RailM - High Strength Low AlloyP - RailAp - TransportationCd - Typical manufacturing
Micrographic detail of a transverse section of the rail, in the head, showing a fully perlitic structure.
57
VIEW
ML00096 / Oct.2017
Carbon Steel Tee Rail
M - High Strength Low AlloyP - RailAp - TransportationCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Perlite
Micrography of a transverse section of the rail, in the head, showing equiaxial grains. Perlitic microstructure.
54
VIEW
ML00096 / Oct.2017
Carbon Steel Tee Rail
M - High Strength Low AlloyP - RailAp - TransportationCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Transverse Section
ML00090 — Carbon Steel Tubing for Structural ApplicationM - Low Carbon SteelP - TubeAp - StructureCd - Typical manufacturing
Micrography of a longitudinal section of the tube, in the center of the thickness. ND 3". 7.6 mm thick.
55
VIEW
ML00090 / Sep.2017
Carbon Steel Tubing for Structural Application
M - Low Carbon SteelP - TubeAp - StructureCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of a longitudinal section of the tube, in the center of the thickness. ND 3". 7.6 mm thick.
43
VIEW
ML00090 / Sep.2017
Carbon Steel Tubing for Structural Application
M - Low Carbon SteelP - TubeAp - StructureCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
ML00071 — Reheating Cracking of a CrMo Vessel WeldM - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Micrographic aspect of opened cracks, filled with oxides.
63
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Micrographic details of opened cracks, filled with oxides.
56
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Micrographic aspect of thin cracks.
59
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Micrographic details of thin cracks.
63
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks