Kalling Etched Micrography by OM

18 cases · 147 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Aged microstructure of the HP stainless steel, modified with 1%Nb, cast fitting, tubular, operating for 6 years in a furnace which design temperature is 1100°C. The material presented a network of primary carbides, white and grey, and an austenitic matrix with coalescing secondary precipitation. Some voids. The Vickers identation indicates a hardness value about 260HV 100g in the aged austenitic matrix.
492
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Microhardness identations
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure.
55
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrography of a longitudinal section, in the center, of the broken 5/8" bolt, presenting an aged martensitic structure. There are vertical "lines" that correspond to segregation bands due to the forming direction. These bands are evident only using low magnification microscopy.
168
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Microstructure of the spring in a transverse section, presenting an aged martensitic structure.
96
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a transverse section of the ring presenting a uniform tempered martensite structure.
43
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
17-4 PH rod. Micrography of the longitudinal section in the center of the thickness, presenting an aged martensitic structure. The darker lines are bands of (sligthly) segregated regions. This material presents properties that correspond to the H1150 grade.
73
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of the pin microstructure at the longitudinal section showing a tempered martensitic structure and a band of retained austenite.
61
VIEW
ML00085 / Nov.2017
Corrosion Fatigue of a Martensitic SS Pin
M - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a longitudinal section of the pin, presenting a tempered martensitic structure with aligned delta ferrite and carbide phases.
80
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides

More from these cases

ML00173 — Welding Cracks in an Aged HP Cast FittingM - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cast fitting microstructure. Network of primary carbides and austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Cast fitting microstructure. The material presented a network of primary carbided and an austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Micrographic detail of the network of primary carbided, white and grey, and an austenitic matrix with coalescing secondary precipitation.
30
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Fusion line between the aged base metal (in the top) and the weld metal (in the bottom). The adopted filler metal is similar to the base metal.
27
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Fusion Line
Fusion line between the aged base metal (in the top) and the weld metal (in the bottom). There is a region where the primary carbides melted (partially melted zone), that appears dark, and a region of high dilution cloe to the fusion line.
26
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Fusion Line

+4 more from this case →

ML00148 — Brittle Fracture of a 420 SS Barrel NutM - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Microstructural aspect of a longitudinal section of the nut, in the middle of the thickness. Martensitic structure, banded.
46
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Microstructural detail of the banded structure. The rough aspect of the band is created by the carbides (better seen in the higher magnification image) in the segregation band.
38
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrographic detail of the nut longitudinal section presenting the large carbides (white islands) in the segregation band, and small precipitates all through the martensite matrix, indicating that this high carbon steel was tempered in a high temperature. The 36HRc hardness also confirms this high tempering temperature.
39
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Martensite
Vickers microhardness identations using 100 grams. In a position out of the band (top line). Values from left to right, 380HV; 390HV and 394HV. In a position inside the band (bottom line). Values from left to right, 433HV, 483HV and 473 HV.
33
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure. It is possible to see that the contact pressure in the thread caused a surface plastically deformation.
24
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure

+6 more from this case →

ML00139 — Hydrogen Fracture of a 17-4 PH Allen BoltM - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Micrography of a longitudinal section, in the center, of the broken 5/8" bolt, presenting an aged martensitic structure.
133
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrographic detail of the aged martensitic structure. The bolt presented variations in the previous austenite grain boundaries from the center of the thickness to the surface. No delta ferrite or retained austenite islands are evidenced.
107
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a longitudinal section of the 5/8" bolt, at the bottom of the thread, presenting a refined structure compared to the center of the bolt and a mark at the thread flank that was probably created during tightening of the bolt.
95
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the 5/8" bolt, at the bottom of the thread, presenting a refined structure compared to the center of the bolt. The structure is aged martensite.
91
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrographic detail of the aged martensite structure, refined when compared to the structure in the center of the bolt.
87
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Martensite

+16 more from this case →

ML00137 — Brittle Fracture of a 15-5 PH Valve SpringM - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Micrographic detail of a longitudinal section of the spring indicating that under the deposits there are intergranular cracks initiating at the spring surface.
60
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Micrography of a longitudinal section of the spring indicating that under the deposits there are intergranular cracks initiating at the spring surface.
57
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Micrographic detail of a longitudinal section of the spring indicating that under the deposits there are intergranular cracks initiating at the spring surface.
57
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Micrography of a section transverse to the fracture, in the starting point, showing the intergranular morphology of the fracture surface.
38
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Intergranular Fracture
Micrographic detail of the intergranular morphology of the fracture surface, in the starting point of the failure.
40
VIEW
ML00137 / Mar.2021
Brittle Fracture of a 15-5 PH Valve Spring
M - Precipitation Hardened Stainless SteelP - SpringAp - Oil and GasCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Intergranular Fracture

+5 more from this case →

ML00124 — MIC of a Martensitic Valve RingM - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Micrography of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface.
27
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface. it is possible to identify dissolution of the structure adjacent to the grain boundaries,
25
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Crack
Micrographic detail of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface. it is possible to identify dissolution of the structure adjacent to the grain boundaries,
24
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Micrograph showing a fine acicular martensitic matrix with a branching crack network, more extensive near the right edge.
25
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Crack
Micrography of a transverse section of the ring, in the center, where the cracking was closed. The cracks are intergranular and not opened to the surface.
29
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Crack

+1 more from this case →

ML00121 — Pitting Corrosion in a Subsea SystemM - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
17-4 PH rod. Micrography of the longitudinal section in the center of the thickness, presenting an aged martensitic structure. The darker lines are bands of (sligthly) segregated regions. This material presents properties that correspond to the H1150 grade.
66
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Martensite
17-4 PH rod. Micrographic detail of the aged martensitic structure. At this magnification level the previous austenite grain boundaries are evidenced. It is also possible to see that the bands of (sligthly) segregated regions are all martensitic.
64
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Martensite
17-4 PH rod. Micrography of the longitudinal section close to the surface, presenting the roughness (the waves at the surface) and a region where a pitting was still in the beginning, not related to any specific microstructure.
70
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Pitting
ML00085 — Corrosion Fatigue of a Martensitic SS PinM - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
Micrographic detail of the pin microstructure at the longitudinal section showing a tempered martensitic structure and a band of retained austenite.
62
VIEW
ML00085 / Nov.2017
Corrosion Fatigue of a Martensitic SS Pin
M - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrographic detail of the pin microstructure at the longitudinal section showing a band of retained austenite in martensitic structure.
58
VIEW
ML00085 / Nov.2017
Corrosion Fatigue of a Martensitic SS Pin
M - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of the pin in a longitudinal section, transverse to the fracture surface, close to the point of cracking iniciation, presenting a flat propagation and a secondary crack, paralel to the fracture surface.
54
VIEW
ML00085 / Nov.2017
Corrosion Fatigue of a Martensitic SS Pin
M - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Kalling Etched Micrography by OMDf - Fracture
Micrography of the pin in a longitudinal section, transverse to the fracture surface, close to the point of cracking iniciation, presenting a flat propagation and a secondary crack, paralel to the fracture surface.
52
VIEW
ML00085 / Nov.2017
Corrosion Fatigue of a Martensitic SS Pin
M - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Kalling Etched Micrography by OMDf - Fracture
Micrographic detail of a secondary cracking close to the fracture position. The crack presents no plastic deformation, is slightly branched and filled with products.
52
VIEW
ML00085 / Nov.2017
Corrosion Fatigue of a Martensitic SS Pin
M - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Kalling Etched Micrography by OMDf - Fatigue Fracture

+5 more from this case →

ML00046 — Brittle Fracture of SS Shear PinM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Micrographic detail of the pin structure, in the longitudinal section, at the segregated band with aligned inclusions and phases, delta ferrite and carbides.
70
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the pin structure, in the longitudinal section, presenting a martensitic matriz, aligned inclusions (grey, delta ferrite islands (poligonal white phases) and carbides (also white phases) surrounding the delta ferrite.
64
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides