Sampling and Analysis

113 cases · 516 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Capture method: Optical Microscope clear all

Sampling and Analysis — sub-branches

At the Surface 37Base Metal 59Close to the External Surface 36Close to the Internal Surface 30External Surface 6Fusion Line 23General View 2Heat Affected Zone 73In the Center of the Thickness 35In the Center of the Weld 2Internal Surface 7Longitudinal Section 68Low Mag 6Microhardness Indentations 1Microhardness identations 1Radial Section 1T/4 of the external surface 2Transverse Section 33Weld Metal 80Weld Repair 4Welded Joint 10

Results

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Low magnification micrography of a strain hardened pearlitic structure, in a longitudinal section, of one 3.2mm round wire of one strand.
62
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Sample surface. Microstructure of the plate base metal, exposed to high temperature exhausting gases. Refined austenite and some cracks.
24
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Oxalic Acid Electrolytic EtchDf - Base Metal
Aged microstructure of the HP stainless steel, modified with 1%Nb, cast fitting, tubular, operating for 6 years in a furnace which design temperature is 1100°C. The material presented a network of primary carbides, white and grey, and an austenitic matrix with coalescing secondary precipitation. Some voids. The Vickers identation indicates a hardness value about 260HV 100g in the aged austenitic matrix.
492
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Microhardness identations
Micrography of a transverse section of the spring, at the surface showing pits full of deposits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
Metallographic image of a longitudinal section of the clamp (axis in the vertical direction), showing a refined ferritic perlitic structure.
34
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrography of a transverse section of the tube at the localized reduced thickness point. Close to the internal surface.
28
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Internal Surface
Micrography of a longitudinal section of the pipe, at the external pipe surface, where there is a corroded spot. The microstructure is tempered martensite and at the surface the pipe is slightly decarburized.
28
VIEW
ML00169 / Nov.2020
Drill Pipe Fracture in the Pipe Body
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - External Surface
The stub end was manufactured from a plate and the microstructure in a longitudial section shows a refined granular austenitic structure.
62
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section

More from these cases

ML00175 — Localized External Wear of a Wire RopeM - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Metallographic aspect of the wire surface in one strand external wire, showing the presence of oxides.
42
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - At the Surface
Low magnification micrography of a strain hardened pearlitic structure, in a longitudinal section, of the 1.6mm round wire in the core.
34
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Metallographic aspect of the wire surface in the core wire of the IWRC, presenting the galvanized layer.
35
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - At the Surface
ML00174 — Carburization of a 347 SS Welded JointM - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Sample surface. Microstructure of the weld metal, exposed to high temperature exhausting gases. Austeno-ferritic structure and some cracks.
20
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Oxalic Acid Electrolytic EtchDf - Weld Metal
Sample surface. Microstructure of the heat affected zone (weld metal to the left side and base metal to the right side), exposed to high temperature exhausting gases. Large austenitic grain size and cracks fully opened and filled with oxides.
24
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Oxalic Acid Electrolytic EtchDf - Heat Affected Zone
ML00173 — Welding Cracks in an Aged HP Cast FittingM - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cast fitting microstructure. Network of primary carbides and austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
As polished micrography of the fusion line presenting several microcracks . The base metal is to the top and the weld metal is to the bottom.
23
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - As polished micrographyDf - Fusion Line
ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Micrography of the transverse section of the spring wire, in the center, presenting a refined structure and segregation bands that are detected only in low magnification.
24
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
ML00171 — Corrosion Fatigue of U Bolt Pipe ClampM - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
The clamp presented several cracks, parallel, transverse to the axis. The appearance of the cracks in the metallographic section shows that some cracks propagate and growth with a irregular path.
24
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
ML00170 — MIC in Aluminum Brass TubesM - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Micrographic detail of a transverse section of the tube at the localized reduced thickness point. Close to the internal surface.
26
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Internal Surface
MIC in Aluminum Brass Tubes
2
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Close to the Internal Surface
ML00169 — Drill Pipe Fracture in the Pipe BodyM - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Micrography of a longitudinal section of the pipe, at the internal pipe surface, where the coating was detached. The strain hardening effect of the blasting is evident. The microstructure is tempered martensite and the surface is slightly decarburized.
28
VIEW
ML00169 / Nov.2020
Drill Pipe Fracture in the Pipe Body
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
Micrography of a longitudinal section of the pipe, at the internal pipe surface, where the coating was detached. The strain hardening effect of the blasting is evident. The microstructure is tempered martensite and the surface is slightly decarburized.
26
VIEW
ML00169 / Nov.2020
Drill Pipe Fracture in the Pipe Body
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
Micrographic detail of the strain hardening effect, probably generated by blasting before applying the coating. The microstructure is tempered martensite and the surface it is slightly decarburized.
23
VIEW
ML00169 / Nov.2020
Drill Pipe Fracture in the Pipe Body
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Internal Surface
Drill Pipe Fracture in the Pipe Body
2
VIEW
ML00169 / Nov.2020
Drill Pipe Fracture in the Pipe Body
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - As polished micrographyDf - External Surface
Drill Pipe Fracture in the Pipe Body
2
VIEW
ML00169 / Nov.2020
Drill Pipe Fracture in the Pipe Body
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - As polished micrographyDf - External Surface

+2 more from this case →

ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Micrography of the stub end, external side to the top, presenting multiple cracks propagating throught wall.
48
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - As polished micrographyDf - Close to the External Surface
Micrography of the stub end close to the external surface, outer diameter in the top of the image, presenting multiple cracks starting fro the surface and propagating into the thickness, through wall.
32
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Close to the External Surface
Micrography of the stub end in the middle of the thickness, outer diameter to the top of the image, presenting multiple branched cracks.
27
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - In the Center of the Thickness