Raw Material

10 cases · 85 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Subsea Capture method: Optical Microscope clear all

Raw Material — sub-branches

Bar 2Forging 3Heat Treated Part 1Machined Part 2Pipe 1Rolled Plate 1Tube 1Tubular Forging 1Wire 1

Results

SortNewestOldestTitle A-ZTitle Z-A
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
106
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
74
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of the tubing fusion line. The welding was conducted in two passes. The average hardness at the heat affected zone of the tubing is 257 HV5.
825
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - Fusion Line Left Side
Micrographic detail of the austenitic structure at the surface, where the grain size of the material increased. By optical microscopy the intragranular precipitation due to solution annealing and aging is not revealed.
794
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
Micrography of the longitudinal section of the forging material, presenting a granular austenite, precipitation hardened.
84
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
The longitudinal section of the spring wire shows a strain hardened martensitic structure, aged to high strength (602 HV 0.3kg). Previous austenite grains are elongated.
55
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Base metal micrographic detail presenting a tempered martensitic microstructure.
27
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
The micrography of the pipe in the longitudinal section shows an aligned structure.
60
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal

More from these cases

ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic detail of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
102
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Metallographic detail of the large amount of sigma phase, associated to the ferritic structure.
105
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Microstructural analysis of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
67
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
63
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
61
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite

+8 more from this case →

ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
61
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. The ferrite amount, measured by metallographic method, manual counting, is 59%.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. The average austenite spacing is 80 microns, a lot larger than the maximum allowed in the specification, of 30 microns. No detrimental phases were identified at the ferrite/austenite interfaces, but the ferrite phase presented a rough aspect. Higher magnification analysis would be required to identify precipitation.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrographic detail of the ferrite and austenite structure in the transverse section of the forged bar, in the center of the thickness.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the ferrite and austenite structure in the longitudinal section of the forged bar, in the center of the thickness.
55
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
ML00100 — Superduplex Tubing to Forging Welded JointM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Micrography of the tubing heat affected zone.
69
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - HAZ Left Side
Micrography of the tubing heat affected zone.
68
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - HAZ Left Side
Low magnification micrography of the superduplex stainless steel tubing (base metal), in the longitudinal direction. Refined ferritic-austenitic structure. The average hardness in the section is 264HV5.
58
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - Base Metal Left Side
Micrography of the superduplex stainless steel tubing (base metal), in the longitudinal direction. Refined ferritic-austenitic structure.
55
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Micrographic detail of the superduplex stainless steel tubing (base metal), in the longitudinal direction. Refined ferritic-austenitic structure.
53
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure

+10 more from this case →

ML00089 — Inconel 718 Allen Bolt for Subsea ApplicationM - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
The micrography of a longitudinal section of the bolt close to the surface, at the thread, shows that it was machined from a bar, not rolled.
37
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
The micrography of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"), shows an equiaxial granular structure. Although the material was hardened by heat treatment (solution annealing and aging), the microstructure at this magnification does not reveal the intragranular precipitation.
34
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Micrographic detail of a longitudinal section of the bolt, close to the surface (ND 1/2"). The grain size is higher than the center of the bolt.
28
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
ML00078 — Hydrogen Cracking of IN 718 Subsea ConnectorM - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the conector, at the fracture position, showing secondary cracks from the fracture surface.
64
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Fracture
The micrographic detail of the longitudinal section at the fracture surface shows intergranular morphology for the secondary cracks (longitudinal to the forging axis).
64
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Secondary Cracks
Micrographic detail of a longitudinal section of the connector, at the fracture surface (in the top), showing intergranular secondary cracks.
54
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Micrographic detail of a longitudinal section of the connector, at the fracture surface (in the top), showing intergranular secondary cracks. There is a large amount of delta phase precipitated intergranular and intragranluar.
48
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Secondary Cracks
ML00076 — Hydrogen Cracking of a 17-7 PH Subsea SpringM - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Micrographic detail of the strain hardened aged martensitic structure. Small aligned delta ferrite islands can be seen.
51
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
The transverse section of the spring wire shows a strain hardened martensitic structure, aged to high strength (602 HV 0.3kg).
48
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Transverse Section
Micrographic detail of the strain hardened aged martensitic structure.
48
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Transverse Section
Micrography of a longitudinal section of the wire, at the fracture surface (top of the figure) evidencing the intergranular and transgranular aspects of the hydrogen assisted cracking mechanism.
37
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Micrography by OM using A262 Method ADf - Secondary Cracks
Micrographic detail of a longitudinal section of the wire, at the fracture surface (top of the figure) evidencing the intergranular and transgranular aspects of the hydrogen assisted cracking mechanism. The electrolytic oxalic acid etch reveals the delta ferrite phase. Compare with the Kalling etch in the other figure.
31
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Micrography by OM using A262 Method ADf - Fracture

+2 more from this case →

ML00045 — Subsea Tubular F6NM Martensitic SSM - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Micrographic detail of the heat-affected zone close to the base metal.
29
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the heat-affected zone close to the fusion line.
31
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the tempered martesite weld metal close to the fusion line. The columnar grains can be observed .
22
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Weld Metal
Micrography of the base metal showing a tempered martensitic microstructure.
29
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Micrography of the heat-affected zone. The fusion line is in the right and the coarse structure of the base metal is refined at the heat affected zone.
28
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone

+8 more from this case →

ML00053 — SAW Longitudinal Seam of X70 PipeM - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Detail of the microstructure in the center of the plate, in the longitudinal section. The structure is refined and presents different ferritic grain sizes.
49
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Detail of the microstructure in the center of the plate, in the longitudinal section. The ferritic structure is refined and presents different grain sizes. Carbides are presented in different morphologies (perlite, precipitated) and there are probably microphases (aligned in a central segregation line).
55
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of the fusion line of the second pass (not reheated). The HAZ is bainitic and the weld metal microstructure is predominantly formed by acicular ferrite.
51
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Fusion Line
Center of the weld in the second pass. Columnar grains of the previous austenite.
45
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Weld Metal
Fusion line of the first pass (reheated in high temperature). The HAZ is bainitic and the weld metal microstructure is predominantly formed by acicular ferrite.
43
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Fusion Line

+6 more from this case →