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Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: High Temperature clear all

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Aspect of the 3 1/2" diameter tube after the water leakage in high temperature.
962
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - Aspect Before AnalysisDf - General View
The carcass was manufactured using niobium stabilized plates, grade AISI 347, with circumferential welds, where the through wall cracks were detected.
300
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Field photoDf - General View
Aspect as received, side A, of the part removed from the rectangular tube that was manufactured from plates, and originally presented two welded seams (not included in the sample). Close to the edges of the sample, where probably were the corners of the rectangular tube, the degradation is in a highest level. Three samples were analysed, with different thicknesses (indicated in the figure). Side A is the side that was in contact with the reaction (product side).
445
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Aspect Before AnalysisDf - General View
Micrographic detail of the longitudinal section of the tube, close to the external surface. The carburizing layer consists of a bainitic structure, with intergranular and intragranular carbide precipitation.
1184
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Carburized Layer
Micrography of the new tube close to a region of a casting defect (shrinkage), presenting only austenitic structure with a network of primary precipitates.
351
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides
Aspect of the cracking after Dye Check Test (Liquid Penetrant) in the external side of the line that operates at 800°C, insulated, and presented the leakage associated to the longitudinal seam weld of the fitting. The circumferential butt weld of the fitting to a pipe did not fail. See the schematic drawing in the next figure
371
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Aspect by NDTDf - Through Wall Cracking
Micrography of the transverse section of the NEW TUBE, in the center of the thickness, showing the austenitic structure with primary carbides network.
410
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides
Micrography of a longitudinal section of the bolt at the fracture surface. The material showed several creep voids and interconnected cracks. The broken bolt remained in service during some time and the fracture surface presented a thick oxide layer(grey). As polished.
529
VIEW
ML00004 / Jun.2018
Creep in High Temperature Bolts
M - CrMo SteelP - FastenerAp - Gas TurbineCd - Creep
Cm - Micrography by OMDf - Oxide Layer

More from these cases

ML00180 — Local Melting of Copper Cooling TubesM - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
View of the iinternal side of the tube (water side), deformed in the overheated area. There are several leaking points.
115
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - Aspect Before AnalysisDf - Internal Surface
Macroscopic aspect after cutting longitudinally in two halfs, at the damaged area. The tube internal surface showed a red copper colour at the overheated region and the perforation is associated to longitudinal cracks.
104
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - Longitudinal Section AspectDf - Internal Surface
Detail of the perforation point, internal view. Aligned perforations in the overheated region and interconnected longitudinal cracks.
94
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - Longitudinal Section AspectDf - Leakage
Micrographic aspect of the tube out of the damaged region, in a longitudinal section, showing the grain refined copper structure.
96
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - FeCl3+HCl+H2O Etched MicroDf - In the Center of the Thickness
Micrographic detail of the granular copper structure, a little far from the overheated region.
102
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - FeCl3+HCl+H2O Etched MicroDf - Granular structure

+14 more from this case →

ML00174 — Carburization of a 347 SS Welded JointM - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
The circumferential welds presented several regions where the multiple cracks appeared, mainly revealed by dye check test.
49
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect by NDTDf - Multiple cracks
Aspect of one region where the cracks appeared, after grinding and polishing. Several branched cracks located in welded regions. It is the region where the sample was taken.
36
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect Before AnalysisDf - At the Surface
The small sample removed for analysis. This wedge sample presents three faces: one polished face (that corresponds to the surface), one fractured face and one cut face.
38
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Testpiece aspectDf - Fracture
The small wedge sample is 4 mm deep in the thickness and the circumferential weld are is about 15 mm width where it appears in the internal side of the carcass. The image shows the crack surface (fracture) where the weld aspect is evident.
32
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect Before AnalysisDf - Fracture
The fracture surface in the sample shows columnar grains in the weld and large facets in the heat affected zone (HAZ) close to the internal surface of the carcass (to the top of the image).
32
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Fractography by SEMDf - Brittle Fracture

+10 more from this case →

ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Aspect as received, side B, of the same part. Side B is the external side of the rectangular tube, that was in contact with the electric furnace atmosphere. This surface of side B presented less degradation than the internal surface (side A).
88
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Aspect Before AnalysisDf - General View
Transverse section macrography of the plate where the degradation by thinning is worst, close to the original corners of the tube. The thinning is occurrring from the product reaction side (side A to the bottom of the figure). The macrography shows a reduction in the thickness from 2 mm (right side, sample 2) to almost zero (left side, sample 1).
86
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Transverse Section AspectDf - Thinning
Longitudinal section macrography of the plate where the degradation by thinning is reducing the thickness from 6mm to 4mm (sample 3). The thinning is occurrring from the product reaction side (side A to the bottom of the figure).
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Longitudinal Section AspectDf - Thinning
SAMPLE 1 AT THE FRACTURE - Micrography in low magnification where the thickness is reduced to zero (fracture). Side A (process side) to the bottom and side B (furnace environment side) to the top.
85
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Low Mag
SAMPLE 1 AT THE FRACTURE - Micrography at the position where the thickness is reduced to zero. Side A to the bottom. The microstructure is austenite with intergranular and transgranular precipitation. The position of the zero thickness presents aspect of an intergranular fracture, and in side A there are several intergranular cracks from the surface.
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation

+22 more from this case →

ML00107 — Carburized 9Cr1MoV Superheater TubeM - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Micrography of the longitudinal section of the tube, close to the internal surface. A thick scale is evident, but no microstructural changes compared to the center of the tube.
183
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Bainite
Aspect of the superheater ND 1" tube that was in operation for about 35,000 hours and presented a thick deposit at the external surface.
211
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Aspect Before AnalysisDf - General View
Micrography of a longitudinal section of the tube in the center of the thickness, showing a ferritic-bainitic structure of this CrMoV steel.
156
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Bainite
Micrography of a longitudinal section of the tube in the center of the thickness, showing a ferritic-bainitic structure of this CrMoV steel.
137
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Bainite
Micrography of a longitudinal section of the tube in the center of the thickness, showing a ferritic-bainitic structure of this CrMoV steel.
142
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Bainite

+9 more from this case →

ML00097 — Cast SS Tube Removed From High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
The macrography of a transverse section of the new tube shows that there are shrinkage voids close to the internal surface, that is exposed to high temperature air. The tube is a 4" diameter and 1/4" thick.
62
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Transverse Section AspectDf - Casting Structure
Micrography close to the external surface of a new tube, sound.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the External Surface
Micrography close to the internal surface of a new tube, presenting casting defects.
47
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography of the tube removed from service after 6 month, close to a region of a casting defect (shrinkage), presenting austenitic structure with a network of primary precipitates (initial stage of coarsening) and intragranular secondary precipitation.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation
The macrography of a transverse section of the tube removed from service after 6 months, with damage close to the internal tube surface. The tube is a 4" diameter and 1/4" thick.
41
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Transverse Section AspectDf - Casting Structure

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ML00061 — Creep in a Seam Weld of a 304H SS FittingM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Schematic drawing presenting the aspect of the cracking after Dye Check Test (Liquid Penetrant) in the external side of the line that operates at 800°C, insulated, and presented the leakage associated to the longitudinal seam weld of the fitting. The circumferential butt weld of the fitting to a pipe did not fail.
62
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Identification drawingDf - Through Wall Cracking
Aspect of the internal side of the fitting, at the longitudinal seam weld, and macrography of a transverse section showing the through wall cracks.
62
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Transverse Section
Through wall cracking in the longitudinal seam weld of the fitting. Several cracks, longitudinal to the weld, were created by the connection of voids in the weld metal, associated to a strong microstructural evolution.
191
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Cracks
Micrography of a longitudinal section of the fitting, at the base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
44
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal
Micrographic detail of the fitting base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
40
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal

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ML00038 — Cast SS Tube for High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Micrography of the transverse section of the NEW TUBE, close to the external surface, showing the austenitic structure with primary carbides network.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Close to the External Surface
Macrography of the NEW TUBE, centrifugally cast, in the transverse section, presenting columnar grains close to the external surface.
50
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Kalling Etched MacroDf - Transverse Section
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects close to the external surface.
49
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Close to the External Surface
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects in the center of the thickness.
47
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Transverse Section
Micrography of the transverse section of the TUBE REMOVED FROM SERVICE, in the center of the thickness, showing the austenitic structure with primary carbides network and secondary precipitation.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation

+4 more from this case →

ML00004 — Creep in High Temperature BoltsM - CrMo SteelP - FastenerAp - Gas TurbineCd - Creep
Micrographic detail of the creep voids and interconnected cracks. The broken bolt remained in service during some time and the fracture surface presented a thick oxide layer(grey). As polished.
121
VIEW
ML00004 / Jun.2018
Creep in High Temperature Bolts
M - CrMo SteelP - FastenerAp - Gas TurbineCd - Creep
Cm - Micrography by OMDf - Interconnected Cracks
Micrographic detail of the creep voids and interconnected cracks. The broken bolt remained in service during some time and the fracture surface presented a thick oxide layer(grey). As polished.
101
VIEW
ML00004 / Jun.2018
Creep in High Temperature Bolts
M - CrMo SteelP - FastenerAp - Gas TurbineCd - Creep
Cm - Micrography by OMDf - Voids
Micrography of a longitudinal section of a CrMov steel bolt that broke in service by a creep mechanism in a gas turbine. Tempered structure. Interconnected cracks paralled to the fracture surface.
95
VIEW
ML00004 / Jun.2018
Creep in High Temperature Bolts
M - CrMo SteelP - FastenerAp - Gas TurbineCd - Creep
Cm - Nital Etched Micrography by OMDf - Crack
Micrographic detail of a longitudinal section of the bolt far from the fracture, presenting a tempered structure.
82
VIEW
ML00004 / Jun.2018
Creep in High Temperature Bolts
M - CrMo SteelP - FastenerAp - Gas TurbineCd - Creep
Cm - Nital Etched Micrography by OMDf - Tempered Structure
Micrographic detail of a longitudinal section of the bolt close to the fracture, presenting an overtempered structure.
76
VIEW
ML00004 / Jun.2018
Creep in High Temperature Bolts
M - CrMo SteelP - FastenerAp - Gas TurbineCd - Creep
Cm - Nital Etched Micrography by OMDf - Overtempered Structure