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Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Damage Microstructure: Austenite clear all

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Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
756
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Nitronic 60 cylinder. Scanning electron microscopy image of a corroded region at the external surface of the cylinder, that is austenitic. The image shows the localized corroded regions in form of pits.
1228
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
The scanning electron microscopy image of the internal surface of the tube in position 2 shows a localized corrosion region with intergranular morphology, as well a crack from the corroded region.
1237
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
Micrography of the new tube close to a region of a casting defect (shrinkage), presenting only austenitic structure with a network of primary precipitates.
351
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides
Micrographic detail of the fatigue cracking at the margin of the flange to shell fillet weld.
484
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Fatigue Crack
Aspect of the cracking after Dye Check Test (Liquid Penetrant) in the external side of the line that operates at 800°C, insulated, and presented the leakage associated to the longitudinal seam weld of the fitting. The circumferential butt weld of the fitting to a pipe did not fail. See the schematic drawing in the next figure
371
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Aspect by NDTDf - Through Wall Cracking
The micrography of the transverse section of the plate, as polished, close to the surface. The material presents intergranular corrosion and some grains were lost.
1184
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrography of the transverse section of the NEW TUBE, in the center of the thickness, showing the austenitic structure with primary carbides network.
410
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides

More from these cases

ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Aspect of a 5/16" bolt manufactured in an AISI 316 austenitic stainless steel, that was also operating inside the pressure vessel, but was not yet damaged. It is a hexagonal head bolt, 1 1/2" long, fastened with a hexagonal nut and a lock washer.
118
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Low magnification micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides.
100
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides, strain hardened. The hardness values of the material are from 200HV1 to 300HV1, that meets the class 2 of strenght (ASTM A193 B8M class 2).
79
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Strain Hardened
Detail of the strain hardened austenitic microstructure. Micrography by optical microscope, of the longitudinal section of a bolt, in the center of the thickness.
76
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Strain Hardened
Aspect of a broken 5/16" bolt that was operating inside the pressure vessel in a condition that exceeds the limits of use of the AISI 316 steel. The fracture is located close to the position where there was the bolt head and the threads were "removed" close to the fracture surface.
75
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Fracture

+8 more from this case →

ML00121 — Pitting Corrosion in a Subsea SystemM - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Aspect of the Nitronic 60 cylinder, OD 36.4mm, presenting pits at the external surface.
219
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Aspect Before AnalysisDf - External Surface
Nitronic 60 cylinder. Detailed aspect of the pitting in a low magnification microscope.
197
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface AspectDf - Pitting
Nitronic 60 cylinder. Micrography of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, equiaxial grains, and evidences of the manufacturing process by hot forming.
179
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Nitronic 60 cylinder. Micrography of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, with some aligned non metallic inclusions.
157
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Nitronic 60 cylinder. Micrographic detail of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, equiaxial grains, typical of a solution annealed condition.
136
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite

+14 more from this case →

ML00086 — Intergranular Corrosion of Sensitized 304SSM - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in the colder part of the equipment, position 1. The material presented carbide precipitation at grain boundaries (not yet fully surrounding the grains) and at this point the tube presented no internal corrosion.
338
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 2, where the temperature was higher and the carbide precipitation increased during service.
272
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 3, where intergranular and transgranular carbide precipitation occurred during service.
234
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation
The low magnification image of the internal surface of the tube, in position 2, shows several points of localized corrosion, with intergranular morphology.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
Micrography of a longitudinal section of the tube in position 2, presenting thinning by intergranular corrosion at the internal surface.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion

+3 more from this case →

ML00097 — Cast SS Tube Removed From High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
The macrography of a transverse section of the new tube shows that there are shrinkage voids close to the internal surface, that is exposed to high temperature air. The tube is a 4" diameter and 1/4" thick.
62
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Transverse Section AspectDf - Casting Structure
Micrography close to the external surface of a new tube, sound.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the External Surface
Micrography close to the internal surface of a new tube, presenting casting defects.
47
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography of the tube removed from service after 6 month, close to a region of a casting defect (shrinkage), presenting austenitic structure with a network of primary precipitates (initial stage of coarsening) and intragranular secondary precipitation.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation
The macrography of a transverse section of the tube removed from service after 6 months, with damage close to the internal tube surface. The tube is a 4" diameter and 1/4" thick.
41
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Transverse Section AspectDf - Casting Structure

+2 more from this case →

ML00050 — Fatigue Failure of a 316SS Pressure StabilizerM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Aspect of the equipment presenting a through wall cracking at the margin of the fillet weld.
142
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Aspect Before AnalysisDf - Cracking
Macrography of the welded joint between the flange and the shell, indicating the position where the cracking was detected, at 90°.
116
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Welded Joint
The shell plate micrography showed an austenitic structure.
101
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Austenite
The macrography of a transverse section of the shell to flange weld (Lepto's etch) shows that the cracking occurred through the shell plate thickness, at the margin of the fillet weld.
93
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Transverse Section AspectDf - Cracking
Fracture surface after opening the shell cracking, presenting fatigue striation. The fracture presents also foreign particles.
132
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Striation

+3 more from this case →

ML00061 — Creep in a Seam Weld of a 304H SS FittingM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Schematic drawing presenting the aspect of the cracking after Dye Check Test (Liquid Penetrant) in the external side of the line that operates at 800°C, insulated, and presented the leakage associated to the longitudinal seam weld of the fitting. The circumferential butt weld of the fitting to a pipe did not fail.
62
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Identification drawingDf - Through Wall Cracking
Aspect of the internal side of the fitting, at the longitudinal seam weld, and macrography of a transverse section showing the through wall cracks.
62
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Transverse Section
Through wall cracking in the longitudinal seam weld of the fitting. Several cracks, longitudinal to the weld, were created by the connection of voids in the weld metal, associated to a strong microstructural evolution.
191
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Cracks
Micrography of a longitudinal section of the fitting, at the base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
44
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal
Micrographic detail of the fitting base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
40
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal

+10 more from this case →

ML00015 — Intergranular Corrosion of 304SS PlateM - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Microstructure of the plate in the center of the ¼” thickness. Equiaxed austenitic grains with delta ferrite stringers and grain boundary carbide precipitation (sensitization).
303
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Microstructure of the plate in the center of the ¼” thickness. Equiaxed austenitic grains with delta ferrite stringers and grain boundary carbide precipitation (sensitization).
201
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrographic aspect of a longitudinal section of the plate, close to the surface, in a region where it was detected intergranular corrosion up to 0,5 mm depth. As polished.
188
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrographic detail of intergranular corrosion, up to 0,5 mm depth. As polished.
171
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrographic aspect of a longitudinal section of the plate, close to the surface, in a region with intergranular corrosion. Several loose grains were removed, indicating that the structure was embrittled by the intergranular corrosion.
171
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion

+5 more from this case →

ML00038 — Cast SS Tube for High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Micrography of the transverse section of the NEW TUBE, close to the external surface, showing the austenitic structure with primary carbides network.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Close to the External Surface
Macrography of the NEW TUBE, centrifugally cast, in the transverse section, presenting columnar grains close to the external surface.
50
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Kalling Etched MacroDf - Transverse Section
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects close to the external surface.
49
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Close to the External Surface
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects in the center of the thickness.
47
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Transverse Section
Micrography of the transverse section of the TUBE REMOVED FROM SERVICE, in the center of the thickness, showing the austenitic structure with primary carbides network and secondary precipitation.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation

+4 more from this case →