Microstructure

5 cases · 10 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Brittle Behavior Capture method: Scanning Electron Microscope clear all

Microstructure — sub-branches

Graphite in Flakes 1Intragranular Secondary Precipitation 1Martensite 2Sigma 4Zn Layer 2

Results

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Micrographic detail of the martensitic structure, clearly obtained from a refined previous austenitic structure .
19
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Martensite
Micrography of the longitudinal section of the cylinder, at the external diameter (right side of the figure), presenting smaller interdendritic graphite flakes in a ferritic-perlitic matrix. This surface is painted.
32
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Graphite in Flakes
Micrography of the casting at the surface, presenting a zinc layer deposited in a hot dip process. The thickness of the layer is about 0.3mm in this position, that is higher than expected for this process. The steel substrate is not revealed because the etch was light and the zinc layer protects the low aloy steel during the etch.
93
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by SEMDf - Zn Layer
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
92
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Micrography of the blade, view inside the grain. The intragranular precipitation presents one unique size of precipitation, not yet coalesced, although the blade was in high temperature service for 50.000 hours. Etched by H2SO4 + HNO3 + H3PO4 reagent.
66
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - Micrography by SEMDf - Intragranular Secondary Precipitation

More from these cases

ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Micrographic detail of the martensitic structure.
19
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Martensite
ML00138 — Liquid Metal Embrittlement of a HSLA SteelM - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Scanning electron fractography (originally 500x), showing zinc deposits at the fracture surface.
73
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Fractography by SEMDf - Zn Layer
ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
85
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
High magnification details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
81
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Higher magnification detail of the sigma phase by scaning electron microscopy.
76
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma