Brittle Behavior

12 cases · 217 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Brittle Behavior — sub-branches

Brittle Fracture 9Intergranular Cracking 2Liquid Metal Embrittlement 1

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Tool fixture 5" long, nominal diameter 2", presenting a recess 1/2" deep from two sides. The rupture occurred about 2" from the end of the rod. Scale in milimeters.
523
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Aspect of the broken spring. The wire is 36 mm diameter and the ourter diameter of the spirals is 320 mm. It was broken in different locations.
434
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
General view of the broken socket. The failure occurred during service, when the tool was tightening 3 3/4" bolts at 75% of the torque capacity. The fracture occurred associated to the smaller section of the socket, thickness of 13 mm, at the corner of the radio, that is a stress concentration raiser.
602
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Fractured position of the casting cylinder of 10.5 mm thickness (minimum measured thickness) showing a brittle behavior (lack of plastic deformation), typical of overloading a material with 1% ductility (measured in the tensile test). This is the view of the internal surface of the cylinder, presenting regions of localized thinning in this surface that was in contact with (treated) cooling water. The external side of the cylinder was painted.
918
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fracture Surface AspectDf - General View
Aspect of the fracture surface of the 2" diameter casting. The fracture appeared flat, with secondary cracks, and the position of the fracture during the loading test is located in the region that was in tensile stress during the hot dip galvanized process (the part was sustaining its own weight during the zinc hot dip bath).
800
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Aspect Before AnalysisDf - Brittle Fracture
Aspect of the cracked valve body, after disassembling and removing the internal parts. The valve is part of a lot that was manufactured by forging a cubic 170mm from a forged bar in SDSS UNS S32760, and heat treated (solution annealed) by the forging company. The fabrication using these bodies included the machining, fillet weld two inserts in Alloy 625, machining again, assembling the internals, and pressure test at 15,000 psi. The cracking occurred during test, only for this valve body.
676
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Cracking
The hose connector fracture surface presented different fracture micromechanisms associated to the microstructure: inclusion decohesion, small regions of intergranular fractures (probably due to cementite at grain boundaries), and cleavage of the ferritic structure. All these mechanisms are brittle.
560
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Brittle Fracture
Micrography of a transverse section of the lifting part, showing interdendritic voids close to the surface at the inner diameter of the padeye. The microstructure is tempered martensite.
450
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Casting defects

More from these cases

ML00182 — Brittle Fracture of a LAS Fixing RodM - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Detail of the flat fracture from the notch at the bottom of the recess. No plastic deformation.
113
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Brittle Fracture
Low magnification micrography presenting segregation bands in a martensitic structure. In the segregated regions the Nital etch effect is lower and the bands appear lighter. The black spots and lines are inclusions (some elongated) in the band.
91
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrography presenting segregation bands (less etched) in a tempered martensitic microstructure.
81
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Segregated Regions
Micrography presenting a tempered martensitic microstructure, with light etch in segregated bands.
74
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Tempered Martensite
Low magnification micrography, revealing (in black) the impurities in the segregated bands.
63
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Micro by OM, picric acid+FeCl3+H2O etchDf - Longitudinal Section

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ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Aspect of the fracture of the spring. The spring surface shows shallow pits.
49
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Fracture
Surface to fracture interface. The spring shows corrosion and pits.
46
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Corrosion
Aspect of the spring surface, with a layer of corroded products, and pits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Surface Aspect by SEMDf - Corrosion
Micrography of a transverse section of the spring, at the surface showing pits full of deposits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
Micrographic detail of the transverse section of the spring, at the surface, showing the pits full of corrosion deposits.
31
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Surface Deposits

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ML00161 — Brittle Fracture of a High Strength SocketM - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
General view of the broken socket. It was broken in two parts and shows no evidences of plastic deformation associated to the rupture.
93
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
General view of the broken socket, showing no plastic deformation asociated to the rupture. Looking from this side it is possible to see that the fracture followed the interface of the stem with the socket head.
80
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Micrography of a longitudinal section of the socket at the position where the fracture occurred. Uniform tempered martensitic structure. The hardness of this microstructure is 639 HV1Kg.
74
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of a longitudinal section presenting an uniform tempered martensitic structure.
81
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the tempered martensitic structure.
80
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite

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ML00141 — Brittle Fracture of a Corroded Gray Cast IronM - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Fracture aspect of the casting cylinder at the 10.5 mm thickness, showing a brittle behavior (lack of plastic deformation). The internal side of the cylinder is to the top of the figure, and the painted surface is to the bottom of the figure.
129
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fracture Surface AspectDf - Brittle Fracture
Detailed aspect of the cylinder fracture, the internal surface to the top of the figure and the painted external surface to the bottom of the figure.
103
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Fracture Surface AspectDf - Brittle Fracture
Macrographic aspect of a section of the cast cylinder, transverse to the fracture (top). The internal diameter of the cylinder (exposed to treated water) is to the left side and the external diameter of the cylinder (painted) is to the right side.
96
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - NItal Etched MacroDf - Brittle Fracture
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), close to the internal surface (left side). It is possible to see large graphite flakes.
98
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - Close to the Internal Surface
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), in the center of the thickness. It is possible to see a mixture of large graphite flakes and rosette grouping flakes.
80
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - In the Center of the Thickness

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ML00138 — Liquid Metal Embrittlement of a HSLA SteelM - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Micrography of the high strenght steel, heat treated, of the casting device. The microstructure is bainitic martensitic.
109
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Micrography of the high strenght steel, heat treated, of the casting device. The microstructure is bainitic martensitic.
92
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Micrographic detail of the high strenght steel microstructure, bainitic martensitic.
85
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Micrography of the casting at the surface, presenting a zinc layer deposited in a hot dip process. The thickness of the layer is about 0.3mm in this position, that is higher than expected for this process. The steel substrate is not revealed because the etch was light and the zinc layer protects the low aloy steel during the etch.
93
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by SEMDf - Zn Layer
Micrographic detail of the zinc layer at the surface.
88
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Zn Layer

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ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Detailed aspect of the cracking, straight and presenting a brittle aspect.
122
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Cracking
Detail of the internal bore, showing a brittle crack through the wall.
106
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Cracking
Aspect of a section cut transverse to the center of the body. The crack is brittle, trough wall, and was arrested in the region where the valve body was welded to the insert.
105
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Transverse Section AspectDf - Cracking
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
106
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrographic detail of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
102
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma

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ML00103 — Brittle Fracture of a Free-Cutting ConnectorM - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Aspect of the external side of the connector, with a longitudinally crack of a brittle aspect. It is a 5/8" connector (15.8 mm).
133
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Aspect of the internal side of the connector. The fracture, in the longitudinal direction, presents a brittle aspect. The thickness of the connector is about 2 mm.
126
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Brittle Fracture
Macroscopic detail of the brittle fracture, in the longitudinal direction.
105
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Brittle Fracture
Micrography of the longitudinal section of the fitiing, in a free-cutting steel. The microstructure is predominantly ferritic and there is a large amount of sulfide inclusions, aligned perpendicular to the forming direction.
97
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of the longitudinal section of the fitiing, in a free-cutting steel. The microstructure is predominantly ferritic, with small perlitic areas and some free cementite at ferritic grain boundaries. There is a large amount of sulfide inclusions, aligned perpendicular to the forming direction.
106
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Non Metallic Inclusions

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ML00098 — Brittle Fracture of a Casting Lifting DeviceM - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Aspect of the broken padeye. The outer diameter is about 10" and the thickness of the casting is about 2".
22
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - General View
Aspect of the fracture surface, showing a brittle morphology. Flat fracture with chevron marks from regions close to the internal diameter of the padeye, where there are secondary cracks.
22
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Aspect Before AnalysisDf - Fracture
Micrography of the lifting padeye showing a dendritic path of a quenched and tempered martensitic microstructure. The segregated regions (white interdendritic regions) are more clearly identified in low magnification. Voids are located in these segregated regions.
21
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. Voids are located in interdendritic segregated regions.
20
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the lifting padeye showing a quenched and tempered martensitic microstructure. Voids are located in interdendritic segregated regions. At this magnification the segregation is not clear.
16
VIEW
ML00098 / Nov.2017
Brittle Fracture of a Casting Lifting Device
M - Low Alloy Medium Carbon QTP - CastingAp - LiftingCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite

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