Optical Microscope

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Optical Microscope — sub-branches

As polished micrography 43Eletrolytically Etched Micrography by OM 6Glyceregia Etched Micrography by OM 6Kalling Etched Micrography by OM 64Micrography by OM 26Micrography by OM using A262 Method A 58NaOH Electrolytic Etched Micro 52Nital Etched Micrography by OM 381Oxalic Acid Electrolytic Etch 13

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Longitudinal section micrography in a position of the thread, far from the failure. The stud presented a quenching and tempering structure and the thread was machined.
84
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
106
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrographic aspect of the rolled thread that was heat treated later. Longitudinal section.
134
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
74
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Nitronic 60 cylinder. Micrography of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, equiaxial grains, and evidences of the manufacturing process by hot forming.
179
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrographic detail of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Pearlite colonies in bands.
401
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of a transverse section of the 5 mm thick tubing, in the center of the thickness. Ferritic-pearlitic structure, with the pearlite presenting a coalesced aspect. The tubing was in service at ambient temperature, painted, and the coalesced aspect was generated before service, perhaps during the tubing manufacturing.
393
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Pearlite colonies in bands.
346
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite

More from these cases

ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Microstructure of the stud in the longitudinal section, presenting segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration.
69
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Microstructure of the stud in the longitudinal section, out of a region of segregation, where the tempered martensitic microstructure appears more uniform.
72
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration. The localized microhardness (50g) in the band showed levels about 540HV, and out of the band, in the same localtion, presented an average hardness of 321 HV, indicating that the material is non uniform in the regions where there are bands.
66
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrographic detail of the martensitic structure of the stud in the longitudinal section, out of a region of segregation, where the microstructure appears more uniform and the microhardness is about 370HV (50g).
62
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Low magnification micrography of a stud longitudinal section in the first thread fillet adjacent to the fracture, presenting a large secondary crack without any deformation evidence. This reveals a brittle material behavior, although the hardness measured at the stud end revealed 33HRc, as should be expected by the material specification.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Secondary Cracks

+17 more from this case →

ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic detail of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
102
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Metallographic detail of the large amount of sigma phase, associated to the ferritic structure.
105
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Microstructural analysis of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
67
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
63
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
61
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite

+8 more from this case →

ML00130 — Fatigue Fracture of Overloaded BoltsM - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Micrographic aspect of the rolled thread that was heat treated later. Longitudinal section. The bolt was quenched and tempered to 30HRc and presented a martensitic structure.
124
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrographic detail of the rolled thread that was heat treated later. The bolt was quenched and tempered to 30 HRc and presented a martensitic structure.
110
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
The microstructure of the bolt is martensitic in the center of the thickness. Longitudinal section.
110
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
The microstructure of the bolt is martensitic in the center of the thickness. Longitudinal section.
103
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic aspect of the rolled thread that was heat treated later. Longitudinal section.
115
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - At the Surface

+3 more from this case →

ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
61
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. The ferrite amount, measured by metallographic method, manual counting, is 59%.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. The average austenite spacing is 80 microns, a lot larger than the maximum allowed in the specification, of 30 microns. No detrimental phases were identified at the ferrite/austenite interfaces, but the ferrite phase presented a rough aspect. Higher magnification analysis would be required to identify precipitation.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrographic detail of the ferrite and austenite structure in the transverse section of the forged bar, in the center of the thickness.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the ferrite and austenite structure in the longitudinal section of the forged bar, in the center of the thickness.
55
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
ML00121 — Pitting Corrosion in a Subsea SystemM - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Nitronic 60 cylinder. Micrography of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, with some aligned non metallic inclusions.
157
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Nitronic 60 cylinder. Micrographic detail of the longitudinal section in the center of the thickness, presenting a fully austenitic microstructure, equiaxial grains, typical of a solution annealed condition.
136
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Nitronic 60 cylinder. Micrography of the longitudinal section close to the surface, presenting a fully austenitic microstructure, with a shadow close to the external surface that is associated to a small layer of strain hardened structure (deformation twins).
133
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Nitronic 60 cylinder. Micrography of the longitudinal section close to the surface, presenting a fully austenitic microstructure, with a 0.15mm layer of strain hardened structure (deformation twins).
120
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Strain Hardened
Nitronic 60 cylinder. Micrographic detail of the longitudinal section close to the surface, presenting a fully austenitic microstructure, with a layer of strain hardened structure (deformation twins).
113
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Strain Hardened

+4 more from this case →

ML00116 — CMn Steel Structural Tubing 6 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic banded structure.
30
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Bands of pearlite colonies. Refined grains.
26
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of a transverse section of the tubing in the center of the thickness. Ferritic-pearlitic structure. The structure is fully ferritic in a small extension at the surface, due to a decarburization effect during manufacturing.
26
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrographic detail of a transverse section of the tubing, close to the internal surface. Ferritic-pearlitic structure, refined.
20
VIEW
ML00116 / Jan.2018
CMn Steel Structural Tubing 6 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00115 — CMn Steel Structural Tubing 5 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Banded structure, ferritic-pearlitic.
16
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. The pearlite is banded and presented a coalesced aspect.
12
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrographic detail of a transverse section of the tubing, at the external surface. Ferritic-pearlitic structure. The roughness of the surface is high because the structure was painted and a blasting treatment was probably applied to the surface to improve adherence.
15
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrographic detail of a transverse section of the tubing, close to the internal surface. Ferritic-pearlitic structure. Very close to the surface the amount of ferrite is higher than in the center and the grain is coarser, due to a decarburization effect probably occurred when the surface was exposed to high temperature during manufacturing.
13
VIEW
ML00115 / Jan.2018
CMn Steel Structural Tubing 5 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
ML00114 — CMn Steel Structural Tubing 8 mm thickM - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Low magnification micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic banded structure.
29
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the tubing, in the center of the thickness. Ferritic-pearlitic structure. Bands of pearlite colonies. Refined grains.
30
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of a transverse section of the tubing, at the external surface. Ferritic-pearlitic structure. The roughness of the surface is high because the structure was painted and a blasting treatment was probably applied to the surface to improve adherence.
20
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrography of a transverse section of the tubing, close to the internal surface. Ferritic-pearlitic structure, refined.
16
VIEW
ML00114 / Jan.2018
CMn Steel Structural Tubing 8 mm thick
M - CMn SteelP - Seamless Round ShapeAp - StructureCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface