Scanning Electron Microscope

5 cases · 21 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Subsea Standard: A clear all

Scanning Electron Microscope — sub-branches

Fractography by SEM 8Kalling Etched Micrography by SEM 3Micrography by SEM 4Nital Etched Micrography by SEM 1Surface Aspect by SEM 5

Results

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Fractographic aspect of the stud fracture surface, by scanning electron microscopy, close to the bottom of the thread fillet. In the center of the image it is possible to see secondary cracks with intergranular morphology.
59
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
92
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Fractographic detail of the longitudinal Charpy V testpiece, broken at -46°C and presenting energy of 64J (the average energy of three tespieces was 70J). The Charpy V testpiece was removed from the center of the bar. The micromechanism is quasicleavage and the test in this direction presented energy values superior than the minimum requirement of 45J.
944
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
Nitronic 60 cylinder. Scanning electron microscopy image of a corroded region at the external surface of the cylinder, that is austenitic. The image shows the localized corroded regions in form of pits.
1228
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
Fusion line micrographic detail. The weld metal is in the right and HAZ in the left.
27
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by SEMDf - Fusion Line

More from these cases

ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Fractographic detail by scanning electron microscopy of the secondary cracks with intergranular morphology.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Secondary Cracks
Micrography of the bottom of the thread fillet, presenting secondary cracks of intergranular morphology, propagating transverse to the stud axis, but presenting longitudinal openings.
28
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by SEMDf - Cracks
ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
85
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
High magnification details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
81
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Higher magnification detail of the sigma phase by scaning electron microscopy.
76
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Fractographic aspect of the valve body fracture surface after opening the crack. The fracture micromechanism is brittle, by cleavage, with several secondary microcracks associated to the sigma phase.
54
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets
Fractographic detail of the valve body fracture surface after opening the crack. The fracture micromechanism is brittle, by cleavage, with several secondary microcracks associated to the sigma phase.
52
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets

+1 more from this case →

ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Fractography of the broken Charpy V testpiece, longitudinal, broken at -46°C and presenting energy of 64J (the average of three values was 70J). In this direction the material presented an energy value higher than the minimum requirement of 45J.
109
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
Fractography of the Charpy V testpiece, transverse section, broken at -46°C and presenting energy of 20J (the average of three results was 33J). The coarse structure and the alignement created a condition for low energy results in this specific direction, and the material did not present the minimum requirement of 45J.
103
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
ML00121 — Pitting Corrosion in a Subsea SystemM - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Nitronic 60 cylinder. Scanning electron microscopy image of a corroded region at the external surface of the cylinder, that is austenitic. The image shows the structure revealed by dissolution of the material (inside the pits) evidencing the strain hardened layer that is presented at the cylinder surface due to the manufacturing process.
106
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
Nitronic 60 cylinder. Scanning electron microscopy image detail of a corroded region inside a pitting showing the etched structure (strain hardened austenitic structure).
103
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
Nitronic 60 cylinder. Scanning electron microscopy image of a corroded region in a pit, at the external surface of the cylinder. The corrosion (dissolution) revealed the strain hardened layer at the surface.
96
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
17-4 PH rod. Surface aspect by scanning electron microscopy showing a region where the passivation layer was destroyed and a pitting was in the begining.
86
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Pitting
ML00045 — Subsea Tubular F6NM Martensitic SSM - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Micrographic detail of the base metal tempered martensite.
24
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by SEMDf - Base Metal
Micrographic detail of the weld metal tempered martensitic microstructure.
25
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by SEMDf - Weld Metal