Sampling and Analysis

10 cases · 41 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Bainite Capture method: Optical Microscope clear all

Sampling and Analysis — sub-branches

At the Surface 1Base Metal 12Close to the External Surface 2Close to the Internal Surface 2External Surface 1Fusion Line 3Heat Affected Zone 7In the Center of the Thickness 1Longitudinal Section 3Weld Metal 9

Results

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Micrography of the external tube surface, presenting a crack at the weld margin. This cracking could have been created by thermal induced cycles (fatigue), but it did not propagate into the tube wall. In some regions of the external side of the tube the weld metal was detached.
77
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - External Surface
Micrography of a longitudinal section of the pipe substrate, in low magnification, showing a uniform microstructure,
51
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of a longitudinal section of the pipe substrate, in low magnification, showing a uniform microstructure,
79
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Shaft microstructure in the longitudinal section, showing aligned segregations typical of the material forming.
31
VIEW
ML00108 / Dec.2017
Thermal Spray Layer in a Pinion Shaft
M - High Strength Low AlloyP - ShaftAp - EngineCd - Coating Defect
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrography of the longitudinal section of the tube, close to the external surface, presenting a thick deposit.
109
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - As polished micrographyDf - Close to the External Surface
Micrography of the 4130 steel, normalized and tempered. The structure is sligthly banded (segregated) and the average hardness level is 20 HRc.
92
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of a longitudinal section of the pin, in the center. The low carbon content of the steel in the center of the pin makes the structure bainitic even though it was quenched and tempered after carburizing.
80
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
The liquation crack is a hot crack in the base metal (at the HAZ) that induces a solidification crack in the weld metal.
66
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Weld Metal

More from these cases

ML00163 — Corrosion Fatigue of a Boiler Waterwall TubeM - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Micrography of the external tube surface, presenting the cracking at the margin of the weld. This cracking could have been created by thermal induced cycles (fatigue), but it did not propagate into the tube wall.
85
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Fusion Line
ML00133 — Seam Welded Pipe Cladded with Alloy 625M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Micrography of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure obtained by the pipe quenching and tempering,
48
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
ML00132 — Seamless Pipe Overlaid with Alloy 625M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Micrography of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure obtained by the pipe quenching and tempering,
72
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Low magnification micrography of a longitudinal section of the pipe at the interface between overlay layers, with electrolytic etch that reveals the Ni alloy structure, large columnar grains with celular morphology.
66
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Chromic Acid Electrolytic EtchedDf - Weld Metal
Micrography of a longitudinal section of the pipe at the interface between overlay layers, with electrolytic etch that reveals the Ni alloy structure, large grains with celular dendritic morphology.
52
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Chromic Acid Electrolytic EtchedDf - Weld Metal
Micrographic detail of a longitudinal section of the pipe in the overlay weld metal, with electrolytic etch that reveals the Ni alloy structure with celular dendritic morphology and precipitates.
48
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Chromic Acid Electrolytic EtchedDf - Weld Metal
ML00107 — Carburized 9Cr1MoV Superheater TubeM - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Micrography of the longitudinal section of the tube, close to the internal surface, presenting a thick deposit.
98
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography of the longitudinal section of the tube, close to the external surface. A scale is evident at the surface as well as a carburizing layer.
83
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of the longitudinal section of the tube, close to the internal surface. A thick scale is evident, but no microstructural changes compared to the center of the tube.
92
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00102 — AISI 4130 Forging Welded and OverlaidM - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Micrography of the 4130 steel, normalized and tempered. The microstructure is bainitic.
88
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) of the Inconel overlay (white because it was not etched with the Nital). The structure is ferritic/bainitic because the overlay was conducted in two layers, and all the HAZ was reheated during welding.
66
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) of the Inconel overlay (white because it was not etched with the Nital). The structure is ferritic/bainitic because the overlay was conducted in two layers, and all the HAZ was reheated during welding.
61
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the tubular 4130 forging at the heat affected zone (HAZ), butt weld face. The structure is tempered martensite because the welded joint was PWHT at 630°C. The original forging was normalized and tempered at 660°C.
48
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) at the face of the butt weld. The structure is a tempered martensite because the joint was PWHT at 630°C. The original forging was normalized and tempered at 660°C.
43
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone

+2 more from this case →

ML00081 — Hydrogen Cracking of a Chromium Plated Carburized PinM - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Micrographic detail a longitudinal section of the pin, at the surface, showing the case hardened. The pin carburized, quenched and tempered structure presents a gradient of carbon content and consequently a gradient of martensitic structure and hardness. Close to the surface the hardness level is 742 HV1 .
87
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - At the Surface
ML00072 — Liquation Cracks in a High Strength JointM - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Micrographic detail of the cracks at the fusion line of the welded joint, at the connector side. The cracking presents morphology of melting regions of impurities at grain boundaries of the large grains of the heat affected zone (HAZ).
57
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Fusion Line
Micrography of the AISI 4130 forging, 5/8" thickness, close to the welded region, in the longitudinal section.
42
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal Left Side
Micrographic detail of the AISI 4130 forging, 5/8" thickness, close to the welded region, in the longitudinal section.
45
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal Left Side
Micrography of the X65 pipe, 5/8" thickness, in the longitudinal section.
45
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal Right Side
Micrographic detail of the X65 pipe, 5/8" thickness, in the longitudinal section.In the center of the pipe thickness there is a segregation band of bainitic structure. The cracking was not associated to the pipe but to the other side, the forged connector.
43
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal Right Side

+2 more from this case →