Optical Microscope

12 cases · 107 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Fabrication Defect Standard: A clear all

Optical Microscope — sub-branches

As polished micrography 1Kalling Etched Micrography by OM 17Micrography by OM 2NaOH Electrolytic Etched Micro 6Nital Etched Micrography by OM 81

Results

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Quenched and tempered structure of the F22 steel forging, presenting about 230HV10 average hardness.
133
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
BASE METAL SURFACE - Ferritic structure, grain refined.
90
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Base Metal
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure.
55
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
74
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a transverse section of the pipe, external diameter 33.4 mm schedule XXS, in the center of the 9.1 mm thickness. The structure is predominantly ferritic. Small amount of pearlite.
556
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Predominantly Ferritic
Micrography of a transverse section of the pipe, external diameter 26.7 mm, in the center of the 7.85mm thickness. Refined structure but not uniform. Ferrite and pearlite.
512
VIEW
ML00111 / Dec.2017
3/4" XXS Pipe Not Qualified for Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the forging lap defect that appears at the nut surface like a crack, filled with oxides. The nut presented a martensitic structure in the center of the nut, but in the regions adjacent to the defect the structure is ferritic-bainitic due to decarburization. There are several globular oxides (grey spots) that became entrapped during the forging.
654
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Crack
The micrographic aspect of the cracks in a section transverse to the weld (the removed sample), shows that there are cracks with different sizes, the larger are filled with products that indicate they were opened for longer times.
67
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking

More from these cases

ML00178 — Cold cracks in Cr-Mo Welded ForgingM - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Tempered martensitic structure for the F22 forging base metal.
129
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Tempered Martensite
Fusion line of the forging side, in the cap, showing the weld metal (to the top of the image) and the base metal (to the bottom of the image). The heat affected zone hardness is about 270HV10.
108
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Grain coarsened martensitic heat affected zone. The hardness values about 270HV10 indicates that the joint was post welding heat treated (PWHT).
97
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Detail of the quenched and tempered martensitic structure at the heat affected zone.
64
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Tempered Martensite
The columnar grains of the weld metal in the cap presented a martensitic structure.
60
VIEW
ML00178 / Jan.2022
Cold cracks in Cr-Mo Welded Forging
M - CrMo SteelP - ForgingAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Weld Metal

+1 more from this case →

ML00177 — Cr-Mo Seam Welded TubeM - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
BASE METAL SURFACE - The micrography (transverse to the tube) presents the ferritic/pearlitic/bainitic structure.
75
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Granular structure
BASE METAL SURFACE - The microstructure of the base metal is ferritic/pearlitic/bainitic.
74
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Grain refined structure
HAZ SURFACE
72
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Last Bead HAZ
HAZ SURFACE
66
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Last Bead HAZ
HAZ SURFACE
55
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Bainitic HAZ

+18 more from this case →

ML00148 — Brittle Fracture of a 420 SS Barrel NutM - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Microstructural aspect of a longitudinal section of the nut, in the middle of the thickness. Martensitic structure, banded.
46
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Microstructural detail of the banded structure. The rough aspect of the band is created by the carbides (better seen in the higher magnification image) in the segregation band.
38
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrographic detail of the nut longitudinal section presenting the large carbides (white islands) in the segregation band, and small precipitates all through the martensite matrix, indicating that this high carbon steel was tempered in a high temperature. The 36HRc hardness also confirms this high tempering temperature.
39
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Martensite
Vickers microhardness identations using 100 grams. In a position out of the band (top line). Values from left to right, 380HV; 390HV and 394HV. In a position inside the band (bottom line). Values from left to right, 433HV, 483HV and 473 HV.
33
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure. It is possible to see that the contact pressure in the thread caused a surface plastically deformation.
24
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure

+6 more from this case →

ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
61
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. The ferrite amount, measured by metallographic method, manual counting, is 59%.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. The average austenite spacing is 80 microns, a lot larger than the maximum allowed in the specification, of 30 microns. No detrimental phases were identified at the ferrite/austenite interfaces, but the ferrite phase presented a rough aspect. Higher magnification analysis would be required to identify precipitation.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrographic detail of the ferrite and austenite structure in the transverse section of the forged bar, in the center of the thickness.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the ferrite and austenite structure in the longitudinal section of the forged bar, in the center of the thickness.
55
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
ML00112 — 1" XXS Pipe Not Qualified For Low TempM - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Micrography of a transverse section of the pipe, close to the external surface (OD). The pipe presented a predominatly ferritic structure.
43
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of a transverse section of the pipe, close to the external surface (OD). The pipe presented a 0.2 mm decarburized layer, fully ferritic.
35
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of a transverse section of the pipe, close to the external surface (OD). The pipe presented a predominatly ferritic structure.
31
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Predominantly Ferritic
Micrography of a transverse section of the pipe, close to the internal surface (ID). The pipe presented a predominatly ferritic structure.
29
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
Micrography of a transverse section of the pipe, close to the internal surface (ID). The pipe presented a predominatly ferritic structure.
22
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface

+2 more from this case →

ML00111 — 3/4" XXS Pipe Not Qualified for Low TempM - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Micrography of a transverse section of the pipe, close to the internal surface (ID). Refined structure. Ferrite and pearlite.
64
VIEW
ML00111 / Dec.2017
3/4" XXS Pipe Not Qualified for Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
Micrography of a transverse section of the pipe, close to the internal surface (ID). Refined structure, but not uniform. Ferrite and pearlite. The pearlite colonies appear in a network.
45
VIEW
ML00111 / Dec.2017
3/4" XXS Pipe Not Qualified for Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
Micrography of a transverse section of the pipe, close to the internal surface (ID). Refined structure. Ferrite and pearlite. The structure is not uniform. There is a large variation in the ferritic grain size and the pearlite colonies appear forming a network.
39
VIEW
ML00111 / Dec.2017
3/4" XXS Pipe Not Qualified for Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of a transverse section of the pipe, close to the external surface (OD). Refined structure. Ferrite and pearlite.
33
VIEW
ML00111 / Dec.2017
3/4" XXS Pipe Not Qualified for Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of a transverse section of the pipe, close to the external surface (OD). Refined structure. Ferrite and pearlite.
34
VIEW
ML00111 / Dec.2017
3/4" XXS Pipe Not Qualified for Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the External Surface

+2 more from this case →

ML00099 — Forging Defect in a Cadmium Plated NutM - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Micrography of the nut in a section transverse to the surface indication. There are several microcracks (parallel and perpendicular to the nut surface) filled with oxides. The nut presented a martensitic microstructure in the center of the thickness and a ferritic-bainitic microstructure at surface and adjacent to the defect, due to decarburization occurred during high temperature forging.
130
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Crack
Micrographic detail of the lap at the nut surface, as polished. The 20 microns cadmium layer is evident, penetrating in the lap.
46
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - As polished micrographyDf - Lap
Tempered martensitic microstructure in the transverse section of the nut, in the center. The material presented 29 HRc that is typical of a quenched and tempered steel.
30
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Ferritic-bainitic microstructure in the transverse section of the nut, at the surface where the cadmium plate is also evident. The nut surface presents a decarburized layer and the lap entrapped oxides.
30
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Bainitic Ferrite
ML00071 — Reheating Cracking of a CrMo Vessel WeldM - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Micrographic aspect of opened cracks, filled with oxides.
63
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Micrographic details of opened cracks, filled with oxides.
56
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Micrographic aspect of thin cracks.
59
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Micrographic details of thin cracks.
63
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracks