Optical Microscope

11 cases · 79 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Corrosion Standard: A clear all

Optical Microscope — sub-branches

Kalling Etched Micrography by OM 4Micrography by OM 7Micrography by OM using A262 Method A 22NaOH Electrolytic Etched Micro 6Nital Etched Micrography by OM 33Oxalic Acid Electrolytic Etch 7

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Micrography of the thread at the valve body surface, showing localized dissolution of the thread.
73
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Corroded Thread
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
756
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Nitronic 60 cylinder. Micrography of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, equiaxial grains, and evidences of the manufacturing process by hot forming.
179
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in the colder part of the equipment, position 1. The material presented carbide precipitation at grain boundaries (not yet fully surrounding the grains) and at this point the tube presented no internal corrosion.
338
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrography of the shell plate in the longitudinal section. Ferritic-perlitic microstructure.
96
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Typical branched stress corrosion cracks in a low carbon steel, ferritic-pertlitic structure. The cracks are filled with corrosion products.
771
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Branched Cracks
A small sample was removed from the steam drum and the micrography shows that the cracks are intergranular (previous austenite) and located in the weld metal.
285
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
The micrography of the transverse section of the plate, as polished, close to the surface. The material presents intergranular corrosion and some grains were lost.
1184
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion

More from these cases

ML00184 — Dissimilar Steels in a Threaded ConnectionM - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Micrography of the valve body carbon steel thread, in the valley. Ferritic-bainitic structure.
77
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Transverse Section
Micrographic detail of the valve body carbon steel thread, in the valley. Ferritic-bainitic structure.
69
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Bainitic Ferrite
Micrography of the valve body carbon steel thread, in the peak. Ferritic-bainitic structure.
64
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Corroded Thread
Micrographic detail of the valve body carbon steel thread, in the peak. Ferritic-bainitic structure.
55
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Corroded Thread
Cross-section near a threaded surface showing an acicular matrix structure bordered by a dark, layered corrosion/oxide band along the thread root.
1
VIEW
ML00184 / Apr.2023
Dissimilar Steels in a Threaded Connection
M - Low Carbon SteelP - ForgingAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Oxide Layer
ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Low magnification micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides.
100
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides, strain hardened. The hardness values of the material are from 200HV1 to 300HV1, that meets the class 2 of strenght (ASTM A193 B8M class 2).
79
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Strain Hardened
Detail of the strain hardened austenitic microstructure. Micrography by optical microscope, of the longitudinal section of a bolt, in the center of the thickness.
76
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Strain Hardened
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were fully cracked by the stress corrosion mechanism.
58
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Optical micrography of a longitudinal section of the fractured bolt, under the thread, showing stress corrosion cracks through the section.
46
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks

+2 more from this case →

ML00121 — Pitting Corrosion in a Subsea SystemM - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Nitronic 60 cylinder. Micrography of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, with some aligned non metallic inclusions.
157
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Nitronic 60 cylinder. Micrographic detail of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, equiaxial grains, typical of a solution annealed condition.
136
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Nitronic 60 cylinder. Micrography of the longitudinal section close to the surface, presenting a fully austenitic microstructure, with a shadow close to the external surface that is associated to a small layer of strain hardened structure (deformation twins).
133
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Nitronic 60 cylinder. Micrography of the longitudinal section close to the surface, presenting a fully austenitic microstructure, with a 0.15mm layer of strain hardened structure (deformation twins).
120
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Nitronic 60 cylinder. Micrographic detail of the longitudinal section close to the surface, presenting a fully austenitic microstructure, with a layer of strain hardened structure (deformation twins).
113
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Strain Hardened

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ML00086 — Intergranular Corrosion of Sensitized 304SSM - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 2, where the temperature was higher and the carbide precipitation increased during service.
272
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 3, where intergranular and transgranular carbide precipitation occurred during service.
234
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation
Micrography of a longitudinal section of the tube in position 2, presenting thinning by intergranular corrosion at the internal surface.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion
Micrographic detail of the intergranular corrosion at the internal surface of the tube in position 2. Several grains were already removed by the corrosion.
171
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion
Micrography of a longitudinal section of the tube in position 3, at the internal surface. Although there is a strong precipitation, both intergranular and transgranular, the tube did not corrode at this point.
144
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation

+1 more from this case →

ML00019 — Transgranular SCC in Boiler Steam DrumM - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Micrographic detail of the shell plate in the longitudinal section. Ferritic-perlitic microstructure.
89
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of the cracking showing the branched nature, typical of a stress corrosion cracking. The cracks started from the internal surface of the steam drum.
94
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Branched Cracks
Micrographic detail of the cracking showing the branched nature, typical of a stress corrosion cracking. The cracks presented a transgranular morphology
86
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Transgranular Crack
Micrographic detail of the transgranular stress corrosion cracking.
80
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Transgranular Crack
Micrographic detail of the transgranular stress corrosion cracking.
157
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Transgranular Crack
ML00018 — SCC in Boiler Steam DrumM - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Ferritic perlitic structure of the shell plate.
207
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of the crack at the internal surface of the steam drum. The shell plate presents a ferritic perlitic structure.
162
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Branched Cracks
Micrography of a crack, in a sample as polished, presenting the opened crack.
144
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Micrography by OMDf - Branched Cracks
Stress corrosion cracks propagating in the ferritic-perlitic structure.
120
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Branched Cracks
Micrography of a crack, as polished, presenting the cracks filled with corrosion products.
100
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Micrography by OMDf - Branched Cracks

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ML00020 — Intergranular SCC in Boiler Steam Drum RepairM - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
The micrography of the small sample removed from the steam drum shows that the cracks are intergranular (previous austenite) and located in the weld metal.
274
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
Secondary cracks in the weld metal showing an intergranular morphology. Stress Corrosion Cracking.
249
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
Detail of the secondary cracks in the weld metal with intergranular morphology. Stress Corrosion Cracking.
251
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
Detail of the intergranular stress corrosion cracking of the drum shell weld repair.
217
VIEW
ML00020 / Apr.2017
Intergranular SCC in Boiler Steam Drum Repair
M - Low Carbon SteelP - Repair WeldAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
ML00015 — Intergranular Corrosion of 304SS PlateM - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Microstructure of the plate in the center of the ¼” thickness. Equiaxed austenitic grains with delta ferrite stringers and grain boundary carbide precipitation (sensitization).
303
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Microstructure of the plate in the center of the ¼” thickness. Equiaxed austenitic grains with delta ferrite stringers and grain boundary carbide precipitation (sensitization).
201
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrographic aspect of a longitudinal section of the plate, close to the surface, in a region where it was detected intergranular corrosion up to 0,5 mm depth. As polished.
188
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrographic detail of intergranular corrosion, up to 0,5 mm depth. As polished.
171
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrographic aspect of a longitudinal section of the plate, close to the surface, in a region with intergranular corrosion. Several loose grains were removed, indicating that the structure was embrittled by the intergranular corrosion.
171
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion

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