Microstructure

69 cases · 264 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Standard: A Capture method: Optical Microscope clear all

Microstructure — sub-branches

Austenite 17Austenitic with Primary Carbides 2Bainite 5Bainitic Ferrite 3Bainitic HAZ 3Bainitic Martensitic 3Banded Pearlite 7Banded Structure 11Carburized Layer 2Clad Interface 3Coalesced structure 6Coarse Structure 4Coating Layer 2Columnar Grains 2Delta Ferrite Islands 2Delta ferrite 4Duplex structure 6Equiaxial Grains 2Ferrite 2Ferrite and Austenite 6Ferrite and Bainite 3Ferrite and Pearlite 33Free Carbides in Pearlite Colonies 1Fusion Line 6Grain refined structure 9Granular structure 1Graphite Type A (ASTM A247) 2Graphite in Flakes 5Graphite in Imperfect Nodules 1Graphite in Nodules 6Intergranular Precipitation 3Intragranular Secondary Precipitation 5Martensite 27Matrix of ferrite and pearlite 5Network of Primary Carbides 2Non Metallic Inclusions 4Overtempered Structure 1Pearlite 7Pearlite Matrix 3Predominantly Ferritic 14Predominantly Pearlitic 2Sigma 3Strain Hardened 18Tempered Martensite 3Tempered Structure 1Uniform Structure 1Zn Layer 6

Results

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Microstructure of the stud in the longitudinal section, presenting segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration.
69
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
106
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrographic detail of the rolled thread that was heat treated later. The bolt was quenched and tempered to 30 HRc and presented a martensitic structure.
110
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the ferrite and austenite structure in the transverse section of the forged bar, in the center of the thickness.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Nitronic 60 cylinder. Micrography of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, equiaxial grains, and evidences of the manufacturing process by hot forming.
179
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrographic detail of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Pearlite colonies in bands.
401
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of a transverse section of the 5 mm thick tubing, in the center of the thickness. Ferritic-pearlitic structure, with the pearlite presenting a coalesced aspect. The tubing was in service at ambient temperature, painted, and the coalesced aspect was generated before service, perhaps during the tubing manufacturing.
393
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Pearlite colonies in bands.
346
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite

More from these cases

ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Microstructure of the stud in the longitudinal section, out of a region of segregation, where the tempered martensitic microstructure appears more uniform.
72
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration. The localized microhardness (50g) in the band showed levels about 540HV, and out of the band, in the same localtion, presented an average hardness of 321 HV, indicating that the material is non uniform in the regions where there are bands.
66
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrographic detail of the martensitic structure of the stud in the longitudinal section, out of a region of segregation, where the microstructure appears more uniform and the microhardness is about 370HV (50g).
62
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic detail of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
102
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Metallographic detail of the large amount of sigma phase, associated to the ferritic structure.
105
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Microstructural analysis of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
67
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
63
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
61
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
ML00130 — Fatigue Fracture of Overloaded BoltsM - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
The microstructure of the bolt is martensitic in the center of the thickness. Longitudinal section.
103
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Micrographic detail of the ferrite and austenite structure in the longitudinal section of the forged bar, in the center of the thickness.
55
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
ML00121 — Pitting Corrosion in a Subsea SystemM - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Nitronic 60 cylinder. Micrography of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, with some aligned non metallic inclusions.
157
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Nitronic 60 cylinder. Micrographic detail of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, equiaxial grains, typical of a solution annealed condition.
136
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Nitronic 60 cylinder. Micrography of the longitudinal section close to the surface, presenting a fully austenitic microstructure, with a shadow close to the external surface that is associated to a small layer of strain hardened structure (deformation twins).
133
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Nitronic 60 cylinder. Micrography of the longitudinal section close to the surface, presenting a fully austenitic microstructure, with a 0.15mm layer of strain hardened structure (deformation twins).
120
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Nitronic 60 cylinder. Micrographic detail of the longitudinal section close to the surface, presenting a fully austenitic microstructure, with a layer of strain hardened structure (deformation twins).
113
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Strain Hardened

+3 more from this case →

ML00116 — CMn Steel Structural Tubing 6 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic banded structure.
30
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
ML00115 — CMn Steel Structural Tubing 5 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Banded structure, ferritic-pearlitic.
16
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
ML00114 — CMn Steel Structural Tubing 8 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic banded structure.
29
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure