Sampling and Analysis

113 cases · 516 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Capture method: Optical Microscope clear all

Sampling and Analysis — sub-branches

At the Surface 37Base Metal 59Close to the External Surface 36Close to the Internal Surface 30External Surface 6Fusion Line 23General View 2Heat Affected Zone 73In the Center of the Thickness 35In the Center of the Weld 2Internal Surface 7Longitudinal Section 68Low Mag 6Microhardness Indentations 1Microhardness identations 1Radial Section 1T/4 of the external surface 2Transverse Section 33Weld Metal 80Weld Repair 4Welded Joint 10

Results

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Micrography, as polished, of the transverse section of the forged pin with the layer applied by a (thermal) spray and fuse process. The structure of the layer that is 0.7 mm thick, presented entrapped pores and globular oxides. The layer was melted after application by thermal spray (in this case using a flame) and the pin was quenched and tempered after the full application and melting of the layer.
360
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - As polished micrographyDf - Transverse Section
Shaft microstructure in the longitudinal section, showing aligned segregations typical of the material forming.
31
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrography of the longitudinal section of the tube, close to the external surface, presenting a thick deposit.
110
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - As polished micrographyDf - Close to the External Surface
Micrography of a longitudinal section in the center of the bolt. Granular austenitic microstructure, equiaxial, primary precipitates (isolated), precipitation hardened (not detectable by metalography, only because of the hardness level)
63
VIEW
ML00106 / Dec.2017
Inconel 718 Submarine Bolt
M - NiCrFe AlloyP - BoltAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Low magnification micrography of the bolt in a longitudinal section, at the bolt thread, showing no evidences of forming operations, indicating it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial, precipitation hardened (shadow in the grains).
45
VIEW
ML00105 / Jun.2018
Inconel 718 Bolt of Special Head
M - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
The micrography of the longitudinal section of the tube, close to OD, shows the paralel cracks, filled with oxides, perpendicular to the surface.
1441
VIEW
ML00104 / Dec.2017
Thermal Fatigue of a Boiler Tube
M - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
Cm - As polished micrographyDf - Close to the External Surface
Micrography of the longitudinal section of the fitiing, in a free-cutting steel. The microstructure is predominantly ferritic and there is a large amount of sulfide inclusions, aligned perpendicular to the forming direction.
98
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrography of the 4130 steel, normalized and tempered. The structure is sligthly banded (segregated) and the average hardness level is 20 HRc.
92
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal

More from these cases

ML00109 — Thermal Spray and Fuse Layer in Forged PinM - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Low magnification micrography of the pin in the center of the 25 mm thickness. Bainitic structure of the material that was quenched and tempered after spray and fuse application. Transverse section presenting a uniform structure.
12
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - Nital Etched Micrography by OMDf - Base Metal
ML00107 — Carburized 9Cr1MoV Superheater TubeM - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Micrography of the longitudinal section of the tube, close to the internal surface, presenting a thick deposit.
98
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography of the longitudinal section of the tube, close to the external surface. A scale is evident at the surface as well as a carburizing layer.
83
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of the longitudinal section of the tube, close to the internal surface. A thick scale is evident, but no microstructural changes compared to the center of the tube.
92
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00106 — Inconel 718 Submarine BoltM - NiCrFe AlloyP - BoltAp - SubseaCd - Typical manufacturing
Low magnification micrography of the bolt in a longitudinal section, at the bolt thread, showing no evidences of forming operations, indicating that it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial.
54
VIEW
ML00106 / Dec.2017
Inconel 718 Submarine Bolt
M - NiCrFe AlloyP - BoltAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
ML00105 — Inconel 718 Bolt of Special HeadM - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Low magnification micrography of the bolt in a longitudinal section, at the bolt head, showing no evidences of forming operations, indicating it was machined from a heat treated bar. Austenitic microstructure, granular, equiaxial, precipitation hardened (shadow in the grains).
31
VIEW
ML00105 / Jun.2018
Inconel 718 Bolt of Special Head
M - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Low magnification micrography of the bolt in a longitudinal section, in the center of the thickness. Austenitic microstructure, granular, equiaxial, precipitation hardened (shadow in the grains).
30
VIEW
ML00105 / Jun.2018
Inconel 718 Bolt of Special Head
M - NiCrFe AlloyP - FastenerAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
ML00104 — Thermal Fatigue of a Boiler TubeM - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
The micrography of the longitudinal section of the tube, close to ID, shows the paralel cracks, filled with oxides, perpendicular to the surface.
229
VIEW
ML00104 / Dec.2017
Thermal Fatigue of a Boiler Tube
M - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
Cm - As polished micrographyDf - Close to the Internal Surface
ML00103 — Brittle Fracture of a Free-Cutting ConnectorM - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Micrography of the transerse section of the fitiing, in a free-cutting steel. The microstructure is predominantly ferritic and the inclusions appear as dots.
97
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
ML00102 — AISI 4130 Forging Welded and OverlaidM - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Micrography of the 4130 steel, normalized and tempered. The microstructure is bainitic.
88
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) of the Inconel overlay (white because it was not etched with the Nital). The structure is ferritic/bainitic because the overlay was conducted in two layers, and all the HAZ was reheated during welding.
66
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) of the Inconel overlay (white because it was not etched with the Nital). The structure is ferritic/bainitic because the overlay was conducted in two layers, and all the HAZ was reheated during welding.
61
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the tubular 4130 forging at the heat affected zone (HAZ), butt weld face. The structure is tempered martensite because the welded joint was PWHT at 630°C. The original forging was normalized and tempered at 660°C.
48
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) at the face of the butt weld. The structure is a tempered martensite because the joint was PWHT at 630°C. The original forging was normalized and tempered at 660°C.
43
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone

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