Scanning Electron Microscope

14 cases · 57 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Subsea Condition: Damage clear all

Scanning Electron Microscope — sub-branches

Fractography by SEM 39Micrography by SEM 4Nital Etched Micrography by SEM 1Surface Aspect by SEM 13

Results

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The fractographic aspect of the broken bolt shows intergranular micromechanism, typical of a hydrogen embrittlement condition for this aged martensitic material.
88
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
Fractographic aspect of the stud fracture surface, by scanning electron microscopy, close to the bottom of the thread fillet. In the center of the image it is possible to see secondary cracks with intergranular morphology.
59
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
92
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Aspect of the fracture surface of the bolt, after cleaning with a plastic brush. Although there is a layer of oxides it is possible to see the intergranular morphology of the fracture, typical of a hydrogen embrittlement mechanism.
1154
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
Fractographic detail of the longitudinal Charpy V testpiece, broken at -46°C and presenting energy of 64J (the average energy of three tespieces was 70J). The Charpy V testpiece was removed from the center of the bar. The micromechanism is quasicleavage and the test in this direction presented energy values superior than the minimum requirement of 45J.
944
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
Nitronic 60 cylinder. Scanning electron microscopy image of a corroded region at the external surface of the cylinder, that is austenitic. The image shows the localized corroded regions in form of pits.
1228
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
Aspect by scanning electron microscopy of the cracking at the external surface of the fitting.
47
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Microscopic detail of the fracture surface in the position where the fracture is intergranular, probably due to the MIC attack creating an embrittled condition of the material.
31
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture

More from these cases

ML00139 — Hydrogen Fracture of a 17-4 PH Allen BoltM - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Fractographic aspect by scanning electron microscopy, close to the surface the broken bolt, presenting intergranular fracture micromechanism.
79
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
Microscopic detail of the intergranular fracture close to the bolt surface.
71
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
Fractographic aspect by scanning electron microscopy, in the center of the broken bolt, presenting transgranular fracture micromechanism.
45
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Cleavage Facets
Fractographic detail of the transgranular fracture micromechanism, brittle.
43
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Cleavage Facets
ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Fractographic detail by scanning electron microscopy of the secondary cracks with intergranular morphology.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Secondary Cracks
Micrography of the bottom of the thread fillet, presenting secondary cracks of intergranular morphology, propagating transverse to the stud axis, but presenting longitudinal openings.
28
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by SEMDf - Cracks
ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
85
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
High magnification details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
81
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Higher magnification detail of the sigma phase by scaning electron microscopy.
76
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Fractographic aspect of the valve body fracture surface after opening the crack. The fracture micromechanism is brittle, by cleavage, with several secondary microcracks associated to the sigma phase.
54
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets
Fractographic detail of the valve body fracture surface after opening the crack. The fracture micromechanism is brittle, by cleavage, with several secondary microcracks associated to the sigma phase.
52
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets

+1 more from this case →

ML00126 — Hydrogen Fracture of Subsea Allen BoltsM - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Detailed aspect of the fracture surface of the bolt, evidencing the intergranular morphology of the fracture (although with an oxide scale), typical of a hydrogen embrittlement mechanism.
114
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Fractography of the broken Charpy V testpiece, longitudinal, broken at -46°C and presenting energy of 64J (the average of three values was 70J). In this direction the material presented an energy value higher than the minimum requirement of 45J.
109
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
Fractography of the Charpy V testpiece, transverse section, broken at -46°C and presenting energy of 20J (the average of three results was 33J). The coarse structure and the alignement created a condition for low energy results in this specific direction, and the material did not present the minimum requirement of 45J.
103
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - Fractography by SEMDf - Broken Testpiece
ML00121 — Pitting Corrosion in a Subsea SystemM - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Nitronic 60 cylinder. Scanning electron microscopy image of a corroded region at the external surface of the cylinder, that is austenitic. The image shows the structure revealed by dissolution of the material (inside the pits) evidencing the strain hardened layer that is presented at the cylinder surface due to the manufacturing process.
106
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
Nitronic 60 cylinder. Scanning electron microscopy image detail of a corroded region inside a pitting showing the etched structure (strain hardened austenitic structure).
103
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
Nitronic 60 cylinder. Scanning electron microscopy image of a corroded region in a pit, at the external surface of the cylinder. The corrosion (dissolution) revealed the strain hardened layer at the surface.
96
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
17-4 PH rod. Surface aspect by scanning electron microscopy showing a region where the passivation layer was destroyed and a pitting was in the begining.
86
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Pitting
ML00094 — MIC of a Subsea Hydraulic LineM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Aspect by scanning electron microscopy of the cracking at the external surface of the fitting. Interesting to observe that the cracks are deformed.
39
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - External Surface
Aspect by scanning electron microscopy of the cracking at the internal surface of the fitting.
36
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Internal Surface
Aspect by scanning electron microscopy of the cracking at the internal surface of the fitting. Interesting to observe multiple cracks with brittle characteristic.
39
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Internal Surface
The internal surface of the fitting presents multiple cracks not associated to pitting.
39
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Internal Surface
The through wall cracking was opened by citting the two sides and the aspect was characterized by SEM. Although there was a film at the fracture surface, probably because the fitting was removed from service some time after it was leaking, the fracture micromechanism is by quasecleavage, typical of a stress corrosion cracking.
56
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
ML00080 — MIC of Stacking Disc SpringsM - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Microscopic detail of the fracture surface in the position where the fracture is intergranular, probably due to the MIC attack creating an embrittled condition of the material. A surface film is evident in this position suggesting that the fracture remained open and exposed to the environment during a certain time before the failure was detected.
29
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Fracture micromechanisms. Intergranular fracture in the top of the figure (close to the groove) and transgranular fracture in the bottom of the figure, where the mechanism changed to transgranular by quasecleavage.
27
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Microscopic detail of the fracture surface where it is transgranular, by quasecleavage. This aspect is similar to the one expected for this high strenght material without any embrittlement.
27
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
Microscopic detail of the fracture surface where it is transgranular, by quasecleavage. This aspect is similar to the one expected for this high strenght material without any embrittlement.
26
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture