Optical Microscope

109 cases · 908 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Optical Microscope — sub-branches

As polished micrography 64Chromic Acid Electrolytic Etched 6Eletrolytically Etched Micrography by OM 6FeCl3+HCl+Ethanol Etched Micro 14FeCl3+HCl+H2O Etched Micro 12Glyceregia Etched Micrography by OM 6H2SO4+HNO3+H3PO4 Etched Micro 3Kalling Etched Micrography by OM 108Keller Etched Micrography by OM 46Kroll Etched Micrography by OM 5Micro by OM, picric acid+FeCl3+H2O etch 1Micrography by OM 53Micrography by OM using A262 Method A 44Micrography by OM, HF + HNO3 + H2O etch 6NaOH Electrolytic Etched Micro 47Nital Etched Micrography by OM 460Oxalic Acid Electrolytic Etch 27

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Micrography of a transverse section of the ring presenting a uniform tempered martensite structure.
43
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
74
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography, as polished, of the transverse section of the forged pin with the layer applied by a (thermal) spray and fuse process. The layer presented entrapped pores and globular oxides. It was melted after application by thermal spray (in this case using a flame) but the pin was not heat treated after the full application and melting of the layer and the base metal is ferritc-pearlitic.
51
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - As polished micrographyDf - Transverse Section
Micrographic detail of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Pearlite colonies in bands.
401
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of a transverse section of the 5 mm thick tubing, in the center of the thickness. Ferritic-pearlitic structure, with the pearlite presenting a coalesced aspect. The tubing was in service at ambient temperature, painted, and the coalesced aspect was generated before service, perhaps during the tubing manufacturing.
393
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Pearlite colonies in bands.
346
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of a longitudinal section of a 4 mm diameter wire, presenting an aligned and highly strained pearlitic structure. Base metal.
386
VIEW
ML00113 / Jan.2018
Autogenous Weld of a Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Welding
Cm - Nital Etched Micrography by OMDf - Strain hardened pearlite
Micrography of a transverse section of the pipe, external diameter 33.4 mm schedule XXS, in the center of the 9.1 mm thickness. The structure is predominantly ferritic. Small amount of pearlite.
553
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Predominantly Ferritic

More from these cases

ML00124 — MIC of a Martensitic Valve RingM - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Micrography of a transverse section of the ring, at the pitting position, as polished, showing that there are intergranular cracks and the martensitic structure is corroded (chemical dissolution) inside the pitting.
33
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - As polished micrographyDf - Corrosion
Micrographic detail of a transverse section of the ring, showing the corroded martensitic structure (chemical dissolution) inside the pitting.
32
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - As polished micrographyDf - Corrosion
Micrographic detail of a transverse section of the ring, showing the corroded martensitic structure (chemical dissolution) inside the pitting.
33
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - As polished micrographyDf - Intergranular Cracking
Micrography of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface.
27
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface. it is possible to identify dissolution of the structure adjacent to the grain boundaries,
25
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Crack

+4 more from this case →

ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
61
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. The ferrite amount, measured by metallographic method, manual counting, is 59%.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. The average austenite spacing is 80 microns, a lot larger than the maximum allowed in the specification, of 30 microns. No detrimental phases were identified at the ferrite/austenite interfaces, but the ferrite phase presented a rough aspect. Higher magnification analysis would be required to identify precipitation.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrographic detail of the ferrite and austenite structure in the transverse section of the forged bar, in the center of the thickness.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the ferrite and austenite structure in the longitudinal section of the forged bar, in the center of the thickness.
55
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
ML00110 — Non Conformance in Spray and Fuse PinM - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Micrography, as polished, of the transverse section of the forged pin with the layer applied by a (thermal) spray and fuse process. The layer was melted after thermal spray application and the layer presents a continuous matrix, but there are globular oxides and pores entrapped.
36
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - As polished micrographyDf - Surface Layer
Micrographic detail, as polished, of the transverse section of the forged pin at the interface between the pin and the spray and fuse layer. The interface presents globular oxides and small pores, entrapped.
35
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - As polished micrographyDf - Surface Layer
Low magnification micrography of the interface between the pin and the spray and fuse layer. Close to the surface, under the layer, the pin presents a ferritic perlitic structure, non conform with the high strenght requirement. Transverse section.
37
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - As polished micrographyDf - Low Mag
Micrography of the pin close to the interface with the spray and fuse layer. Transverse section. The fuse was conducted in high temperature and the pin was cooled very slowly, forming a ferritic-perlitic structure even for this high hardenability base metal.
35
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Low magnification micrography of the pin in the center of the 25 mm thickness. Ferritic-pearlitic structure of the material that slowly cooled after spray and fuse application. Transverse section.
24
VIEW
ML00110 / Jan.2018
Non Conformance in Spray and Fuse Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Base Metal

+5 more from this case →

ML00116 — CMn Steel Structural Tubing 6 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic banded structure.
30
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Bands of pearlite colonies. Refined grains.
26
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of a transverse section of the tubing in the center of the thickness. Ferritic-pearlitic structure. The structure is fully ferritic in a small extension at the surface, due to a decarburization effect during manufacturing.
26
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrographic detail of a transverse section of the tubing, close to the internal surface. Ferritic-pearlitic structure, refined.
20
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00115 — CMn Steel Structural Tubing 5 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Banded structure, ferritic-pearlitic.
16
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. The pearlite is banded and presented a coalesced aspect.
12
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrographic detail of a transverse section of the tubing, at the external surface. Ferritic-pearlitic structure. The roughness of the surface is high because the structure was painted and a blasting treatment was probably applied to the surface to improve adherence.
15
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrographic detail of a transverse section of the tubing, close to the internal surface. Ferritic-pearlitic structure. Very close to the surface the amount of ferrite is higher than in the center and the grain is coarser, due to a decarburization effect probably occurred when the surface was exposed to high temperature during manufacturing.
13
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00114 — CMn Steel Structural Tubing 8 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic banded structure.
29
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Bands of pearlite colonies. Refined grains.
29
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of a transverse section of the tubing, at the external surface. Ferritic-pearlitic structure. The roughness of the surface is high because the structure was painted and a blasting treatment was probably applied to the surface to improve adherence.
20
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of a transverse section of the tubing, close to the internal surface. Ferritic-pearlitic structure, refined.
16
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00113 — Autogenous Weld of a Carbon Steel WireM - Medium Carbon SteelP - WireAp - OffshoreCd - Welding
Micrography of a longitudinal section of a 4 mm diameter wire base metal, presenting a strain hardened and aligned pearlitic structure.
42
VIEW
ML00113 / Jan.2018
Autogenous Weld of a Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Low magnification micrography of a longitudinal section of a 4 mm diameter base metal wire, presenting a strain hardened and aligned pearlitic structure.
32
VIEW
ML00113 / Jan.2018
Autogenous Weld of a Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Low magnification micrography of a longitudinal section of a 4 mm diameter wire, at the region where the pearlitic strain hardened wire is affected by the welding. The base metal is to the left side and the region of the HAZ that starts with a grain growth is to the right side.
24
VIEW
ML00113 / Jan.2018
Autogenous Weld of a Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of a longitudinal section of a 4 mm diameter wire, at the heat affected zone created by the autogenous welding, presenting a tempered martensitic structure.
19
VIEW
ML00113 / Jan.2018
Autogenous Weld of a Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of a longitudinal section of a 4 mm diameter wire, at the heat affected zone created by the autogenous welding, presenting a tempered martensitic structure.
23
VIEW
ML00113 / Jan.2018
Autogenous Weld of a Carbon Steel Wire
M - Medium Carbon SteelP - WireAp - OffshoreCd - Welding
Cm - Nital Etched Micrography by OMDf - Martensite

+3 more from this case →

ML00112 — 1" XXS Pipe Not Qualified For Low TempM - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Micrography of a transverse section of the pipe, close to the external surface (OD). The pipe presented a predominatly ferritic structure.
43
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of a transverse section of the pipe, close to the external surface (OD). The pipe presented a 0.2 mm decarburized layer, fully ferritic.
35
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of a transverse section of the pipe, close to the external surface (OD). The pipe presented a predominatly ferritic structure.
31
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Predominantly Ferritic
Micrography of a transverse section of the pipe, close to the internal surface (ID). The pipe presented a predominatly ferritic structure.
29
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
Micrography of a transverse section of the pipe, close to the internal surface (ID). The pipe presented a predominatly ferritic structure.
22
VIEW
ML00112 / Dec.2017
1" XXS Pipe Not Qualified For Low Temp
M - Low Carbon SteelP - Seamless PipeAp - RefineryCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface

+2 more from this case →