Microstructure

11 cases · 50 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Brittle Behavior clear all

Microstructure — sub-branches

Bainitic Martensitic 3Coarse Structure 1Decarburized Surface 1Ferrite and Austenite 3Ferrite and Pearlite 1Graphite in Flakes 3Graphite in Nodules 1Intragranular Secondary Precipitation 1Martensite 14Martensite, delta ferrite & carbides 3Non Metallic Inclusions 1Predominantly Ferritic 1Predominantly Pearlitic 2Sigma 7Tempered Martensite 1Zn Layer 7

Results

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Micrography presenting a tempered martensitic microstructure, with light etch in segregated bands.
74
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Tempered Martensite
Micrographic detail of spring surface, showing the pits full of corrosion deposits and a small decarburized layer (probably from the manufacturing processes).
30
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Decarburized Surface
Micrography of a longitudinal section of the socket at the position where the fracture occurred. Uniform tempered martensitic structure. The hardness of this microstructure is 639 HV1Kg.
74
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the longitudinal section of the cylinder, at the internal diameter, in contact with the treated cooling water, presenting large graphite flakes in a predominatly perlitic matrix. It is important to mention that the flakes are almost interconnecting themelves.
47
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Graphite in Flakes
Micrography of the high strenght steel, heat treated, of the casting device. The microstructure is bainitic martensitic.
109
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
106
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrographic detail of the longitudinal section of the fitiing, in a free-cutting steel. The microstructure is predominantly ferritic, with small perlitic areas and some free cementite at ferritic grain boundaries. There is a large amount of sulfide inclusions, aligned perpendicular to the forming direction.
107
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Non Metallic Inclusions
Micrography of the lifting padeye showing a dendritic path of a quenched and tempered martensitic microstructure. The segregated regions (white interdendritic regions) are more clearly identified in low magnification. Voids are located in these segregated regions.
21
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite

More from these cases

ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Micrographic detail of the transverse section of the spring wire, martensitic.
24
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the martensitic structure, uniform through thickness.
17
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the martensitic structure, clearly obtained from a refined previous austenitic structure .
19
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Martensite
Micrographic detail of the martensitic structure.
19
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Martensite
ML00161 — Brittle Fracture of a High Strength SocketM - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Micrography of a longitudinal section presenting an uniform tempered martensitic structure.
81
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the tempered martensitic structure.
80
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Brittle Fracture of a High Strength Socket
4
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
ML00141 — Brittle Fracture of a Corroded Gray Cast IronM - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Micrography of the longitudinal section of the cylinder, at the internal diameter, in contact with the treated cooling water, presenting large graphite flakes in a predominatly perlitic matrix. It is important to mention that the flakes are almost interconnecting themelves.
48
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Predominantly Pearlitic
Micrography of the longitudinal section of the cylinder, in the center of the thickness, presenting large graphite flakes in a predominatly perlitic matrix. There are also ferritic regions.
33
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Graphite in Flakes
Micrography of the longitudinal section of the cylinder, in the center of the thickness, presenting large graphite flakes in a predominatly pearlitic matrix.
31
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Predominantly Pearlitic
Micrography of the longitudinal section of the cylinder, at the external diameter (right side of the figure), presenting smaller interdendritic graphite flakes in a ferritic-perlitic matrix. This surface is painted.
32
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Graphite in Flakes
Micrography of the longitudinal section of the cylinder, at the external diameter (right side of the figure), presenting smaller interdendritic graphite flakes in a ferritic-perlitic matrix. It is also possible to see free carbides (cementite) very close to the cylinder surface (less than 50 microns), associated to positions of graphite. This surface was painted.
25
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
ML00138 — Liquid Metal Embrittlement of a HSLA SteelM - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Micrography of the high strenght steel, heat treated, of the casting device. The microstructure is bainitic martensitic.
92
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Micrographic detail of the high strenght steel microstructure, bainitic martensitic.
85
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Micrography of the casting at the surface, presenting a zinc layer deposited in a hot dip process. The thickness of the layer is about 0.3mm in this position, that is higher than expected for this process. The steel substrate is not revealed because the etch was light and the zinc layer protects the low aloy steel during the etch.
93
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by SEMDf - Zn Layer
Micrographic detail of the zinc layer at the surface.
88
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Zn Layer
Scanning electron fractography (originally 500x), showing zinc deposits at the fracture surface.
73
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Fractography by SEMDf - Zn Layer

+4 more from this case →

ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic detail of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
102
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Metallographic detail of the large amount of sigma phase, associated to the ferritic structure.
105
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
92
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Micrographic details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
85
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
High magnification details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
81
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma

+4 more from this case →

ML00103 — Brittle Fracture of a Free-Cutting ConnectorM - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Micrographic detail of the transverse section of the fitiing, in a free-cutting steel. The microstructure is predominantly ferritic, some perlitic areas and free cementite at ferritic grain boundaries. There is a large amount of inclusions, that appear as spots.
82
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Predominantly Ferritic
ML00098 — Brittle Fracture of a Casting Lifting DeviceM - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. Voids are located in interdendritic segregated regions.
20
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. Voids are located in interdendritic segregated regions. At this magnification the segregation is not clear.
16
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. The hardness level of the material is about 39 HRc.
14
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of a region where there is a large amount of casting defects. Shrinkage voids in interdendritic spaces, some interconnected and cracked.
13
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of a region where there is a large amount of casting defects. Shrinkage voids in interdendritic spaces, some interconnected and cracked.
13
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite