Oil and Gas

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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The location of the threaded fitting started leaking after less than five years in service. Although the corrosion rate was not high, the localized material loss in the threaded surface of the carbon steel flange allowed the connection leakage.
769
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Aspect Before AnalysisDf - General View
Aspect of the wire rope, 1 1/2" diameter, presenting regions of flattened areas at the surface of the outer wires. It is a 6 x 19 Seale construction, right regular lay.
552
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Aspect Before AnalysisDf - General View
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
756
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Fractographic detail of the longitudinal Charpy V testpiece, broken at -46°C and presenting energy of 64J (the average energy of three tespieces was 70J). The Charpy V testpiece was removed from the center of the bar. The micromechanism is quasicleavage and the test in this direction presented energy values superior than the minimum requirement of 45J.
944
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
Micrographic detail of the forging lap defect that appears at the nut surface like a crack, filled with oxides. The nut presented a martensitic structure in the center of the nut, but in the regions adjacent to the defect the structure is ferritic-bainitic due to decarburization. There are several globular oxides (grey spots) that became entrapped during the forging.
654
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Crack
Micrography of a transverse section of the lifting part, showing interdendritic voids close to the surface at the inner diameter of the padeye. The microstructure is tempered martensite.
450
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Casting defects
Longitudinal section of the fitting in the center of the thickness (2"). Refined ferritic structure.
370
VIEW
ML00030 / Jan.2017
Forging for High Pressure Application
M - Microalloyed SteelP - Machined PartAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Bainitic Ferrite
Ferritic perlitic microstructure, banded, in the center of the 5/16" thick C-Mn plate. Refined Structure.
371
VIEW
ML00021 / Dec.2017
5/16" CMn Steel Plate for Pressure Vessel
M - CMn SteelP - PlateAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Grain refined structure

More from these cases

ML00184 — Dissimilar Steels in a Threaded ConnectionM - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
The painting of the valve body was detaching at the vent location where the fitting was installed, not fully tighted. Three threaded fillets were outside of the body.
190
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Aspect After CleaningDf - Painting Detachment
The austenitic stainless steel fitting was removed from the valve body and presented the sdhesion of oily deposits.
150
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Aspect Before AnalysisDf - Surface Deposits
The cleaned fitting is sound. No corrosion, only surface stains.
121
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Aspect After CleaningDf - General View
The threads of the carbon steel valve body is corroded. The offshore ambient is wet and chloride rich, creating an aggressive environment for the carbon steel threads.
99
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Surface AspectDf - Corrosion
Not only the threads were corroded but all regions under the painting that was detached from the surface.
86
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Surface AspectDf - Corrosion

+8 more from this case →

ML00175 — Localized External Wear of a Wire RopeM - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Macrosection of the wire rope, transverse, showing 6 strands and an independent wire rope core (IWRC). Each strand presents three layers in a SEALE construction.
92
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Transverse Section AspectDf - Plastic Deformation
Low magnification micrography of a strain hardened pearlitic structure, in a longitudinal section, of one 3.2mm round wire of one strand.
62
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Highly strain hardened pearlitic structure of one external wire, 3.2mm diameter, of one strand.
55
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Pearlite
Micrographic detail of the strain hardened pearlitic structure, in a longitudinal section, of a 3.2mm external round wire of one strand. This structure presented a hardness level about 500 HV (1kg), measured in the center of the thickness in the metallographic section.
47
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Strain Hardened
Metallographic aspect of the wire surface in one strand external wire, showing the presence of oxides.
41
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - At the Surface

+11 more from this case →

ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Aspect of a 5/16" bolt manufactured in an AISI 316 austenitic stainless steel, that was also operating inside the pressure vessel, but was not yet damaged. It is a hexagonal head bolt, 1 1/2" long, fastened with a hexagonal nut and a lock washer.
118
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Low magnification micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides.
100
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides, strain hardened. The hardness values of the material are from 200HV1 to 300HV1, that meets the class 2 of strenght (ASTM A193 B8M class 2).
79
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Strain Hardened
Detail of the strain hardened austenitic microstructure. Micrography by optical microscope, of the longitudinal section of a bolt, in the center of the thickness.
76
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Strain Hardened
Aspect of a broken 5/16" bolt that was operating inside the pressure vessel in a condition that exceeds the limits of use of the AISI 316 steel. The fracture is located close to the position where there was the bolt head and the threads were "removed" close to the fracture surface.
75
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Fracture

+8 more from this case →

ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Fractography of the broken Charpy V testpiece, longitudinal, broken at -46°C and presenting energy of 64J (the average of three values was 70J). In this direction the material presented an energy value higher than the minimum requirement of 45J.
109
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
Fractography of the Charpy V testpiece, transverse section, broken at -46°C and presenting energy of 20J (the average of three results was 33J). The coarse structure and the alignement created a condition for low energy results in this specific direction, and the material did not present the minimum requirement of 45J.
103
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
74
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
61
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. The ferrite amount, measured by metallographic method, manual counting, is 59%.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section

+3 more from this case →

ML00099 — Forging Defect in a Cadmium Plated NutM - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Micrography of the nut in a section transverse to the surface indication. There are several microcracks (parallel and perpendicular to the nut surface) filled with oxides. The nut presented a martensitic microstructure in the center of the thickness and a ferritic-bainitic microstructure at surface and adjacent to the defect, due to decarburization occurred during high temperature forging.
130
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Crack
The general aspect of the 1 1/8" 2H nut, presenting rejectable indications that appear like cracks, located in the face and in the lateral side of the nut.
46
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Aspect Before AnalysisDf - General View
Aspect in detail of the 1 1/8" 2H nut face, presenting rejectable indications that appear like cracks.
49
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Aspect Before AnalysisDf - Lap
The general aspect of the lateral side of the 1 1/8" 2H nut, presenting a rejectable indication that looks like a straight crack.
48
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Aspect Before AnalysisDf - Lap
Micrographic detail of the lap at the nut surface, as polished. The 20 microns cadmium layer is evident, penetrating in the lap.
46
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - As polished micrographyDf - Lap

+2 more from this case →

ML00098 — Brittle Fracture of a Casting Lifting DeviceM - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Aspect of the broken padeye. The outer diameter is about 10" and the thickness of the casting is about 2".
22
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Aspect of the fracture surface, showing a brittle morphology. Flat fracture with chevron marks from regions close to the internal diameter of the padeye, where there are secondary cracks.
22
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Fracture
Micrography of the lifting padeye showing a dendritic path of a quenched and tempered martensitic microstructure. The segregated regions (white interdendritic regions) are more clearly identified in low magnification. Voids are located in these segregated regions.
21
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. Voids are located in interdendritic segregated regions.
20
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. Voids are located in interdendritic segregated regions. At this magnification the segregation is not clear.
16
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite

+12 more from this case →

ML00030 — Forging for High Pressure ApplicationM - Microalloyed SteelP - Machined PartAp - Oil and GasCd - Typical manufacturing
Longitudinal section of the fitting in the center of the thickness (2"). Refined ferritic structure.
66
VIEW
ML00030 / Jan.2017
Forging for High Pressure Application
M - Microalloyed SteelP - Machined PartAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Grain refined structure
Longitudinal section of the fitting in the center of the thickness (2"). Refined ferritic structure.
63
VIEW
ML00030 / Jan.2017
Forging for High Pressure Application
M - Microalloyed SteelP - Machined PartAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Grain refined structure
ML00021 — 5/16" CMn Steel Plate for Pressure VesselM - CMn SteelP - PlateAp - Oil and GasCd - Typical manufacturing
Ferritic perlitic microstructure, banded, in the center of the 5/16" thick C-Mn plate. Refined Structure.
64
VIEW
ML00021 / Dec.2017
5/16" CMn Steel Plate for Pressure Vessel
M - CMn SteelP - PlateAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Banded Pearlite
Ferritic perlitic microstructure, banded, in the center of the 5/16" thick C-Mn plate. Refined Structure.
54
VIEW
ML00021 / Dec.2017
5/16" CMn Steel Plate for Pressure Vessel
M - CMn SteelP - PlateAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Longitudinal Section