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19 cases · 179 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Macrography of a ring transverse section presenting a large variation in the grain size, revealing the diferences in the solidification rate.
453
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O solution Etched MacroDf - Casting Structure
Macrography of a wheel section close to the tread, where the material receives a localized surface hardening by quenching and tempering. The average hardness at the surface is 346HB and in the center is 196HB. The wheel was in operation for a long time and the analyzed part is at the wheel tread.
902
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - NItal Etched MacroDf - Transverse Section
The coasters present a handmake look. The grooves are of different sizes and the octogonal shape is irregular. The pieces presented a weight that suggested that the bright finish is a metallic coating, later identified by EDS analysis as silver coating, typical of a decorative plating.
452
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Aspect Before AnalysisDf - General View
The shaft was removed from service without a failure. It was 4' long and the diameters varied from 2 1/2" to 4 1/2". It was analyzed to be specified for purchasing a new one but properties evidenced bad ductility and brittle behavior even at ambient temperature, associated to a microestruture "as hot rolled".
1238
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Aspect Before AnalysisDf - General View
Micrographic detail of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Pearlite colonies in bands.
401
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of a transverse section of the 5 mm thick tubing, in the center of the thickness. Ferritic-pearlitic structure, with the pearlite presenting a coalesced aspect. The tubing was in service at ambient temperature, painted, and the coalesced aspect was generated before service, perhaps during the tubing manufacturing.
393
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Pearlite colonies in bands.
346
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the ferritic-pearlitic structure of the angle L shape, equal legs, in the transverse section.
468
VIEW
ML00035 / Dec.2017
Carbon Steel L Shape
M - Low Carbon SteelP - Rolled ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite

More from these cases

ML00166 — Tin Bronze Wear Ring of Seawater PumpM - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Low magnification micrography of a transverse section of the ring showing a dendritic structure.
64
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of a transverse section of the ring showing a cored alpha structure with segregation at interdendritic regions. This structure is in a region close to the ring surface.
52
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of a transverse section of the ring showing a cored alpha structure with strong segregation at interdendritic regions, and regions of a white structure at grain boundaries. This structure is in a region close to the center of the ring.
51
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrographic detail of the cored alpha structure with light segregation at intergranular regions (light layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the ring surface, where the solidification was quicker.
49
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics
Micrographic detail of the cored alpha structure with strong segregation at intergranular regions (dark layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the center of the ring, where the solidification was slower.
47
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics

+2 more from this case →

ML00158 — Surface Hardened Carbon Steel WheelM - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Micrography of the wheel in the center of the thickness. The material presents a coarse structure.
88
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of the wheel in the center of the thickness, presenting a predominantly pearlitic structure and average hardness abot 196HB.
74
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Micrographic detail of the coarse pearlitic structure in the center of the wheel thickness. The part presents a wrought structure.
73
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Pearlite
Micrography of the wheel at the surface that was quenched and tempered. The material presents a tempered martensitic structure, with hardness that varied from 327HB to 363HB.
55
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrography of the wheel at the hardened surface, presenting a refined martensitic structure, tempered for average hardness of 346 HB.
50
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - At the Surface

+5 more from this case →

ML00156 — Antique Silver Plated Decorative PieceM - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Piece that was analysed by non destructive tests. Octogonal shape. Two irregular grooves. The coaster was manufactured in a cooper alloy substrate and a metallic coating. The analysis to reveal the substrate microstructure was conducted on the back of the part, in a non destructive preparation, that included light grinding, polishing and etching.
61
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Aspect Before AnalysisDf - General View
Light grinding the back of the coaster. The surface was only partially ground, removing the metallic coating, and exposing the substrate, that appeared yellow indicating the manufacturing in a cooper alloy.
63
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Preparation TechniqueDf - General View
Aspect of the back of the coaster after grinding. The coating was partially removed. The chemical analysis was conducted in the ground part to obtain the composition of the substrate, that showed to be a yellow brass alloy. It is interesting to note that the alloy presented 2.3% lead.
63
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Preparation TechniqueDf - At the Surface
Back of the coaster showing the region that was prepared for the non destructive analysis. It was ground and polished (the coating was removed), showing the yellow aspect of the substrate, in the left bottom part of the image.
64
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - As polishedDf - General View
Image presenting the back of the coaster where the microstructure of the substrate was identified. The composition of the brass (about 35% Zn) indicates that the expected structure is alpha plus beta. The front of the coaster presents two grooves which surface morphology was analyzed by scanning electron microscopy.
65
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Surface AspectDf - General View

+10 more from this case →

ML00152 — Low Alloy Steel Pump ShaftM - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
The longitudinal section of the shaft shows a coarse structure. Only very close to the surface the structure is slightly refined.
99
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - NItal Etched MacroDf - Longitudinal Section
The longitudinal section of the shaft, in the center of the thickness, shows a coarse structure, and a ferritic/bainitic structure with pearlite islands.
97
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
The coarse structure in the center of the shaft thickness is evidenced by free ferrite islands at the previous austenite grains. The presence of a pearlitic structure evidences the slow cool of the material.
85
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Micrographic detail of the pearlitic structure in the center of the shaft thickness.
82
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by SEMDf - Pearlite
The longitudinal section of the shaft, at the surface, also shows a coarse structure, and a ferritic/bainitic structure with pearlite islands. There is only a small refining in the previous austenite grain boundaries, indicating that the material was not heat treated.
75
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Longitudinal Section

+2 more from this case →

ML00116 — CMn Steel Structural Tubing 6 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic banded structure.
30
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Bands of pearlite colonies. Refined grains.
26
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of a transverse section of the tubing in the center of the thickness. Ferritic-pearlitic structure. The structure is fully ferritic in a small extension at the surface, due to a decarburization effect during manufacturing.
26
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrographic detail of a transverse section of the tubing, close to the internal surface. Ferritic-pearlitic structure, refined.
20
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00115 — CMn Steel Structural Tubing 5 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Banded structure, ferritic-pearlitic.
16
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. The pearlite is banded and presented a coalesced aspect.
12
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrographic detail of a transverse section of the tubing, at the external surface. Ferritic-pearlitic structure. The roughness of the surface is high because the structure was painted and a blasting treatment was probably applied to the surface to improve adherence.
15
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrographic detail of a transverse section of the tubing, close to the internal surface. Ferritic-pearlitic structure. Very close to the surface the amount of ferrite is higher than in the center and the grain is coarser, due to a decarburization effect probably occurred when the surface was exposed to high temperature during manufacturing.
13
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00114 — CMn Steel Structural Tubing 8 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic banded structure.
29
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Bands of pearlite colonies. Refined grains.
29
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of a transverse section of the tubing, at the external surface. Ferritic-pearlitic structure. The roughness of the surface is high because the structure was painted and a blasting treatment was probably applied to the surface to improve adherence.
20
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of a transverse section of the tubing, close to the internal surface. Ferritic-pearlitic structure, refined.
16
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00035 — Carbon Steel L ShapeM - Low Carbon SteelP - Rolled ShapeAp - StructureCd - Removed From Service
Micrography of the transverse section of the rolled shape presenting an aligned structure, ferritic-pearlitic. Transverse section.
97
VIEW
ML00035 / Dec.2017
Carbon Steel L Shape
M - Low Carbon SteelP - Rolled ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of the transverse section of the rolled shape presenting a ferritic-pearlitic microstructure. Transverse section, close to the surface.
80
VIEW
ML00035 / Dec.2017
Carbon Steel L Shape
M - Low Carbon SteelP - Rolled ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrography of the transverse section of the rolled shape presenting an aligned structure, ferritic-pearlitic.
62
VIEW
ML00035 / Dec.2017
Carbon Steel L Shape
M - Low Carbon SteelP - Rolled ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Transverse Section
Micrography of the transverse section of the rolled shape presenting an aligned structure, ferritic-pearlitic, and long sulfide inclusions. Center of the leg of 12 mm thickness.
58
VIEW
ML00035 / Dec.2017
Carbon Steel L Shape
M - Low Carbon SteelP - Rolled ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Non Metallic Inclusions