Sampling and Analysis

2 cases · 9 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Damage Microstructure: Detrimental phases Capture method: Optical Microscope clear all

Sampling and Analysis — sub-branches

Close to the External Surface 1External Surface 1Heat Affected Zone 4In the Center of the Thickness 1Internal Surface 1Welded Joint 1

Results

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Micrography of a longitudinal section of the sleeve, at the external surface where there are two layers of coating. The electrolytic etch evidenced the duplex stainless steel substrate (bottom of the figure) and the weave interface of the substrate and the first thermal spray layer, about 1 mm thick, in a stainless steel. The surface layer, of tugnsten carbide, about 0.2 mm thick, is black and not clearly visible in this figure.
50
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - External Surface
Low magnification micrography of the valve at the welded joint of the body to the insert (fillet weld). The cracking was arrested at the position of this welded joint because the structures of the weld metal, insert and heat affected zones are tough (austenitic in the weld metal and insert, and free from sigma in the HAZ) .
48
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Welded Joint

More from these cases

ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Micrography of the longitudinal section of the sleeve, at the interface between the substrate and the first thermal spray layer. The substrate (bottom of the figure) shows a ferritic-austenitic microstructure and detrimental phases that look like sigma. The thermal spray layer (top of the figure) presents the non-etched stainless steel, disposed in layers, with oxides (gray) and voids (black). The substrate is deformed in a thin layer at the interface.
38
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Close to the External Surface
Micrography of the longitudinal section of the cast sleeve in the middle of the thickness. The microstructure is coarse, austenitic ferritic.
34
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - In the Center of the Thickness
Micrography of the longitudinal section of the cast sleeve, close to the internal diameter (ID). The microstructure is coarse, austenitic ferritic, and presents the same microstructure, ferritic and austenitic, all through the thickness.
21
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Internal Surface
ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrography of the valve at the welded joint of the body to the insert (fillet weld). The cracking was arrested at the position of this welded joint because the structures of the weld metal, insert and heat affected zones are tough (austenitic in the weld metal and insert, and free from sigma in the HAZ) .
46
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrographic detail of the fusion line of the welded joint of the body to the insert (fillet weld). The cracking was arrested at the position of this welded joint because the structures of the weld metal, insert and heat affected zones are tough (austenitic in the weld metal and insert, and free from sigma in the HAZ) .
39
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrography of the valve at the welded joint of the body to the insert (fillet weld). The heat affected zone shows that the sigma phase was removed, which means that the base metal was degradated and during welding the thermal cycle created a condition to remove the sigma phase (dissolve it).
38
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrographic detail of the heat affected zone of the valve to the insert joint showing that the sigma phase was removed, which means that the base metal was degradated and during welding the thermal cycle created a condition to dissolve the sigma phase.
39
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone