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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Red painted device where the 50 mm x 50 mm 6061 T6 aluminum alloy plate was positioned (in the circle). The image presents the target, positioned 100 meters far from the gun, after the shot and the projectile perforated the plate.
478
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Aspect Before AnalysisDf - General View
Aspect of the internal side of the drilling tool, after cleaning for inspection. Several regions of corrosion where detected where the drilling mud was adhered and remained uncleaned for a period a little longer than 1 month.
775
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Aspect Before AnalysisDf - Internal Surface
Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a longitudinal seam welded pipe, with substrate in low alloy steel X65 and clad plate in Alloy 625 (welded by a solid state process). The region is a detail in the side of the Ni alloy clad plate where a grain refinement has occurred probably due to recrystallization of a strain hardened region during later heat treatment. The microhardness of this region is a lot higher than the value obtained out of this region, in the clad plate.
904
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface
Micrographic detail of the austenitic structure at the surface, where the grain size of the material increased. By optical microscopy the intragranular precipitation due to solution annealing and aging is not revealed.
794
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
Region of the leakage close to the welded joint between the pipe and the 90° elbow, in the 1 1/2" nominal diameter piping, SCH 40 (3.7 mm thick). See the schematic drawing in the next figure
966
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Aspect Before AnalysisDf - Leakage
Detail of the fracture surface, predominantly transgranular with secondary cracks of intergranular morphology.
831
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Internal surface detail of the 3 1/2" pipe, cut in a longitudinal section (transverse to the weld), presenting a localized corrosion at the margin of the welded joint (Keller etched), in the root. The pipeline was assembled with pipes manufactured in two different aluminum alloys, AA 3003 (top of the figure) and AA 6063 (bottom of the figure), and the localized corrosion occurred at the fusion line of the 6063 pipe.
1296
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Surface AspectDf - Welded Joint
Micrography of the nut in the longitudinal direction, in the center of the thickness, presenting a granular austenitic structure free from detrimental phases.
475
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - In the Center of the Thickness

More from these cases

ML00145 — Impact of a .380 Winchester on 6061 T6 PlateM - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Aspect of a typical .308 Winchester projectile, similar to the one adopted to shot the plate, cut in a longitudinal section. It is a Cu alloy case filled with Pb-Sb.
61
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Longitudinal Section AspectDf - Longitudinal Section
Aspect of the 3/8" thickness plate, 50 mm x 50 mm, of the aluminum alloy plate, in the face of impact with the projectile. The plate was perforated by the bullet.
52
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Aspect Before AnalysisDf - General View
Micrography of the plate in a section, in the middle of the thickness. The aligned pitting is associated to the chemical etch of inclusions and second phases. The structure is granular but the grain boundaries do not appear at that magnification, originally 50x.
50
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Aligned particles
Micrography of the plate in a section, in the middle of the thickness, in a position where the plate was not affected by the shot. The microstructure is granular although the grain boundaries are not resolvable at this magnification. The black spots are localized corrosion in aligned particles.
49
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Aligned particles
Micrographic detail of the plate in the middle of the thickness. At this magnification it is possible to see the grain boundaries and the black spots are localized etching in aligned particles.
43
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Granular structure

+45 more from this case →

ML00135 — MIC of a Non Magnetic Drilling ToolM - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Aspect of the external side of the nominal diameter 6 3/4" drilling tool, after cleaning for inspection. Several regions of corrosion where detected where the drilling mud was adhered and remained for a period a little longer than 1 month. This tool is a high strength steel, cold worked.
163
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Aspect Before AnalysisDf - General View
Aspect of the external side of the nominal diameter 6 3/4" drilling tool, after cleaning for inspection. Several regions of corrosion where detected where the drilling mud was adhered and remained for a period a little longer than 1 month. This tool is a high strength steel, cold worked.
125
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Aspect Before AnalysisDf - Localized Corrosion
Microscopical aspect by scanning electron microscopy (SEM) of the external surface of a drilling tool in a position that presented localized deposits and corrosion under deposit. The deep corrosion in a short time is only possible associated to the biological growth and aggressive environment generated by the microorganisms metabolites - Microbiologically Induced Corrosion (MIC).
104
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Deposits
Microscopical aspect by scanning electron microscopy (SEM) of the external surface of a drilling tool in a position that presented localized deposits and corrosion under deposit. It is possible to see that the strain hardened surface was etched by the aggressive metabolites of the microorganisms.
90
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
Optical micrography of the transverse section of the drill collar, in the center of the thickness, presenting an uniform, granular, fully austenitic microstructure.
76
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transverse Section

+13 more from this case →

ML00133 — Seam Welded Pipe Cladded with Alloy 625M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
The 6 1/2" nominal diameter longitudinal seam welded pipe is internally cladded with Alloy 625. The pipe was manufactured by forming a cladded plate (probably welded by rolling) and welding it longitudinally. The pipe was heat treated (quenched and tempered) after the seam weld.
97
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Aspect Before AnalysisDf - Welded Joint
The macrography of a longitudinal section shows the low alloy (C-Mn) steel pipe, internally cladded with Ni alloy clad plate.
72
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Electrolytically Etched MacroDf - Longitudinal Section
Micrography of a longitudinal section of the pipe substrate, in low magnification, showing a uniform microstructure,
51
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure obtained by the pipe quenching and tempering,
48
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure,
50
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Bainite

+12 more from this case →

ML00089 — Inconel 718 Allen Bolt for Subsea ApplicationM - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
The macrography shows the longitudinal section of the allen bolt, 1/2" nominal diameter, that was machined from a heat treated bar (solution annealed and aged). The granular structure presents differences in the grain sizes. At the bolt head (external surface of the original bar) the austenitic grain size is larger than in the center of the bar where the particles in segregated bands "arrested" the grains during hot forming and solution annealing.
58
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched MacroDf - Machined Thread
The micrography of a longitudinal section of the bolt close to the surface, at the thread, shows that it was machined from a bar, not rolled.
37
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
The micrography of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"), shows an equiaxial granular structure. Although the material was hardened by heat treatment (solution annealing and aging), the microstructure at this magnification does not reveal the intragranular precipitation.
34
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Micrographic detail of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"). Although the material was hardened by heat treatment (solution annealing and aging), the microstructure observed by optical microscopy does not reveal the intragranular precipitation.
33
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched MacroDf - Austenite
The micrography of a longitudinal section, at the bolt head close to the surface of the original bar. In this region the material increased the grain size due to the lack of particles (inclusions), to "arrest" the grain boundaries (during hot forming and solution annealing). The smaller grain size is located in the center of the bar, that concentrated the inclusions.
30
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched MacroDf - Dual grain sizes

+1 more from this case →

ML00065 — Erosion Corrosion of Monel PipingM - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Schematic drawing presenting the External piping surface
339
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Identification drawingDf - Leakage
Aspect of the piping cut in the longitudinal direction, presenting the leakage region close to the welded joint between the pipe and the 90° elbow. The original SCH 40 (3.7 mm thickness) presents an actual average thickness of 2 mm all through the piping extension, evidencing a general thinning. See the schematic drawing in the next figure.
364
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Aspect Before AnalysisDf - Leakage
Schematic drawing presenting the internal piping surface
234
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Identification drawingDf - Leakage
Detail of the internal piping surface, showing lack of deposits and a shinning surface, suggesting erosive conditions.
226
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Surface AspectDf - Leakage
Macrography of the pipe to fitting welded joint, in a region where the thickness loss is almost uniform. The pipe is in the left of the figure and the elbow is in the right, with a general thinning (average of 2 mm, considering that the original thickness was 3.7 mm), and a slightly more intense thickness loss at the weld metal near the elbow side.
183
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched MacroDf - Welded Joint

+18 more from this case →

ML00078 — Hydrogen Cracking of IN 718 Subsea ConnectorM - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Brittle aspect of the failure of the conector in the male thread. Both sides of the fracture.
96
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View
Micrography of the longitudinal section of the forging material, presenting a granular austenite, precipitation hardened.
84
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Fractography by SEM, showing intergranular and transgranular fracture micromechanisms.
72
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Micrography of the longitudinal section of the conector, at the fracture position, showing secondary cracks from the fracture surface.
64
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Fracture
The micrographic detail of the longitudinal section at the fracture surface shows intergranular morphology for the secondary cracks (longitudinal to the forging axis).
64
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Secondary Cracks

+3 more from this case →

ML00059 — Intergranular Corrosion of Aluminum PipingM - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
The macrography of the welded joint shows the AA 6063 alloy pipe in the right and the AA 3003 pipe in the left, welded in two passes. The root presents small regions of corrosion in the weld metal and a localized corrosion at the fusion line of the 6063 pipe (knife-line attack morphology).
397
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched MacroDf - Localized Corrosion
Micrography of a longitudinal section of the pipe AA 3003. Granular structure that reveals the forming direction and dispersed particles.
229
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Base Metal Left Side
Micrographic detail of a longitudinal section of the pipe AA 3003. Granular structure and dispersed particles.
199
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Base Metal Left Side
Micrography of a longitudinal section of the pipe AA 6063. Granular structure and dispersed particles.
169
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Base Metal Right Side
Micrographic detail of a longitudinal section of the pipe AA 6063. Granular structure and dispersed particles.
138
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched MacroDf - Base Metal Right Side

+12 more from this case →

ML00062 — Inconel 718 Lock Nut with Polymer InsertM - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
The nut was sectioned in the longitudinal direction to reveal the position of the Nylon insert.
59
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - Transverse Section
Micrography of the nut in the longitudinal direction, at the thread, presenting a granular austenitic structure free from detrimental phases or cold forming effects.
56
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
Micrographic detail of the nut at the thread, presenting a granular austenitic structure free from cold forming effects.
52
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
Micrography of the nut in the longitudinal direction, at the Nylon insert position, showing a cold formed region at the end of the nut, with high hardness levels (about 600 HV100g).
53
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Strain Hardened
Micrographic detail of the nut at the cold formed region where the nut was bent over the Nylon insert. It is possible to see strain hardened structures (600HV 100g).
41
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Strain Hardened