Nital Etched Micrography by OM

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Micrographic detail of the weld metal with islands of a coarse ferritic structure, degradated (recristalized) from an acicular morphology during to the long heat treatment cycle in high temperature. The post welding heat treatment (PWHT) was conducted during 12 hours at 640°C.
700
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Micrographic aspect, after Nital etching, of the longitudinal section of the cylinder, at the surface, in a region where the damage is in the begining. There are two layers at the surface. A first Ni layer, 160 microns thick and 300HV average hardness, over the low carbon steel substrate, 200HV average hardness, and a chromium plated layer, 250 microns thick and 1100HV average hardness.
59
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Corrosion
Micrography of the longitudinal section of the stud presenting a tempered martensite structure, slightly banded. Hardness 45 HRc.
33
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the longitudinal section of the bolt showing a martensitic structure, with segregation bands evidenced by the chemical etch.
99
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a longitudinal section of the bolt in the center of the thickness, presenting a ferritic pearlitic structure with elongated grains due to the forming process, without later heat treatment.
173
VIEW
ML00120 / Jun.2018
Ductile Rupture of a Carbon Steel Eye Bolt
M - Low Carbon SteelP - FastenerAp - AutomotiveCd - Overload
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of the plate in a longitudinal section, presenting a typical ferritic pearlitic structure, banded. The plate is 22 mm thick.
182
VIEW
ML00119 / Feb.2018
Thermal Fatigue of a Marine Boiler
M - Low Carbon SteelP - Fabrication WeldAp - ShipCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a longitudinal section of the core wire, 2.0 mm diameter, in the center of the thickness, showing a strain hardened structure, aligned.
113
VIEW
ML00117 / Jan.2018
High Carbon Steel Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of the pin close to the interface with the spray and fuse layer. Transverse section. The fuse was conducted in high temperature and the pin was cooled very slowly, forming a ferritic-perlitic structure even for this high hardenability base metal.
35
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite

More from these cases

ML00129 — Non qualified WPS for High Strength SteelM - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Micrography of the weld metal, at the face, presenting regions of large ferritic grains. The acicular ferrite structure in the columnar (previous austenitic) grains has suffered degradation due to the long heat treatment cycle (12 hours) in high temperature.
96
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Weld Metal
Micrography of the weld metal, at the face, presenting regions of large ferritic grains. The acicular ferrite has suffered degradation due to the long heat treatment cycle (12 hours) in a temperature of 640°C, that is higher than the recommended for the D2 filler metal.
78
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Weld Metal
Micrography of the base metal, in low magnification, showing regions of segregations in a quenched and tempered martensitic structure.
52
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the base metal showing a quenched and tempered martensitic structure. The base metal adopted in the test coupon presented a hardness level of 217HB (Brinell hardness of the certificate) and after the PWHT cycle the measured base metal hardness is 224 HV10.
59
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of the base metal structure, quenched and tempered martensite. The base metal adopted in the test coupon presented a hardness level of 217HB (Brinell hardness of the certificate) and after the PWHT cycle the measured base metal hardness is 224 HV10.
51
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Martensite

+12 more from this case →

ML00128 — MIC of a Stored Hydraulic CylinderM - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Micrographic detail of the longitudinal section of the cylinder, at the surface, in a region where the Cr layer is detaching.
56
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Corrosion
Micrographic aspect of the longitudinal section of the cylinder steel substrate, presenting a ferritic-pearlitic structure.
207
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the ferritic-pearlitic structure of the cylinder steel substrate.
41
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of the longitudinal section of the cylinder , at the surface, where it was not yet damaged. The steel substrate is in the bottom of the figure, the Ni layer is in the center and the Cr layer is in the top of the figure.
38
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Ni layer
Micrography of the interface between the steel substrate and the first Ni layer. The Ni layer, 160 microns thick and 300HV hardness, is uniform and presents no discontinuities.
37
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Ni layer

+1 more from this case →

ML00127 — Hydrogen Cracks of Cadmium Plated StudsM - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the stud presenting a tempered martensite structure in the center of the thickness.
32
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Low magnification micrographic image of the stud thread, in the longitudinal section, showing the segregation lines of the steel cut at the thread indicating it was machined.
30
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrographic detail of the stud at the thread bottom.
26
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrographic detail of the thread top, showing that the thread was machined.
29
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrography of the longitudinal section of the stud showing a crack from the thread fillet, of a ductile aspect, opened during torque.
30
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Fracture

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ML00126 — Hydrogen Fracture of Subsea Allen BoltsM - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the bolt at the bottom of the thread fillet, showing the uniform martensitic structure, not strain hardened.
90
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Uniform Structure
Micrography of the longitudinal section of the bolt at the top of the thread fillet, showing a small circunferential cracking typically of a rolling process to manufacture the thread. The thread presented no evidences of plastic deformation suggesting that the heat treatment was applied later. It is important to mention that this cracking presented no influence in the fracture of the bolt.
101
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Rolled Thread
Micrography of the longitudinal section of the bolt in the center of the thickness (ND 5/8") showing a uniform martensitic structure.
67
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the martensitic structure, uniform in the longitudinal section of the bolt, in the center of the thickness (ND 5/8"). The hardness values of the bolts varied from 39 to 41 HRc.
63
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography, after NItal etching, of the longitudinal section of the bolt, at the fracture (top of the figure), starting from the bottom of the thread (to the left side of the figure). The presence of the coating at the bolt surface shows that the fracture occurred without corrosion.
56
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Fracture

+2 more from this case →

ML00120 — Ductile Rupture of a Carbon Steel Eye BoltM - Low Carbon SteelP - FastenerAp - AutomotiveCd - Overload
Micrographic detail of the ferritic pearlitic structure, with grains sligthly elongated.
156
VIEW
ML00120 / Jun.2018
Ductile Rupture of a Carbon Steel Eye Bolt
M - Low Carbon SteelP - FastenerAp - AutomotiveCd - Overload
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of a longitudinal section of the bolt at the bottom of the thread fillet, presenting a plastically deformed ferritic pearlitic structure in a very small extension from the surface (about 0.1mm). This analysis was conducted in a position far from the failure and the structure was created by the cold forming process to manufacture the thread.
151
VIEW
ML00120 / Jun.2018
Ductile Rupture of a Carbon Steel Eye Bolt
M - Low Carbon SteelP - FastenerAp - AutomotiveCd - Overload
Cm - Nital Etched Micrography by OMDf - Rolled Thread
Micrographic detail of a longitudinal section of the bolt at the bottom of the thread fillet, presenting a plastically deformed ferritic pearlitic structure. This analysis was conducted far from the failure and the structure was created by the cold forming process to manufacture the thread.
147
VIEW
ML00120 / Jun.2018
Ductile Rupture of a Carbon Steel Eye Bolt
M - Low Carbon SteelP - FastenerAp - AutomotiveCd - Overload
Cm - Nital Etched Micrography by OMDf - Strain Hardened
Micrography of a longitudinal section of the bolt at the thread fillet adjacent to the fracture, presenting a ductile cracking from the bottom of the fillet, propagating with a strong plastic deformation. The deformation lines of the cold formed process (thread cold rolling) are also deformed by the cracking propagation.
141
VIEW
ML00120 / Jun.2018
Ductile Rupture of a Carbon Steel Eye Bolt
M - Low Carbon SteelP - FastenerAp - AutomotiveCd - Overload
Cm - Nital Etched Micrography by OMDf - Ductile Crack
Micrographic detail of a longitudinal section of the bolt at the bottom of the thread fillet adjacent to the fracture, presenting a ductile cracking propagating with a plastic deformation. The deformation lines of the cold formed process are also deformed by the cracking propagation and there are some other small secondary cracks at 90° from the principal cracking.
133
VIEW
ML00120 / Jun.2018
Ductile Rupture of a Carbon Steel Eye Bolt
M - Low Carbon SteelP - FastenerAp - AutomotiveCd - Overload
Cm - Nital Etched Micrography by OMDf - Ductile Crack
ML00119 — Thermal Fatigue of a Marine BoilerM - Low Carbon SteelP - Fabrication WeldAp - ShipCd - Thermal Fatigue
Micrography of the plate in a longitudinal section, presenting a typical ferritic pearlitic structure, banded.
165
VIEW
ML00119 / Feb.2018
Thermal Fatigue of a Marine Boiler
M - Low Carbon SteelP - Fabrication WeldAp - ShipCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the ferritic pearlitic structure of the plate in the longitudinal section.
147
VIEW
ML00119 / Feb.2018
Thermal Fatigue of a Marine Boiler
M - Low Carbon SteelP - Fabrication WeldAp - ShipCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of the weld metal in the center os the weld. Columnar grains (of the previous austenite) with primary ferrite in the grain boundaries; ferrite with aligned second phases and acicular ferrite, intragranular.
136
VIEW
ML00119 / Feb.2018
Thermal Fatigue of a Marine Boiler
M - Low Carbon SteelP - Fabrication WeldAp - ShipCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Weld Metal
Micrography of the weld metal in the center os the weld. Columnar grains (of the previous austenite) with primary ferrite in the grain boundaries and acicular ferrite intragranular.
125
VIEW
ML00119 / Feb.2018
Thermal Fatigue of a Marine Boiler
M - Low Carbon SteelP - Fabrication WeldAp - ShipCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Ferritic Weld Metal
Micrographic detail of the weld metal in the center os the weld. Columnar grains (of the previous austenite) with primary ferrite in the grain boundaries; and details of the ferrite with aligned second phases and acicular ferrite, intragranular.
112
VIEW
ML00119 / Feb.2018
Thermal Fatigue of a Marine Boiler
M - Low Carbon SteelP - Fabrication WeldAp - ShipCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Ferritic Weld Metal

+12 more from this case →

ML00117 — High Carbon Steel Wire RopeM - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Typical manufacturing
Micrography of a longitudinal section of the core wire, 2.0 mm diameter, in the center of the thickness, showing a strain hardened pearlitic structure.
89
VIEW
ML00117 / Jan.2018
High Carbon Steel Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of a longitudinal section of the core wire, 2.0 mm diameter, in the center of the thickness, showing a strain hardened pearlitic structure.
81
VIEW
ML00117 / Jan.2018
High Carbon Steel Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Strain hardened pearlite
Micrography of a longitudinal section of the core wire, 2.0 mm diameter, at the surface of the wire, showing that the wire presents no protective layer (not galvanized nor plated) and the microstructure is strain hardened, aligned.
71
VIEW
ML00117 / Jan.2018
High Carbon Steel Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrography of a longitudinal section of the core wire, 2.0 mm diameter, at the surface of the wire, showing that the wire presents no protective layer (not galvanized) and the microstructure is strain hardened, aligned.
60
VIEW
ML00117 / Jan.2018
High Carbon Steel Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of a longitudinal section of the core wire, 2.0 mm diameter, at the surface of the wire, showing that it presents no protective layer (not galvanized nor plated) and the microstructure is pearlitic, strain hardened.
77
VIEW
ML00117 / Jan.2018
High Carbon Steel Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - No Coating Layer

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ML00110 — Non Conformance in Spray and Fuse PinM - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Low magnification micrography of the pin in the center of the 25 mm thickness. Ferritic-pearlitic structure of the material that slowly cooled after spray and fuse application. Transverse section.
24
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the ferritic-pearlitic structure in the center of the thickness of the tubular forging pin. Transverse section. The fuse is conducted in high temperature and the pin was not heat treated after the thermal spray deposition and fuse.
22
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the ferritic-pearlitic structure in the center of the thickness of the tubular forging pin. Transverse section. The fuse is conducted in high temperature and the pin was not heat treated after the thermal spray deposition and fuse.
20
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite