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Crevice Corrosion in a Subsea System — Aspect Before Analysis

Product: Raw Material Microstructure: Austenite clear all

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A 10B 3

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As received aspect of the sacrificial casting, 2" internal diameter. The casting was solution annealed heat treated.
488
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View
The scanning electron microscopy image of the internal surface of the tube in position 2 shows a localized corrosion region with intergranular morphology, as well a crack from the corroded region.
1237
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
Micrography of the new tube close to a region of a casting defect (shrinkage), presenting only austenitic structure with a network of primary precipitates.
351
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides
Micrographic detail of the austenitic structure at the surface, where the grain size of the material increased. By optical microscopy the intragranular precipitation due to solution annealing and aging is not revealed.
794
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
The 8" ND, 1 1/4" thick, seamless pipe that was welded by GMAW process in 6G position. The testpiece was adopted for ASME IX qualification tests.
403
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Aspect Before AnalysisDf - Welded Joint
Aspect of the cracking after Dye Check Test (Liquid Penetrant) in the external side of the line that operates at 800°C, insulated, and presented the leakage associated to the longitudinal seam weld of the fitting. The circumferential butt weld of the fitting to a pipe did not fail. See the schematic drawing in the next figure
371
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Aspect by NDTDf - Through Wall Cracking
Image by scanning electron microscopy of the metallurgically bonded interface of the composite seamless tube (carbon steel externally claded with stainless steel), in the side of the stainless steel where a strain hardening effect plus a carbide precipitation in twins is shown. The hardness of this region (279 HV0.3) is a lot higher than the value obtained out of this region (167 HV0.3) for the same stainless steel.
814
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface
Macroscopic aspect of the 1" shaft fracture surface, revealing beach marks at the surface typical of fatigue, initiated from the surface of the spline shaft at the gear position.
498
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Aspect Before AnalysisDf - Fatigue Fracture

More from these cases

ML00164 — Austenitic SS Casting for Valve BodyM - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Macrography of a longitudinal section of the valve body, presenting the granular structure. The main bore diameter is 2". The casting was tested in two positions. In radial direction in the center of the body (3" solid), and in the longitudinal direction in the wall (1" thick).
78
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Longitudinal Section
Micrography of a longitudinal section, in the center of the valve body, solid 3" thickness. The structure is austenitic with delta ferrite in interdendritic spaces.
67
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography of a longitudinal section, in the center of the valve body. The structure is austenitic with delta ferrite in interdendritic spaces. The austenite presents a cored matrix in the dendrites, indicating the chemical composition was not homogeneized during the heat treatment.
60
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrographic detail of the cored austenitic structure with delta ferrite in interdendritic spaces. The chemical composition was not homogeneized during the heat treatment.
55
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrography of a longitudinal section, in the 1" thickness valve wall. The structure is austenitic with delta ferrite in interdendritic spaces.
48
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite

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ML00086 — Intergranular Corrosion of Sensitized 304SSM - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in the colder part of the equipment, position 1. The material presented carbide precipitation at grain boundaries (not yet fully surrounding the grains) and at this point the tube presented no internal corrosion.
338
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 2, where the temperature was higher and the carbide precipitation increased during service.
272
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 3, where intergranular and transgranular carbide precipitation occurred during service.
234
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation
The low magnification image of the internal surface of the tube, in position 2, shows several points of localized corrosion, with intergranular morphology.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
Micrography of a longitudinal section of the tube in position 2, presenting thinning by intergranular corrosion at the internal surface.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion

+3 more from this case →

ML00097 — Cast SS Tube Removed From High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
The macrography of a transverse section of the new tube shows that there are shrinkage voids close to the internal surface, that is exposed to high temperature air. The tube is a 4" diameter and 1/4" thick.
62
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Transverse Section AspectDf - Casting Structure
Micrography close to the external surface of a new tube, sound.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the External Surface
Micrography close to the internal surface of a new tube, presenting casting defects.
47
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography of the tube removed from service after 6 month, close to a region of a casting defect (shrinkage), presenting austenitic structure with a network of primary precipitates (initial stage of coarsening) and intragranular secondary precipitation.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation
The macrography of a transverse section of the tube removed from service after 6 months, with damage close to the internal tube surface. The tube is a 4" diameter and 1/4" thick.
41
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Transverse Section AspectDf - Casting Structure

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ML00089 — Inconel 718 Allen Bolt for Subsea ApplicationM - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
The macrography shows the longitudinal section of the allen bolt, 1/2" nominal diameter, that was machined from a heat treated bar (solution annealed and aged). The granular structure presents differences in the grain sizes. At the bolt head (external surface of the original bar) the austenitic grain size is larger than in the center of the bar where the particles in segregated bands "arrested" the grains during hot forming and solution annealing.
58
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched MacroDf - Machined Thread
The micrography of a longitudinal section of the bolt close to the surface, at the thread, shows that it was machined from a bar, not rolled.
37
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
The micrography of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"), shows an equiaxial granular structure. Although the material was hardened by heat treatment (solution annealing and aging), the microstructure at this magnification does not reveal the intragranular precipitation.
34
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Micrographic detail of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"). Although the material was hardened by heat treatment (solution annealing and aging), the microstructure observed by optical microscopy does not reveal the intragranular precipitation.
33
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched MacroDf - Austenite
The micrography of a longitudinal section, at the bolt head close to the surface of the original bar. In this region the material increased the grain size due to the lack of particles (inclusions), to "arrest" the grain boundaries (during hot forming and solution annealing). The smaller grain size is located in the center of the bar, that concentrated the inclusions.
30
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched MacroDf - Dual grain sizes

+1 more from this case →

ML00066 — GMAW Welded Joint in 9%Ni Alloy SteelM - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Transversal section of the 625 nickel alloy multipass weld. Pipe of 1 1/4' thickness
72
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - NItal Etched MacroDf - Welded Joint
Schematic drawing presenting the transversal section of the 625 nickel alloy multipass weld
56
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Identification drawingDf - Welded Joint
Micrography of the base metal presenting a banded microstructure in the longitudinal section of the pipe.
52
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of a longitudinal section of the base metal presenting a quenched and tempered microstructure.
50
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of the low temperature heat affected zone of the pipe. The intercritical temperature (IC) is evident in the decorated grain boundaries of the previous austenite.
43
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone

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ML00061 — Creep in a Seam Weld of a 304H SS FittingM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Schematic drawing presenting the aspect of the cracking after Dye Check Test (Liquid Penetrant) in the external side of the line that operates at 800°C, insulated, and presented the leakage associated to the longitudinal seam weld of the fitting. The circumferential butt weld of the fitting to a pipe did not fail.
62
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Identification drawingDf - Through Wall Cracking
Aspect of the internal side of the fitting, at the longitudinal seam weld, and macrography of a transverse section showing the through wall cracks.
62
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Transverse Section
Through wall cracking in the longitudinal seam weld of the fitting. Several cracks, longitudinal to the weld, were created by the connection of voids in the weld metal, associated to a strong microstructural evolution.
191
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Cracks
Micrography of a longitudinal section of the fitting, at the base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
44
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal
Micrographic detail of the fitting base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
40
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal

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ML00056 — Seamless Tube Externally Cladded with SSM - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
The 2 1/2" nominal diameter seamless tube is externally cladded with stainless steel.
196
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Aspect Before AnalysisDf - Welded Joint
The macrography of a transverse section shows the carbon steel tube, externally cladded with stainless steel. The tube was removed from service where it was welded to other tubes to form a wall.
156
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Kalling Etched MacroDf - Transverse Section
Macrography of the tube transversal section presenting the studied assembly.
138
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Transverse Section
Micrography of a longitudinal section of the pipe showing that the carbon steel pipe is slightly banded and there is a decarburized layer at the solid solution welded interface. The stainless steel structure (in the right side of the figure) is not revealed using the Nital etch.
126
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the pipe showing the carbon steel pipe , internal.
123
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite

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ML00041 — Fatigue Fracture of Inconel 718 Spline ShaftM - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
xx
117
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Aspect Before AnalysisDf - At the Surface
Macroscopic aspect of the 1" shaft fracture surface, revealing beach marks at the surface typical of fatigue, initiated from the surface of the spline shaft at the gear position.
121
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Aspect Before AnalysisDf - Fatigue Fracture
SEM fractograph at 1200x magnification showing an intergranular fracture surface with angular, faceted grains and fine feather-like markings.
86
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
Microscopic detail of the transgranular striation in the fracture surface.
78
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
The micrography of a transverse section of the shaft shows the granular austenitic structure close to the surface of the shaft.
67
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - At the Surface

+7 more from this case →