Optical Microscope

8 cases · 75 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Oil and Gas Standard: AISI clear all

Optical Microscope — sub-branches

As polished micrography 7Nital Etched Micrography by OM 61Oxalic Acid Electrolytic Etch 7

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Micrography of a transverse section of the spring, at the surface showing pits full of deposits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
756
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
The longitudinal section of the shaft, in the center of the thickness, shows a coarse structure, and a ferritic/bainitic structure with pearlite islands.
97
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of the weld metal with islands of a coarse ferritic structure, degradated (recristalized) from an acicular morphology during to the long heat treatment cycle in high temperature. The post welding heat treatment (PWHT) was conducted during 12 hours at 640°C.
700
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Micrography of the longitudinal section of the stud presenting a tempered martensite structure, slightly banded. Hardness 45 HRc.
33
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the 4130 steel, normalized and tempered. The structure is sligthly banded (segregated) and the average hardness level is 20 HRc.
92
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of the forging lap defect that appears at the nut surface like a crack, filled with oxides. The nut presented a martensitic structure in the center of the nut, but in the regions adjacent to the defect the structure is ferritic-bainitic due to decarburization. There are several globular oxides (grey spots) that became entrapped during the forging.
654
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Crack
Micrography of the external surface of the tubular equipment, close to the fracture position (it is to the top of the figure), showing multiple cracks, typical of a corrosion fatigue mechanism.
861
VIEW
ML00082 / Dec.2017
Corrosion Fatigue of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Multiple cracks

More from these cases

ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Micrographic detail of the transverse section of the spring, at the surface, showing the pits full of corrosion deposits.
31
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Surface Deposits
Micrographic detail of spring surface, showing the pits full of corrosion deposits and a small decarburized layer (probably from the manufacturing processes).
30
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Decarburized Surface
Micrography of a longitudinal section of the spring, at the surface, indicating that there are multiple intergranular cracks initiating from the pit.
26
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - As polished micrographyDf - Multiple cracks
Micrographic aspect of the multiple intergranular cracks, initiating from the bottom of a pit.
25
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - As polished micrographyDf - Intergranular Cracking
Micrographic detail of the intergranular cracks, initiating from the bottom of a pit.
29
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - As polished micrographyDf - Intergranular Cracking

+3 more from this case →

ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Low magnification micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides.
100
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides, strain hardened. The hardness values of the material are from 200HV1 to 300HV1, that meets the class 2 of strenght (ASTM A193 B8M class 2).
79
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Strain Hardened
Detail of the strain hardened austenitic microstructure. Micrography by optical microscope, of the longitudinal section of a bolt, in the center of the thickness.
76
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Strain Hardened
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were fully cracked by the stress corrosion mechanism.
58
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Optical micrography of a longitudinal section of the fractured bolt, under the thread, showing stress corrosion cracks through the section.
46
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks

+2 more from this case →

ML00152 — Low Alloy Steel Pump ShaftM - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
The coarse structure in the center of the shaft thickness is evidenced by free ferrite islands at the previous austenite grains. The presence of a pearlitic structure evidences the slow cool of the material.
85
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Coarse Structure
The longitudinal section of the shaft, at the surface, also shows a coarse structure, and a ferritic/bainitic structure with pearlite islands. There is only a small refining in the previous austenite grain boundaries, indicating that the material was not heat treated.
75
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
The longitudinal section of the shaft, at the surface, presenting only a small refining in the previous austenite grain boundaries than in the center, indicating that the material was slowed colled from forming and not heat treated.
67
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Micrographic detail of the pearlitic structure at the surface of the shaft thickness.
69
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Pearlite
ML00129 — Non qualified WPS for High Strength SteelM - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Micrography of the weld metal, at the face, presenting regions of large ferritic grains. The acicular ferrite structure in the columnar (previous austenitic) grains has suffered degradation due to the long heat treatment cycle (12 hours) in high temperature.
97
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Weld Metal
Micrography of the weld metal, at the face, presenting regions of large ferritic grains. The acicular ferrite has suffered degradation due to the long heat treatment cycle (12 hours) in a temperature of 640°C, that is higher than the recommended for the D2 filler metal.
78
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Weld Metal
Micrography of the base metal, in low magnification, showing regions of segregations in a quenched and tempered martensitic structure.
52
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the base metal showing a quenched and tempered martensitic structure. The base metal adopted in the test coupon presented a hardness level of 217HB (Brinell hardness of the certificate) and after the PWHT cycle the measured base metal hardness is 224 HV10.
59
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of the base metal structure, quenched and tempered martensite. The base metal adopted in the test coupon presented a hardness level of 217HB (Brinell hardness of the certificate) and after the PWHT cycle the measured base metal hardness is 224 HV10.
51
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Martensite

+12 more from this case →

ML00127 — Hydrogen Cracks of Cadmium Plated StudsM - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the stud presenting a tempered martensite structure in the center of the thickness.
33
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Low magnification micrographic image of the stud thread, in the longitudinal section, showing the segregation lines of the steel cut at the thread indicating it was machined.
30
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrographic detail of the stud at the thread bottom.
27
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrographic detail of the thread top, showing that the thread was machined.
29
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrography of the longitudinal section of the stud showing internal cracks, secondary (not the cracks that opened the fracture). It is evident that the cracking from the thread fillet, of a ductile aspect, presented a different aspect than the internal cracks, of a brittle aspect.
31
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Cracks

+4 more from this case →

ML00102 — AISI 4130 Forging Welded and OverlaidM - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Micrography of the 4130 steel, normalized and tempered. The microstructure is bainitic.
88
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of the bainitic structure of the 4130 steel, normalized and tempered.
87
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Bainite
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) of the Inconel overlay (white because it was not etched with the Nital). The structure is ferritic/bainitic because the overlay was conducted in two layers, and all the HAZ was reheated during welding.
66
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the tubular 4130 forging at the heat affected zone (HAZ) of the Inconel overlay (white because it was not etched with the Nital). The structure is ferritic/bainitic because the overlay was conducted in two layers, and all the HAZ was reheated during welding.
61
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the bainitic heat affected zone (HAZ) of 4130 forging at the Inconel overlay.
50
VIEW
ML00102 / May.2018
AISI 4130 Forging Welded and Overlaid
M - Low Alloy SteelP - CladdingAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Bainitic Ferrite

+6 more from this case →

ML00099 — Forging Defect in a Cadmium Plated NutM - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Micrography of the nut in a section transverse to the surface indication. There are several microcracks (parallel and perpendicular to the nut surface) filled with oxides. The nut presented a martensitic microstructure in the center of the thickness and a ferritic-bainitic microstructure at surface and adjacent to the defect, due to decarburization occurred during high temperature forging.
130
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Crack
Micrographic detail of the lap at the nut surface, as polished. The 20 microns cadmium layer is evident, penetrating in the lap.
46
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - As polished micrographyDf - Lap
Tempered martensitic microstructure in the transverse section of the nut, in the center. The material presented 29 HRc that is typical of a quenched and tempered steel.
30
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Ferritic-bainitic microstructure in the transverse section of the nut, at the surface where the cadmium plate is also evident. The nut surface presents a decarburized layer and the lap entrapped oxides.
30
VIEW
ML00099 / Jan.2018
Forging Defect in a Cadmium Plated Nut
M - Medium Carbon SteelP - NutAp - PipingCd - Fabrication Defect
Cm - Nital Etched Micrography by OMDf - Bainitic Ferrite
ML00082 — Corrosion Fatigue of a Drilling ToolM - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Corrosion Fatigue
Micrographic aspect of the martensitic structure at the longitudinal section.
60
VIEW
ML00082 / Dec.2017
Corrosion Fatigue of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the quenched and tempered structure. Longitudinal section.
51
VIEW
ML00082 / Dec.2017
Corrosion Fatigue of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of the quenched and tempered structure. Longitudinal section. Sligthly banded.
45
VIEW
ML00082 / Dec.2017
Corrosion Fatigue of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Banded Structure
As polished micrography of the external surface of the tubular equipment, close to the fracture position (it is to the top of the figure), showing corrosion fatigue cracks. These are multiple cracks, paralel to the main fracture, slightly branched and fully filled with oxides.
51
VIEW
ML00082 / Dec.2017
Corrosion Fatigue of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - As polished micrographyDf - Multiple cracks
As polished micrography of the external surface of the tubular equipment, close to the fracture position (it is to the top of the figure), showing corrosion fatigue cracks. These are multiple cracks, paralel to the main fracture, slightly branched and fully filled with oxides.
43
VIEW
ML00082 / Dec.2017
Corrosion Fatigue of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - As polished micrographyDf - Multiple cracks

+2 more from this case →